JPS6438059A - Production of 1,7-di(4-hydroxyphenylthio)-3,5-dioxaheptane - Google Patents
Production of 1,7-di(4-hydroxyphenylthio)-3,5-dioxaheptaneInfo
- Publication number
- JPS6438059A JPS6438059A JP62194027A JP19402787A JPS6438059A JP S6438059 A JPS6438059 A JP S6438059A JP 62194027 A JP62194027 A JP 62194027A JP 19402787 A JP19402787 A JP 19402787A JP S6438059 A JPS6438059 A JP S6438059A
- Authority
- JP
- Japan
- Prior art keywords
- production
- dioxaheptane
- hydroxyphenylthio
- organic solvent
- steps
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M5/00—Duplicating or marking methods; Sheet materials for use therein
- B41M5/26—Thermography ; Marking by high energetic means, e.g. laser otherwise than by burning, and characterised by the material used
- B41M5/30—Thermography ; Marking by high energetic means, e.g. laser otherwise than by burning, and characterised by the material used using chemical colour formers
- B41M5/333—Colour developing components therefor, e.g. acidic compounds
- B41M5/3333—Non-macromolecular compounds
- B41M5/3335—Compounds containing phenolic or carboxylic acid groups or metal salts thereof
- B41M5/3336—Sulfur compounds, e.g. sulfones, sulfides, sulfonamides
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Heat Sensitive Colour Forming Recording (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE:To obtain the objective compound in high efficiency, without separating intermediate product in each step, by carrying out the whole steps in the same water-soluble organic solvent in the production of the titled compound from phenol and sulfur chloride in 3 steps. CONSTITUTION:1,7-Di(4-hydroxyphenylthio)-3,5-dioxaheptane is produced by (1) reacting phenol with sulfur chloride, (2) reducing and decomposing the resultant bis(4-hydroxyphenyl) disulfide into 4-mercaptophenol in the presence of a reducing agent or a reduction catalyst and (3) reacting the reduction product with bis(2-haloethoxy)methane. In the above process, the whole steps are carried out in the same water-soluble organic solvent to enable the production of the objective compound without separating and purifying the intermediate products in each step. The reaction efficiency can be improved by this process.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP62194027A JPS6438059A (en) | 1987-08-03 | 1987-08-03 | Production of 1,7-di(4-hydroxyphenylthio)-3,5-dioxaheptane |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP62194027A JPS6438059A (en) | 1987-08-03 | 1987-08-03 | Production of 1,7-di(4-hydroxyphenylthio)-3,5-dioxaheptane |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS6438059A true JPS6438059A (en) | 1989-02-08 |
Family
ID=16317723
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP62194027A Pending JPS6438059A (en) | 1987-08-03 | 1987-08-03 | Production of 1,7-di(4-hydroxyphenylthio)-3,5-dioxaheptane |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS6438059A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9694363B2 (en) | 2013-09-04 | 2017-07-04 | Metso Minerals, Inc. | Mineral material processing plant and a method for operating a processing plant |
-
1987
- 1987-08-03 JP JP62194027A patent/JPS6438059A/en active Pending
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9694363B2 (en) | 2013-09-04 | 2017-07-04 | Metso Minerals, Inc. | Mineral material processing plant and a method for operating a processing plant |
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