JPS62136300A - Dehydration treatment of sludge - Google Patents

Dehydration treatment of sludge

Info

Publication number
JPS62136300A
JPS62136300A JP60275604A JP27560485A JPS62136300A JP S62136300 A JPS62136300 A JP S62136300A JP 60275604 A JP60275604 A JP 60275604A JP 27560485 A JP27560485 A JP 27560485A JP S62136300 A JPS62136300 A JP S62136300A
Authority
JP
Japan
Prior art keywords
sludge
water
heated
dehydration
containing sludge
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP60275604A
Other languages
Japanese (ja)
Inventor
Takashi Furukawa
高司 古川
Toshiharu Kimura
木村 年治
Tomio Wada
和田 富男
Takumi Nonaka
巧 野中
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yoshikawa Kogyo Co Ltd
Nippon Steel Corp
Original Assignee
Yoshikawa Kogyo Co Ltd
Nippon Steel Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Yoshikawa Kogyo Co Ltd, Nippon Steel Corp filed Critical Yoshikawa Kogyo Co Ltd
Priority to JP60275604A priority Critical patent/JPS62136300A/en
Publication of JPS62136300A publication Critical patent/JPS62136300A/en
Pending legal-status Critical Current

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  • Filtration Of Liquid (AREA)
  • Treatment Of Sludge (AREA)

Abstract

PURPOSE:To efficiently dehydrate sludge, by a method wherein water-containing sludge is stirred under heating to be subjected to dehydration treatment and filter cloth after dehydration is washed with warm water. CONSTITUTION:Water-containing sludge S stirred under heating in a first stirring tank 1 is transferred to a second stirring tank 2 by a pump 9 to be heated by a steam blow-in pipe 6 and stirred by a stirrer 8 while held to 40-75 deg.C. Subsequently, the heated sludge is charged in the filter cloth 11 of the dehydrator 10 of a second process to be subjected to dehydration treatment to obtain a sludge cake C. After the sludge cake C was taken out, washing water stored in a water receiving tank 12 and heated to 40-75 deg.C by the steam blow-in pipe 6 is sprayed to the filter cloth 11 after dehydration treatment from a nozzle 14 to wash the same. By this method, the generation of the contamination and clogging of the filter cloth is reduced and operating efficiency is enhanced.

Description

【発明の詳細な説明】 (産業上の利用分野) 本発明は含水スラッジの脱水処理にかかり、特に極微粒
のスラッジ或は油類等の有機物を含むスラッジ等の非容
易性の高いスラッジを対象とした脱水処理方法に関する
ものである。
Detailed Description of the Invention (Industrial Application Field) The present invention relates to the dehydration treatment of water-containing sludge, and is particularly applicable to highly difficult-to-easy sludge such as ultrafine sludge or sludge containing organic matter such as oil. The present invention relates to a dehydration treatment method.

(従来の技術) 従来、含水スラッジから脱水され友スラツジケ回収する
中段としては、一般に、スラッジを撹拌槽中で窩部撹拌
した後、脱水機のP布を用いて脱水し、回収を行なって
いる。ま友、Fiが汚れ、目詰シ等を起し九場合は常温
水によってF布t−洗浄する方法をとっている。
(Prior art) Conventionally, as a middle stage for dewatering and recovering sludge from water-containing sludge, the sludge is generally stirred in the cavity in a stirring tank, then dehydrated using a P cloth of the dehydrator, and then recovered. . However, if the Fi becomes dirty or clogged, the method is to wash the F cloth with room-temperature water.

また、特に脱水処理が困難なものとしてエマルジョン化
し几含油排水処理スカムがあシ、例えば特公昭54−2
8450号公報に示されている工うに80℃以上に加熱
してエマルジョンを破壊し、遠心脱水機にニジ脱水する
方法が知られている。
In addition, it is particularly difficult to dehydrate the scum that is formed into an emulsion and treated with oil-containing wastewater.
A method disclosed in Japanese Patent Application No. 8450 is known in which the emulsion is broken by heating to 80° C. or higher, and the emulsion is dehydrated using a centrifugal dehydrator.

(発明が解決しようとする問題点) しかし、従来の一般的なスラッジ回収方法では以下に示
す欠点がある。
(Problems to be Solved by the Invention) However, the conventional general sludge recovery method has the following drawbacks.

即ち、回収するスラッジが弱酸スラッジのように粒度が
100μm以下と極めて微粒で親水性が強い場合はゾル
化し、FlにLる脱水ができない。
That is, when the sludge to be recovered is extremely fine with a particle size of 100 μm or less and has strong hydrophilic properties, such as weak acid sludge, it becomes a sol and cannot be dehydrated to Fl.

また、圧砥スラッジのように圧砥油、グリース等の有機
物を含んでいる場合はF布の汚れ、目詰りが発生しやす
(、を九富温水による洗浄では効果か弱いため脱水処理
巡、稼働尤の低下が著しく、P布破損等のtJ14度も
高い。
In addition, when grinding sludge contains organic substances such as grinding oil and grease, the F cloth is likely to become stained and clogged. The decrease in the resistance is remarkable, and the tJ14 degrees due to P fabric damage etc. are also high.

また、加熱管内で80℃以上に加熱してエマルジョンを
破壊する手段が適用される含油排水処理スカムの場合に
は弱酸スラッジ、EEiスラッジ等では撹拌槽内で多量
のスラッジを加熱するため、75℃以上に加熱すると含
水スラッジからの水分蒸発が著しく、撹拌槽への付着が
多くなる。ま友、スラッジ水分減少のため粘性が増し、
かえって脱水処理時間が低下する。ζらに、受水槽、撹
拌槽内の含水スラッジ全体ypgoc以上に加熱、保温
することは経済的に困難である。
In addition, in the case of oil-containing wastewater treatment scum, which is heated to 80°C or higher in a heating tube to destroy the emulsion, weak acid sludge, EEi sludge, etc. are heated to 75°C in order to heat a large amount of sludge in a stirring tank. If the sludge is heated to a higher temperature, water evaporates significantly from the water-containing sludge, resulting in increased adhesion to the stirring tank. Mayu, the viscosity increases due to the decrease in sludge moisture,
On the contrary, the dehydration processing time is reduced. In addition, it is economically difficult to heat and keep the entire water-containing sludge in the water receiving tank and stirring tank above ypgoc.

本発明は、これらの回収不能または困難な弱酸スラッジ
お工び圧廷スラッジ等を効巡s(脱水し。
The present invention effectively dewaters these unrecoverable or difficult weak acid sludges, compressed sludges, etc.

回収する方法を提供することを目的とする。The purpose is to provide a method for recovering.

(問題点を解決するための手段) 本発明は1粒度が101)μm以下の極微粒、或は油類
等の有機物を含んだ含水スラッジを脱水するに際し、含
水スラッジを貯溜、撹拌する第1工程と、次いで脱水す
るgz工程とに工す処理する方法において、第1工程で
含水スラッジの@度を40〜75℃に加熱しながら撹拌
し、第2工程で脱水処理を行ない、かつ脱水後の戸布を
40〜75℃の温水にて洗浄することを特徴とするスラ
ッジの脱水処理方法である。第1工程での含水スラッジ
の加熱、撹拌は、第1工程に設けられた含水スラッジ加
熱手段、含水スラッジ流動手段にニジ行なう。
(Means for Solving the Problems) The present invention provides a first method for storing and stirring the water-containing sludge when dehydrating water-containing sludge containing ultrafine particles with a particle size of 101) μm or less or organic matter such as oil. In the method of processing in the step and the gz step of dehydration, in the first step, the water-containing sludge is stirred while being heated to 40 to 75°C, and in the second step, the dehydration treatment is performed, and after dehydration. This is a sludge dehydration treatment method characterized by washing a door cloth with hot water of 40 to 75°C. The heating and stirring of the water-containing sludge in the first step is carried out through the water-containing sludge heating means and the water-containing sludge flowing means provided in the first step.

(作用) 本発明における脱水処理の工程を第1図に示し7’C例
にもとづいて説明する。
(Function) The dehydration process in the present invention is shown in FIG. 1 and will be explained based on Example 7'C.

1け第1撹拌槽、2は第2撹拌酸である。処理対象の含
水スラッジSは貯溜するためにスラリーポンプ3によっ
て第1撹拌槽1に装入される。この際の含水スラッジS
の水分はスラリー輸迷に適した70〜80%に調整され
ており、常温である。
1 is a first stirring tank, and 2 is a second stirring acid. The water-containing sludge S to be treated is charged into the first stirring tank 1 by the slurry pump 3 for storage. At this time, water-containing sludge S
The moisture content of the slurry is adjusted to 70 to 80%, which is suitable for slurry transport, and the temperature is normal.

第1撹拌1)1)の開口部にはフィルター4がついてお
シ、大きな不純物等を除去する。
First stirring 1) A filter 4 is attached to the opening of 1) to remove dust and large impurities.

この撹拌槽1.2には貯溜されfc含水スラッジs2加
熱する装置として蒸気支g5、然気吹込管6が槽内に固
定もしくは移動可能なように設置はれている。蒸気吹込
量ならびに開閉はコック7で調整可能になっている。ま
友%含水スラッジSf:撹拌する友めの装置として撹拌
機8が付いている6加熱の手段としては電熱、燃焼熱等
が考えられ、含水スラッジを流wJζせる手段としては
槽自体の揺動、気体吹込み等が考えられる。加熱用の蒸
気吹込量にLつては蒸気にニジ撹拌を載るととも可能で
ある。
In this stirring tank 1.2, a steam branch g5 and a natural air blowing pipe 6 are fixedly or movably installed as devices for heating the fc water-containing sludge s2 stored in the stirring tank 1.2. The amount of steam blown and opening/closing can be adjusted with a cock 7. % Water-containing sludge Sf: A stirrer 8 is attached as a companion device for stirring 6 Electric heat, combustion heat, etc. can be considered as a means of heating, and shaking of the tank itself is a means to flow the water-containing sludge wJζ , gas blowing, etc. Depending on the amount of steam blown for heating, it is possible to add continuous stirring to the steam.

tg1撹拌槽1で加熱、撹拌された含水スラッジSはポ
ンプ9にて第2撹拌槽2へ移され、同様に蒸気吹込W6
に工り加熱され、撹拌機8にて撹拌される。この場合、
含水スラッジSは第1)を拌槽1にて加熱、昇温これて
いるので、その温度レベルを保持するに足シる熱tを必
要に応じて加えればよい。
The water-containing sludge S heated and stirred in the tg1 stirring tank 1 is transferred to the second stirring tank 2 by a pump 9, and similarly steam-injected W6
The mixture is then heated and stirred using a stirrer 8. in this case,
Since the water-containing sludge S (1) is heated and raised in temperature in the stirring tank 1, sufficient heat t to maintain the temperature level may be added as necessary.

しかし、ここで重要なことは、撹拌工程では含水スラッ
ジの温度を40〜75℃に保つべきであるということで
ある。この温度範囲に限定した理由は、次の通シである
。部ち、加熱これた含水スラッジは微粒子の凝集比が促
進されるとともに、熱変質にニジ親水性が低下するため
ゾル比しにぐ(なシ、水と粒子の分離が容易になる。ま
′fc、 ?布置れ、目詰シの原因となる油脂、グリー
ス等の有機物は昇温にニジ粘性が低下するとともに、一
部は加水分解を起して可溶性となる丸め、P7i5への
付着が減少し、汚れ、目詰シ発生頻度が低下し、回収効
惠が向上される。また、P布に有機物が付着して汚れ、
目詰りが生じた場合も、温水洗浄にニジ洗浄効果が向上
する。
However, what is important here is that the temperature of the water-containing sludge should be maintained at 40-75°C during the stirring process. The reason for limiting the temperature to this range is as follows. In addition, heated water-containing sludge promotes the agglomeration ratio of fine particles, and its hydrophilicity decreases due to thermal alteration, making it easier to separate water and particles than sol. fc, ?The viscosity of organic substances such as oils, fats, and greases that cause fabric placement and clogging decreases as the temperature rises, and some of them undergo hydrolysis and become soluble, resulting in less adhesion to P7i5. This reduces the frequency of dirt and clogging, and improves the recovery efficiency.Also, organic matter adheres to the P cloth and causes dirt,
Even when clogging occurs, the cleaning effect is improved by hot water cleaning.

而して、これらの効果を奏するためには含水スラッジの
温度は少なくとも40℃以上とする必要がある。これニ
ジ低温では脱水処理時間が長くなる。ま友、脱水後のス
ラッジケーキの水分も多く残ることになシ、スラッジケ
ーキの厚みを厚く処理することが困難となるなど、実用
的な価値を失なうことになる。一方、昇温による効果を
期待して必要以上の高温にしても、本願発明対象のスラ
ッジの場合は格別に効果が増大するものではなく、むし
ろ含水スラッジからの水分蒸気が著しく、撹拌飛への付
着が多ぐなったり、含水スラッジの粘性が増加するため
、脱水処理方法が低下する。さらに、加熱に要する費用
の節減を重視することがこの種の廃棄物の処理には重要
で、経済的な操業が最も大切な条件である。また、含水
スラッジ温度を上げることは撹拌設備や脱水設備の劣化
を促進する。以上のことから、含水スラッジの昇温の上
限を75℃に定めた。なお、実用的価値をスラッジの処
理量で評価すると第2図の如く浸る。
Therefore, in order to achieve these effects, the temperature of the water-containing sludge needs to be at least 40°C or higher. At lower temperatures, the dehydration process takes longer. However, since a large amount of moisture remains in the sludge cake after dehydration, it becomes difficult to treat the sludge cake to a thicker thickness, which results in loss of practical value. On the other hand, even if the temperature is raised to a higher temperature than necessary in the hope of achieving an effect from increasing the temperature, the effect will not be particularly increased in the case of the sludge that is the object of the present invention.In fact, the water vapor from the water-containing sludge will be significant, and the agitation will be affected. The dehydration process deteriorates due to increased adhesion and increased viscosity of the water-containing sludge. Furthermore, it is important to focus on reducing heating costs in the treatment of this type of waste, and economical operation is the most important condition. In addition, increasing the temperature of the water-containing sludge accelerates the deterioration of stirring equipment and dehydration equipment. Based on the above, the upper limit of the temperature increase of the water-containing sludge was set at 75°C. In addition, when the practical value is evaluated by the amount of sludge processed, it is as shown in Figure 2.

以上の如く、撹拌槽1.2で加熱、撹拌これ文含水スラ
ッジは第2工程の脱水機1oのF布ll内に装入され、
脱水処理はれ、スラッジケーキCが得られる。
As described above, the water-containing sludge heated and stirred in the stirring tank 1.2 is charged into the F cloth 11 of the dehydrator 1o in the second step,
After dehydration treatment, a sludge cake C is obtained.

脱水処理の終った戸布1)は、スラッジケーキcl取出
し友後に受水W!12に貯溜これ友洗浄水をポンプ13
、ノズル14によって吹付けることによって洗浄される
。この洗浄水は蒸気吹込管6に工っで40〜75℃に昇
温し、P布の洗浄効果を高めている。
After the dewatering process is completed, Tofu 1) receives water after taking out the sludge cake CL! Pump the cleaning water stored in 12 to 13
, by spraying with the nozzle 14. This cleaning water is heated to 40 to 75°C through the steam blowing pipe 6 to enhance the cleaning effect of the P cloth.

なお、本例では蒸気によるスラッジ、洗浄水の昇oAヲ
行なっているが、スラッジ、洗浄水の温度を40〜75
℃に昇温することが可能であれば電熱、燃焼熱等の他の
加熱方法を用いても差支えない。
In addition, in this example, the sludge and cleaning water are raised with steam, but the temperature of the sludge and cleaning water is 40 to 75 degrees.
As long as it is possible to raise the temperature to ℃, other heating methods such as electric heating and combustion heat may be used.

(実施例) 第1図に示す処理工程を用い、1パッチ処理能力38m
’の第1撹拌槽1に水分75%の弱酸スラッジ(圧砥材
の酸洗処理による発生スラッジ)お工び圧廷スラッジを
322装入した。この時の含水スラッジの温度はおおL
そ20℃であった。第1撹拌僧1には200分間貯溜し
たが、初め44分間蒸気吹込管6から30に9/分の蒸
気を吹込んで75℃に昇温しながら撹拌機8にて撹拌し
た。
(Example) Using the processing process shown in Figure 1, the processing capacity for one patch is 38 m.
322 pieces of weak acid sludge (sludge generated by pickling of abrasive material) with a water content of 75% were charged into the first stirring tank 1 of '. The temperature of the water-containing sludge at this time is L
It was 20 degrees Celsius. The first stirrer 1 was stored for 200 minutes, and at first 9 minutes of steam was blown into the steam blowing pipe 6 to 30 for 44 minutes, and the mixture was stirred with the stirrer 8 while the temperature was raised to 75°C.

その後、撹拌を継続しながら60分毎に5分根度蒸気を
吹込み、含水スラッジSの@度を40〜75℃に保った
。その後、含水スラッジSを第2撹拌槽2にポンプ9を
用込て移し、ざらに200分間、加熱、攪r1:を続け
た。
Thereafter, while stirring was continued, steam was blown in for 5 minutes every 60 minutes to maintain the temperature of the water-containing sludge S at 40 to 75°C. Thereafter, the water-containing sludge S was transferred to the second stirring tank 2 using the pump 9, and heating and stirring were continued for roughly 200 minutes.

撹拌後、含水スラッジ81に4r?ずつポンプ9にて脱
水e&10中のF、[1)に装入し、脱水処理を行なっ
た。
After stirring, water-containing sludge 81 is heated with 4r? Each sample was charged into F and [1) in dehydration e&10 using pump 9, and dehydration treatment was performed.

この間に容t6PF/の受水!12に洗浄水を貯め、3
0kp/分の蒸気を8分間吹込んで75℃まで昇温し文
。脱水機10での含水スラッジS約4nIの脱水処理が
終了毎に、40〜75℃に昇@された抗浄水約4Rtボ
ンゾ13にてノズル14ニジP布1)に散水し、洗浄し
た。
During this time, I received t6PF/ of water! Store washing water in 12, 3
The temperature was raised to 75°C by blowing steam at 0 kp/min for 8 minutes. Every time the water-containing sludge S about 4nI was dehydrated in the dehydrator 10, the cloth 1) was sprayed with water at about 4Rt anti-purification water heated to 40 to 75°C using the nozzle 14 of the bonzo 13 and washed.

従来のスラッジ回収方法と本発明に係るスラッジ脱水処
理方法との比較を第1表に示す。
Table 1 shows a comparison between the conventional sludge recovery method and the sludge dewatering method according to the present invention.

同表に示す如く、本発明のスラッジ脱水処理方法による
と、従米回収不昨と寧れていたスラッジの処理が可能と
なり、回収量が1)16m’/M増加し友。また、戸布
の汚れ、目詰シ発生が減少し次ため、P布洗浄周期が1
回/3ケ月から1回/6ケ月と長くなった。このような
稼働巡の向上と、回収処理速度上昇にニジ、処理#ヒカ
が1000m’/M程度から3000m’/Mまで向上
した。
As shown in the table, according to the sludge dewatering method of the present invention, it becomes possible to process sludge, which has previously been difficult to recover, and the amount recovered increases by 1) 16 m'/M. In addition, the occurrence of dirt and clogging of the door cloth is reduced, so the cleaning cycle of the P cloth is reduced to 1.
It has become longer from 3 months/time to 6 months/time. As a result of this improvement in operation cycle and increase in recovery processing speed, processing #hika was improved from about 1000 m'/M to 3000 m'/M.

第   1    表 (発明の効果) 以上、詳細に説明したように、本発明に工れば、従来回
収不能とされてい九スラッジの回収が可能となる。ま友
、P布の汚れ、目詰#)発生が減少して戸布洗浄周期が
長くなシ、稼働工が向上する。
Table 1 (Effects of the Invention) As explained above in detail, by incorporating the present invention, it becomes possible to recover nine sludges that were previously thought to be unrecoverable. Also, the occurrence of dirt and clogging of the P cloth is reduced, the cleaning cycle of the door cloth is lengthened, and the operation efficiency is improved.

【図面の簡単な説明】[Brief explanation of drawings]

第1図は本発明によるスラッジの脱水処理方法の一例を
示す図、第2図は含水スラッジ温度とスラッジ処理能力
との関係を示す図である。 1・・・第1撹拌槽、2・・・第2撹拌槽、3・・・ス
ラリーポンプ、4・・・フィルター、5・・−蒸気支管
、6・・・蒸気吹込管、7・・・コック、8・・・撹拌
機、9・・・ポンプ、10・・・脱水機、1)・・・F
布、12・・・受水槽、13・・・ポンプ、14・・・
ノズル、15・・・給水管。 代理人 弁理士  秋 沢 政 光 他2名 r−r+h>:八υに型−云ミ
FIG. 1 is a diagram showing an example of the sludge dehydration treatment method according to the present invention, and FIG. 2 is a diagram showing the relationship between the water-containing sludge temperature and the sludge treatment capacity. DESCRIPTION OF SYMBOLS 1... 1st stirring tank, 2... 2nd stirring tank, 3... Slurry pump, 4... Filter, 5... Steam branch pipe, 6... Steam blowing pipe, 7... Cock, 8... Stirrer, 9... Pump, 10... Dehydrator, 1)...F
Cloth, 12...Water tank, 13...Pump, 14...
Nozzle, 15... Water supply pipe. Agent Patent attorney Masamitsu Aki Sawa and 2 others

Claims (1)

【特許請求の範囲】[Claims] (1)粒度が100μm以下の極微粒、或は油類等の有
機物を含んだ含水スラッジを脱水するに際し、含水スラ
ッジを貯溜、撹拌する第1工程と、次いで脱水する第2
工程とにより処理する方法において、第1工程で含水ス
ラッジの温度を40〜75℃に加熱しながら撹拌し、第
2工程で脱水処理を行ない、かつ脱水後のろ布を40〜
75℃の温水にて洗浄することを特徴とするスラッジの
脱水処理方法。
(1) When dewatering water-containing sludge containing ultrafine particles with a particle size of 100 μm or less or organic substances such as oil, the first step is to store and stir the water-containing sludge, and the second step is to dehydrate it.
In the first step, the water-containing sludge is stirred while being heated to a temperature of 40 to 75°C, and in the second step, dehydration is performed, and the filter cloth after dehydration is heated to a temperature of 40 to 75°C.
A sludge dewatering method characterized by washing with 75°C hot water.
JP60275604A 1985-12-07 1985-12-07 Dehydration treatment of sludge Pending JPS62136300A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP60275604A JPS62136300A (en) 1985-12-07 1985-12-07 Dehydration treatment of sludge

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP60275604A JPS62136300A (en) 1985-12-07 1985-12-07 Dehydration treatment of sludge

Publications (1)

Publication Number Publication Date
JPS62136300A true JPS62136300A (en) 1987-06-19

Family

ID=17557754

Family Applications (1)

Application Number Title Priority Date Filing Date
JP60275604A Pending JPS62136300A (en) 1985-12-07 1985-12-07 Dehydration treatment of sludge

Country Status (1)

Country Link
JP (1) JPS62136300A (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5214973A (en) * 1975-07-26 1977-02-04 Nobutsugu Ishii Method for cleaning filter cloth
JPS5362353A (en) * 1976-11-16 1978-06-03 Kurita Water Ind Ltd Method for treating coagulated sludge containing protein
JPS5710398A (en) * 1980-06-23 1982-01-19 Ebara Infilco Co Ltd Treatment of muddy substance

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5214973A (en) * 1975-07-26 1977-02-04 Nobutsugu Ishii Method for cleaning filter cloth
JPS5362353A (en) * 1976-11-16 1978-06-03 Kurita Water Ind Ltd Method for treating coagulated sludge containing protein
JPS5710398A (en) * 1980-06-23 1982-01-19 Ebara Infilco Co Ltd Treatment of muddy substance

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