JPS6471824A - Production of aromatic fluoride - Google Patents
Production of aromatic fluorideInfo
- Publication number
- JPS6471824A JPS6471824A JP22773687A JP22773687A JPS6471824A JP S6471824 A JPS6471824 A JP S6471824A JP 22773687 A JP22773687 A JP 22773687A JP 22773687 A JP22773687 A JP 22773687A JP S6471824 A JPS6471824 A JP S6471824A
- Authority
- JP
- Japan
- Prior art keywords
- hydrogen fluoride
- fluoride
- aromatic
- base
- light irradiation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
- B01J19/122—Incoherent waves
- B01J19/123—Ultra-violet light
Abstract
PURPOSE:To obtain an aromatic fluoride safely and in high yield, by reacting an aromatic diazonium halogenoborate with hydrogen fluoride or hydrogen fluoride and a base under light irradiation. CONSTITUTION:An aromatic diazonium halogenoborate is reacted with hydrogen fluoride or hydrogen fluoride and a base under light irradiation at -50-100 deg.C to give an aromatic fluoride. A high-temperature mercury vapor lamp may be cited as a light source used for light irradiation. Irradiation time is 5min-24 hr. An amine compound except a primary amine and an ether compound may be preferable as the base and the amount of the base used is 5-90wt.% based on sum of hydrogen fluoride and the base. The reaction can also be carried out in a solvent such as chlorobenzene, CCl4 or pentane to dissolve the aromatic fluoride but not hydrogen fluoride.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP22773687A JPS6471824A (en) | 1987-09-11 | 1987-09-11 | Production of aromatic fluoride |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP22773687A JPS6471824A (en) | 1987-09-11 | 1987-09-11 | Production of aromatic fluoride |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS6471824A true JPS6471824A (en) | 1989-03-16 |
Family
ID=16865556
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP22773687A Pending JPS6471824A (en) | 1987-09-11 | 1987-09-11 | Production of aromatic fluoride |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS6471824A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH03190826A (en) * | 1989-12-20 | 1991-08-20 | Tokuyama Soda Co Ltd | Method for treating fluorinated product |
-
1987
- 1987-09-11 JP JP22773687A patent/JPS6471824A/en active Pending
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH03190826A (en) * | 1989-12-20 | 1991-08-20 | Tokuyama Soda Co Ltd | Method for treating fluorinated product |
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