JPS633030B2 - - Google Patents

Info

Publication number: JPS633030B2
Authority: JP; Japan
Prior art keywords: compound; compounds; polyfluorinated; perfluorinated; reaction
Prior art date: 1985-09-03
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

JP60193042A

Other languages

English (en)

Japanese (ja)

Other versions

JPS6254093A (ja

Inventor

Shinsuke Morikawa

Mikio Sasabe

Hitoshi Matsuo

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

AGC Inc

Original Assignee

Asahi Glass Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1985-09-03

Filing date

1985-09-03

Publication date

1988-01-21

1985-09-03 Application filed by Asahi Glass Co Ltd filed Critical Asahi Glass Co Ltd

1985-09-03 Priority to JP60193042A priority Critical patent/JPS6254093A/ja

1987-03-09 Publication of JPS6254093A publication Critical patent/JPS6254093A/ja

1988-01-21 Publication of JPS633030B2 publication Critical patent/JPS633030B2/ja

Status Granted legal-status Critical Current

Links

238000003682 fluorination reaction Methods 0.000 claims description 20
-1 perfluoro compound Chemical class 0.000 claims description 13
238000000034 method Methods 0.000 claims description 11
238000006243 chemical reaction Methods 0.000 claims description 10
150000002894 organic compounds Chemical class 0.000 claims description 9
238000004519 manufacturing process Methods 0.000 claims description 3
150000001875 compounds Chemical class 0.000 description 37
239000007789 gas Substances 0.000 description 16
239000000047 product Substances 0.000 description 11
239000011737 fluorine Substances 0.000 description 10
229910052731 fluorine Inorganic materials 0.000 description 10
NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical compound FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 description 10
YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 9
239000007795 chemical reaction product Substances 0.000 description 7
239000002994 raw material Substances 0.000 description 7
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 6
238000005868 electrolysis reaction Methods 0.000 description 6
238000000354 decomposition reaction Methods 0.000 description 5
239000000126 substance Substances 0.000 description 5
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 4
238000004821 distillation Methods 0.000 description 4
125000004435 hydrogen atom Chemical group [H]* 0.000 description 4
229910000040 hydrogen fluoride Inorganic materials 0.000 description 4
238000005406 washing Methods 0.000 description 4
239000007864 aqueous solution Substances 0.000 description 3
238000003776 cleavage reaction Methods 0.000 description 3
230000000052 comparative effect Effects 0.000 description 3
230000007017 scission Effects 0.000 description 3
NJBCRXCAPCODGX-UHFFFAOYSA-N 2-methyl-n-(2-methylpropyl)propan-1-amine Chemical compound CC(C)CNCC(C)C NJBCRXCAPCODGX-UHFFFAOYSA-N 0.000 description 2
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
SMWDFEZZVXVKRB-UHFFFAOYSA-N Quinoline Chemical compound N1=CC=CC2=CC=CC=C21 SMWDFEZZVXVKRB-UHFFFAOYSA-N 0.000 description 2
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
239000002473 artificial blood Substances 0.000 description 2
238000009835 boiling Methods 0.000 description 2
125000001153 fluoro group Chemical group F* 0.000 description 2
239000012535 impurity Substances 0.000 description 2
229910052759 nickel Inorganic materials 0.000 description 2
RVZRBWKZFJCCIB-UHFFFAOYSA-N perfluorotributylamine Chemical compound FC(F)(F)C(F)(F)C(F)(F)C(F)(F)N(C(F)(F)C(F)(F)C(F)(F)C(F)(F)F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F RVZRBWKZFJCCIB-UHFFFAOYSA-N 0.000 description 2
231100000331 toxic Toxicity 0.000 description 2
230000002588 toxic effect Effects 0.000 description 2
QDGSXOLPRIFRJV-UHFFFAOYSA-N 2-(pentoxymethyl)oxolane Chemical compound CCCCCOCC1CCCO1 QDGSXOLPRIFRJV-UHFFFAOYSA-N 0.000 description 1
229910021555 Chromium Chloride Inorganic materials 0.000 description 1
229910021583 Cobalt(III) fluoride Inorganic materials 0.000 description 1
229910021380 Manganese Chloride Inorganic materials 0.000 description 1
GLFNIEUTAYBVOC-UHFFFAOYSA-L Manganese chloride Chemical compound Cl[Mn]Cl GLFNIEUTAYBVOC-UHFFFAOYSA-L 0.000 description 1
239000002253 acid Substances 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
150000001299 aldehydes Chemical class 0.000 description 1
125000002723 alicyclic group Chemical group 0.000 description 1
239000003513 alkali Substances 0.000 description 1
150000008064 anhydrides Chemical class 0.000 description 1
JHXKRIRFYBPWGE-UHFFFAOYSA-K bismuth chloride Chemical compound Cl[Bi](Cl)Cl JHXKRIRFYBPWGE-UHFFFAOYSA-K 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
229910052799 carbon Inorganic materials 0.000 description 1
150000001735 carboxylic acids Chemical class 0.000 description 1
239000000969 carrier Substances 0.000 description 1
208000013557 cerebral hemisphere cancer Diseases 0.000 description 1
201000008860 cerebrum cancer Diseases 0.000 description 1
VYLVYHXQOHJDJL-UHFFFAOYSA-K cerium trichloride Chemical compound Cl[Ce](Cl)Cl VYLVYHXQOHJDJL-UHFFFAOYSA-K 0.000 description 1
125000001309 chloro group Chemical class Cl* 0.000 description 1
QSWDMMVNRMROPK-UHFFFAOYSA-K chromium(3+) trichloride Chemical compound [Cl-].[Cl-].[Cl-].[Cr+3] QSWDMMVNRMROPK-UHFFFAOYSA-K 0.000 description 1
GVPFVAHMJGGAJG-UHFFFAOYSA-L cobalt dichloride Chemical compound [Cl-].[Cl-].[Co+2] GVPFVAHMJGGAJG-UHFFFAOYSA-L 0.000 description 1
YCYBZKSMUPTWEE-UHFFFAOYSA-L cobalt(ii) fluoride Chemical compound F[Co]F YCYBZKSMUPTWEE-UHFFFAOYSA-L 0.000 description 1
ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 description 1
230000000694 effects Effects 0.000 description 1
230000005611 electricity Effects 0.000 description 1
150000002170 ethers Chemical class 0.000 description 1
238000000605 extraction Methods 0.000 description 1
125000000524 functional group Chemical group 0.000 description 1
238000004817 gas chromatography Methods 0.000 description 1
150000004820 halides Chemical class 0.000 description 1
150000008282 halocarbons Chemical class 0.000 description 1
229910000856 hastalloy Inorganic materials 0.000 description 1
239000001307 helium Substances 0.000 description 1
229910052734 helium Inorganic materials 0.000 description 1
SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
150000002391 heterocyclic compounds Chemical class 0.000 description 1
239000010720 hydraulic oil Substances 0.000 description 1
229930195733 hydrocarbon Natural products 0.000 description 1
150000002430 hydrocarbons Chemical class 0.000 description 1
239000011261 inert gas Substances 0.000 description 1
238000001802 infusion Methods 0.000 description 1
238000002347 injection Methods 0.000 description 1
239000007924 injection Substances 0.000 description 1
FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 description 1
150000002576 ketones Chemical class 0.000 description 1
HWSZZLVAJGOAAY-UHFFFAOYSA-L lead(II) chloride Chemical compound Cl[Pb]Cl HWSZZLVAJGOAAY-UHFFFAOYSA-L 0.000 description 1
239000010687 lubricating oil Substances 0.000 description 1
229940099607 manganese chloride Drugs 0.000 description 1
235000002867 manganese chloride Nutrition 0.000 description 1
239000011565 manganese chloride Substances 0.000 description 1
239000000463 material Substances 0.000 description 1
239000000203 mixture Substances 0.000 description 1
229910052757 nitrogen Inorganic materials 0.000 description 1
QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
239000003921 oil Substances 0.000 description 1
FRZFEPXEUZSBLA-UHFFFAOYSA-N perfluoroadamantane Chemical class FC1(F)C(C2(F)F)(F)C(F)(F)C3(F)C(F)(F)C1(F)C(F)(F)C2(F)C3(F)F FRZFEPXEUZSBLA-UHFFFAOYSA-N 0.000 description 1
150000002989 phenols Chemical class 0.000 description 1
238000010992 reflux Methods 0.000 description 1
238000000926 separation method Methods 0.000 description 1
238000007086 side reaction Methods 0.000 description 1
239000007858 starting material Substances 0.000 description 1
238000006467 substitution reaction Methods 0.000 description 1
150000003461 sulfonyl halides Chemical class 0.000 description 1
229940126585 therapeutic drug Drugs 0.000 description 1
229910052723 transition metal Inorganic materials 0.000 description 1
IMFACGCPASFAPR-UHFFFAOYSA-N tributylamine Chemical compound CCCCN(CCCC)CCCC IMFACGCPASFAPR-UHFFFAOYSA-N 0.000 description 1

Landscapes

Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)

JP60193042A 1985-09-03 1985-09-03 パ−フルオロ化合物の製造方法 Granted JPS6254093A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP60193042A JPS6254093A (ja)	1985-09-03	1985-09-03	パ−フルオロ化合物の製造方法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP60193042A JPS6254093A (ja)	1985-09-03	1985-09-03	パ−フルオロ化合物の製造方法

Publications (2)

Publication Number	Publication Date
JPS6254093A JPS6254093A (ja)	1987-03-09
JPS633030B2 true JPS633030B2 (de)	1988-01-21

Family

ID=16301202

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP60193042A Granted JPS6254093A (ja)	1985-09-03	1985-09-03	パ−フルオロ化合物の製造方法

Country Status (1)

Country	Link
JP (1)	JPS6254093A (de)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS63139154A (ja) *	1986-12-01	1988-06-10	Tokuyama Soda Co Ltd	バ−フルオロトリアルキルアミンの製造方法
EP0271272B1 (de) *	1986-12-01	1992-04-15	Tokuyama Corporation	Verfahren zur Herstellung von organischen Perfluoro-Verbindungen

Citations (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2831035A (en) *	1956-02-15	1958-04-15	Allied Chem & Dye Corp	Manufacture of fluorocarbons
US3709800A (en) *	1971-03-19	1973-01-09	Phillips Petroleum Co	Process for preparing perfluorocarbon compounds
US3840445A (en) *	1972-05-15	1974-10-08	Phillips Petroleum Co	Two-stage electrochemical octafluoropropane production
US4035250A (en) *	1976-03-11	1977-07-12	Phillips Petroleum Company	Production of perfluoro-n-heptane

1985
- 1985-09-03 JP JP60193042A patent/JPS6254093A/ja active Granted

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2831035A (en) *	1956-02-15	1958-04-15	Allied Chem & Dye Corp	Manufacture of fluorocarbons
US3709800A (en) *	1971-03-19	1973-01-09	Phillips Petroleum Co	Process for preparing perfluorocarbon compounds
US3840445A (en) *	1972-05-15	1974-10-08	Phillips Petroleum Co	Two-stage electrochemical octafluoropropane production
US4035250A (en) *	1976-03-11	1977-07-12	Phillips Petroleum Company	Production of perfluoro-n-heptane

Also Published As

Publication number	Publication date
JPS6254093A (ja)	1987-03-09

Publication	Publication Date	Title
EP0271272B1 (de)	1992-04-15	Verfahren zur Herstellung von organischen Perfluoro-Verbindungen
EP0062430B1 (de)	1986-11-12	Verfahren zur Herstellung von (omega-Fluorsulfonyl)-haloaliphatischen Carbonsäurefluoriden
US4124456A (en)	1978-11-07	Method of tris(perfluoroalkyl)phosphine oxides
JPS633030B2 (de)	1988-01-21
JPH0463055B2 (de)	1992-10-08
JP4744356B2 (ja)	2011-08-10	電解フッ素化方法
JP2006348381A (ja)	2006-12-28	電解フッ素化による有機化合物の製造方法
EP0099652B1 (de)	1987-09-23	Perfluortricyclische Aminverbindungen
EP0103358A1 (de)	1984-03-21	Tricyclische Perfluor-1-aza-Verbindung
JPH0261081A (ja)	1990-03-01	ペルフルオロカルボン酸またはその可溶性塩を電解的に脱カルボキシル化しそしてその際に生じた遊離基を次いで二量体化する方法
US4387007A (en)	1983-06-07	Process for the manufacture of an aldehyde
EP0219484B1 (de)	1990-07-25	Elektrolytische Herstellung von Perfluoralkansäuren und Perfluoralkanolen
US3876515A (en)	1975-04-08	Method for manufacture of perfluorocyclohexane derivatives
US4120761A (en)	1978-10-17	Electrochemical process for the preparation of acetals of 2-haloaldehydes
JP3846778B2 (ja)	2006-11-15	有機エーテル化合物の電解フッ素化方法
EP0047947B1 (de)	1984-03-14	Omega-Fluorsulfato-perfluor-(2-methyl-alkan-3-one) sowie Verfahren zur Herstellung von Perfluorisopropylketocarbonsäurefluoriden über die erstgenannten Verbindungen
JPH0230785A (ja)	1990-02-01	電解フッ素化方法
RU2107751C1 (ru)	1998-03-27	Способ получения высших перфтормонокарбоновых кислот
JPS6261116B2 (de)	1987-12-19
EP0121614B1 (de)	1987-06-03	Perfluorotricyclische Aminverbindungen
JPS5877891A (ja)	1983-05-11	酸化トリス（パ−フルオロアルキル）ホスフインおよびその製造方法
JPS5917119B2 (ja)	1984-04-19	酸化トリス（パ−フルオロアルキル）ホスフインおよびその製造方法
JPH03240983A (ja)	1991-10-28	パラフルオロベンズアルデヒドの製造方法
DE2620086C3 (de)	1980-02-14	Tris-(perfluoralkyl)-phosphinox'ide und Verfahren zu deren Herstellung
JPH0157108B2 (de)	1989-12-04