JPS59228013A - Flowing bath spinning of viscose rayon - Google Patents
Flowing bath spinning of viscose rayonInfo
- Publication number
- JPS59228013A JPS59228013A JP10170083A JP10170083A JPS59228013A JP S59228013 A JPS59228013 A JP S59228013A JP 10170083 A JP10170083 A JP 10170083A JP 10170083 A JP10170083 A JP 10170083A JP S59228013 A JPS59228013 A JP S59228013A
- Authority
- JP
- Japan
- Prior art keywords
- spinneret
- viscose
- coagulation bath
- spinning
- discharge
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Artificial Filaments (AREA)
- Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
Abstract
Description
【発明の詳細な説明】
本発明はビスコースレーヨンの泥沼紡糸方法に係り、湿
式泥沼紡糸方法の改善に関するものである。DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a viscose rayon bog spinning method, and relates to an improvement of a wet bog spinning method.
ビスコースをはじめとする湿式紡糸可能な紡糸原液は、
紡糸口金を通して凝固浴中に吐出され、凝固せしめられ
た後、浴中まり引き出されて糸条として形成され、必要
に応じて後処理を施されて製品光となる。Wet spinning dope such as viscose is
After being discharged into a coagulation bath through a spinneret and coagulated, it is drawn out from the bath to form a thread, and if necessary, it is subjected to post-treatment to become a product light.
従来より生産性をあげるため、紡糸速度の高速化に関し
て、ｌｋ向浴を吐出糸条の走行方向と同一方向に流動せ
しめ、凝固浴抵抗を軽減して糸条の強伸度の低下を防ぐ
泥沼紡糸方法が数多く提案されている。例えば特願昭５
７−１３２１２８号、特願昭５７−１５８０６１号では
、工業的生産の実施が可能な水準の提案が成されている
。In order to increase productivity, the spinning speed is increased by making the lk bath flow in the same direction as the running direction of the discharged yarn, reducing the coagulation bath resistance and preventing the decrease in strength and elongation of the yarn. Many spinning methods have been proposed. For example,
No. 7-132128 and Japanese Patent Application No. 57-158061 propose a level that allows industrial production.
しかしながら、加工＠での織機の革新化、高速化、間品
市場での多様化、高級化の進む中で、原糸に要求される
工業的仕様もそれにつれて日進月歩で変化しており、日
増しに厳しくなってきている。However, as processing @ looms become more innovative, faster, diversified in the temporary goods market, and become more sophisticated, the industrial specifications required for raw yarn are also changing rapidly and are increasing day by day. It's getting tougher.
とりわけ商品の高級化、高機能化を考える上で必須の、
フィラメントのマルチ化並びに細デニール化に関しては
、従来から提案されている泥沼紡糸方法にて、生産性を
あげるべく高速化してゆくと、毛羽発生、切糸発生等の
工程欠点の増大並びに原糸品質の低下を生じ、その増大
もしくは低下の割合は通常糸とは比較にならぬ根太きプ
エものであり工業的生産の実施には末だ不充分なもので
ある。In particular, it is essential when considering the upgrading and high functionality of products.
Regarding the multiplication and fine denier of filaments, if the speed of the conventionally proposed quagmire spinning method is increased to increase productivity, process defects such as fuzz generation and cut yarn generation will increase, and the quality of the raw yarn will deteriorate. The rate of increase or decrease is incomparably thicker than that of ordinary yarn, and is ultimately insufficient for industrial production.
本発明者らは、かかる技術的現状に鑑み、マルチ糸並び
に細デニール糸の泥沼紡糸方法を用いた高速売ｆＶ下で
の工業的生産を念頭に置き、鋭意研究を重ね１．−結果
、本発明に到達しＴこものである。In view of the current state of the technology, the present inventors have conducted extensive research with an eye to industrial production under high-speed fV using the bog spinning method for multi yarns and fine denier yarns.1. -As a result, we have arrived at the present invention.
即ち、本発明は吐出時のビスコースに凝固浴を流動供給
せしめるビスコースレーヨンの泥沼紡糸方法において、
全ての吐出孔がひとつの円周上にあるように配置して穿
孔した紡糸口金を用いる事を特徴とするビスコースレー
ヨンの泥沼紡糸方法にある。That is, the present invention provides a viscose rayon bog spinning method in which a coagulation bath is fluidly supplied to viscose at the time of discharge.
This method is characterized by using a spinneret in which all discharge holes are arranged so as to be on one circumference.
以下本発明の詳細な説明する。The present invention will be explained in detail below.
本発明は、全ての吐出孔がひとつの円周上にのるように
配置して穿孔した紡糸口金を用いる事によって、従来の
ビスコースレーヨンの泥沼紡糸方法では達成し得なかっ
た次の２点を改善、解決する方法を提供するものである
。The present invention achieves the following two points that could not be achieved with the conventional viscose rayon bog spinning method by using a spinneret in which all discharge holes are arranged on one circumference. It provides a method to improve and solve problems.
第一に、良好な品質水準を維持したままで、容易に高速
紡糸をする方法、第二には、通常糸と同様の工業的生産
水準で、マルチ糸並びに細デニール糸を紡糸する方法を
提供するものである。Firstly, it provides a method for easily performing high-speed spinning while maintaining a good quality level, and secondly, it provides a method for spinning multi-yarns and fine denier yarns at the same industrial production level as regular yarns. It is something to do.
従来、ビスコースレーヨン用の紡糸口金では、吐出孔か
ら吐出されたビスコースが相互接触しないようにとの配
慮から通常、吐出孔間の最短距離を１Ｍ以上設ける、或
いは特殊な場合にあっても０．７ｗ以上設ける事は当業
者にとって周知の事実であり・、従って吐出孔間距離を
可能な限り大きく設りるために、吐出孔を複数の同心円
上に分散して多Ｒ（配列するのが常識となっている。確
かに凝固浴を糸条の進行方向に向けて意図的に流動供給
せしめる事をしない静止浴紡糸方法にあっては、吐出孔
を」−述の複数回）し円上に分散して多重配列した紡糸
口金を用いて、工業的生産がなされており、かつ何ら問
題は生じ′〔いない。Conventionally, in spinnerets for viscose rayon, in order to prevent the viscose discharged from the discharge holes from coming into contact with each other, the shortest distance between the discharge holes is usually set at 1M or more, or even in special cases. It is a well-known fact for those skilled in the art to provide 0.7W or more. Therefore, in order to make the distance between the discharge holes as large as possible, the discharge holes are distributed on multiple concentric circles and It is common knowledge that in the static bath spinning method where the coagulation bath is not intentionally supplied in a flowing direction in the direction of yarn movement, the discharge hole is Industrial production has been carried out using spinnerets dispersed and arranged in multiple layers, and no problems have arisen.
しかしながら、泥沼紡糸方法においては、吐出孔内に異
物等の詰りを生じていないにもかかわらず、吐出孔が半
分詰った時に特徴的に発生する。However, in the quagmire spinning method, the problem characteristically occurs when the discharge hole is half clogged, even though the discharge hole is not clogged with foreign matter or the like.
いわゆる紡糸毛羽と類似の毛羽先端が正常部分の単糸径
よりも明らかに太きくなっている大毛羽が発生し、工程
収率を低下させるという問題が生じている。とりわけ、
単糸本数の多いマルチ糸、並びに細デニールの泥沼紡糸
において、この大毛羽発生が顕著であり、更に又、凝固
浴の流動速度を上げて紡糸速度を高めた場合にも大毛羽
ｉ生率が増加し、工業的生産を限外する大要因となって
おり、未だ解決されていない。A problem arises in that large fluffs similar to so-called spinning fluffs in which the tip of the fluffs is obviously thicker than the single yarn diameter of the normal portion occur, reducing the process yield. Above all,
This generation of large fuzz is noticeable in multi yarns with a large number of single yarns and in muddy spinning with a fine denier.Furthermore, even when the spinning speed is increased by increasing the flow rate of the coagulation bath, the large fuzz generation rate also increases. This has become a major factor limiting industrial production and has not yet been resolved.
本発明者らはこの問題を解決すべく、紡糸部分を外部観
察可能なように透明化し、観察を行なった結果、駕くべ
き事にビスコースが紡糸口金の吐出孔から吐出された直
後に切断して大毛羽が発生していること、それも多重配
列された吐出孔の最外層を除いた内側の全ての層から発
生している事、更に凝固浴の速度をあげればあげる程、
この現象が顕著に且つ頻度も多（なってゆくことを見い
出した。In order to solve this problem, the present inventors made the spun part transparent so that it could be observed externally, and as a result of the observation, it was found that the viscose was cut immediately after being discharged from the discharge hole of the spinneret. It was found that large fuzz was generated from all the inner layers except for the outermost layer of the multi-layered discharge holes, and the more the speed of the coagulation bath was increased, the more
It has been found that this phenomenon is becoming more prominent and frequent.
即ち、多重配列穿孔された紡糸口金においては内層の単
糸に加わる凝固浴の流れベクトルは、流速が増加すれば
する程流れに渦が生じるために乱れて渦動を構成し、又
更に単糸総数が増加してマルチ化すればする程、随伴流
が増大し、撹乱を起こし更に乱れるため、未だ凝固再生
の始まったばかりの単糸がとりわけデニールの細い単糸
がその乱流に巻き込まれて切断し、大毛羽を生じている
のであると思われる。That is, in a spinneret with multiple array perforations, the flow vector of the coagulation bath applied to the single fibers in the inner layer is disturbed and constitutes a vortex as the flow velocity increases, and the total number of single fibers increases. The more the mulch increases, the more the accompanying flow increases, causing turbulence and further turbulence.As a result, single filaments that have just begun to coagulate and regenerate, especially single filaments with fine denier, are caught in the turbulence and cut. This is thought to be due to the formation of large fluff.
これに対して、本発明になる全ての吐出孔がひとつの円
周上にのるように配置して穿孔した紡糸口金にあっては
、全ての単糸は泥沼かも同一の大きさの緊張を受け、か
つ製列を構成している領域に補足される単糸が実質上存
在しなくなり、更に随伴流を含めて、単糸にかかつてい
る全ての流れベクトルは一点に集中するため、凝固浴を
高速化する、若しくはマルチ化して随伴流を増大させて
も、これらの流れが全て単糸に揺れを生じさせず位置を
固定する方向に作用する。On the other hand, in the spinneret according to the present invention, in which all the discharge holes are arranged so that they are arranged on one circumference, all the single yarns have the same amount of tension. There are virtually no single filaments trapped in the area that receives and makes up the production line, and all flow vectors affecting the single filaments, including the accompanying flow, are concentrated at one point, so the coagulation bath Even if the accompaniment flow is increased by increasing the speed or multiplication, all these flows act in the direction of fixing the position of the single yarn without causing any sway.
即ち、凝固浴の速度をあげる程、単糸にかかる緊張力が
増加し、単糸相互間の随伴流の影響を受けに（くなり、
又更に、単糸の揺れが小さくなるので単糸同志が吐出孔
を出て未凝固のまま接触する確率が極めて小さくなり、
従来常識とされていた吐出孔間最短距離を大幅に縮少す
る事が可能である。又この距離を縮少すればする程、単
糸を包んでいる随伴流は一体化し連続した中空円筒形の
スクリーンを形成し、単糸固定効果が極めて増１−とい
う好ましい循環を繰り返している事が考えられる。吐出
孔間最短距離をｇ、 ２７ ｍｍまで縮めても、伺ら工
程性能並びに糸品質に影響が出ない事を確認している。In other words, as the speed of the coagulation bath increases, the tension applied to the single threads increases, and the threads become less affected by the accompanying flow between the single threads.
Furthermore, since the sway of the single threads is reduced, the probability that the single threads exit the discharge hole and come into contact with each other while uncoagulated becomes extremely small.
It is possible to significantly reduce the shortest distance between discharge holes, which was conventionally considered common sense. In addition, as this distance is reduced, the accompanying flow surrounding the single fibers becomes integrated, forming a continuous hollow cylindrical screen, and the effect of fixing the single fibers is greatly increased, repeating a favorable cycle. is possible. It has been confirmed that even if the shortest distance between discharge holes is reduced to 27 mm, there will be no effect on process performance or yarn quality.
以上から明らかなように、本発明は泥沼紡糸を高速化し
てゆ（場合に極めて容易に工業的生産を可能ならしめる
。又、本発明はマルチ糸並びに細デニール糸の泥沼紡糸
を通常糸と同一水準で実施するために極めて有効な方法
となる。As is clear from the above, the present invention speeds up mud spinning (in some cases, makes industrial production extremely easy).The present invention also enables mud spinning of multi yarns and fine denier yarns in the same way as ordinary yarns. This is an extremely effective method for implementing this at a high level.
又更にマルチ化すれば、同一デニールでは吐出孔断面積
が増え、実質的にドラフトが上昇する。Furthermore, if the discharge hole is multiplied, the cross-sectional area of the discharge hole increases for the same denier, and the draft substantially increases.
ドラフトがある上限値を越えると紡糸性に慾影響を及は
すことは当業者には周知であり、従って上限値を越えな
い適正なドラフトに下げる必要がある場合には、吐出孔
径を減少させた紡糸口金を用いているが、当然の事なが
ら異物の孔詰りか増加し、紡糸口金の交換頻度が増加す
る。しかしながら、本発明になる紡糸口金を用いた方法
では、適正ドラフトの上限値が、通常の多重配列紡糸口
金を用いた場合に比較して、約４割位高（て良い事が判
明している。従って吐出孔径減少の必要性は緩和され、
紡糸口金の交換頻度は減少する。理由は定かではないが
、原液の吐出時の流速分布が小さくなり、従ってドラフ
トの単糸間での分布が狭（なっているために上限値が上
ったのではないかと推定される。本発明にいうドラフト
の定義は、巻取速度／吐出線速度である。It is well known to those skilled in the art that when the draft exceeds a certain upper limit, spinnability is adversely affected. Therefore, if it is necessary to lower the draft to an appropriate level that does not exceed the upper limit, the diameter of the discharge hole should be reduced. However, as a matter of course, pore clogging with foreign matter increases and the frequency of replacing the spinneret increases. However, in the method using the spinneret according to the present invention, the upper limit of the appropriate draft is about 40% higher than when using a normal multi-array spinneret. Therefore, the need to reduce the discharge hole diameter is alleviated.
The frequency of spinneret replacement is reduced. The reason is not clear, but it is presumed that the upper limit value has increased because the flow velocity distribution during discharge of the stock solution has become smaller, and therefore the draft distribution between single yarns has become narrower. The definition of draft in the invention is winding speed/discharge linear speed.
本発明の速度にあたっては、縦同浴を流動供給せしめる
凝固浴供給口が、吐出糸条の進行方向に幻して、紡糸口
金の以前にある事が好ましく、又、流管を用いた泥沼紡
糸である事が好ましい。更に凝固浴が、例えば０１（昭
５７−１７８２８１号に記載の整流部品を通過しで整流
されている事がより好ましい。これらはいずれも紡糸口
金以降の凝固浴の乱れをより減少させる効果を持つから
である。Regarding the speed of the present invention, it is preferable that the coagulation bath supply port for supplying the coagulation bath vertically in a fluid manner is located in front of the spinneret in front of the spinneret in the traveling direction of the discharged yarn. It is preferable that Furthermore, it is more preferable that the coagulation bath is rectified by passing through a rectification component described in, for example, 01 (Sho 57-178281).All of these have the effect of further reducing turbulence of the coagulation bath after the spinneret. It is from.
又更に、穿孔された吐出孔間の最短距離が、２削以［で
ある事が一層望ましい。この最短距離が２闘以上になる
と、とりわリーマルチ糸を紡出する場合には吐出孔数が
増えるため、吐出孔の配列さＪするべきＰ、Ｃ，Ｄ、（
Ｐｉｔｃｈ ｏｆ Ｃ１ｒｃｌｅ Ｄｉａｍｅｔｅｒ）
が増加し、紡糸口金の径が増大することになる。従って
、紡出糸条の品質に急影響を及ぼす程の、ビスコース滞
留時間の局部的な斑やビスコースの紡糸口金内での温度
ないしは粘度の斑を生じ、例えばこれらの斑の部分が紡
糸された後の糸条で、強度や伸度を始めとする物性値の
異常を生じたり、或いは工程で受ける張力に耐えきれず
切断や毛羽を生じるからである。Furthermore, it is more desirable that the shortest distance between the drilled discharge holes be two or more cuts. If this shortest distance becomes 2 or more, the number of discharge holes will increase especially when spinning multi-lead yarn, so the arrangement of discharge holes should be P, C, D, (
Pitch of C1rcle Diameter)
will increase, and the diameter of the spinneret will increase. Therefore, local irregularities in the residence time of viscose and irregularities in temperature or viscosity within the viscose spinneret occur, which can drastically affect the quality of the spun yarn. This is because the yarn after being processed may exhibit abnormalities in physical properties such as strength and elongation, or may not be able to withstand the tension applied during the process, resulting in breakage or fluffing.
又、当然のことながら本発明がマルチ糸や細デニール糸
に限らず、通常糸に１６いても良好な効果を発揮するの
は言うまでもない。Moreover, it goes without saying that the present invention is not limited to multi-threads or fine denier threads, but also exhibits good effects even when using normal threads.
本発明になる方法にあっては、凝固浴の流速が上昇すれ
ばする程吐出直后の単糸の揺れが減少し安定走行するの
で、従来の多重配列穿孔された紡糸口金を用いた場合と
比較して、可動上限速度は飛躍的に増加する。In the method of the present invention, as the flow rate of the coagulation bath increases, the shaking of the single yarn immediately after discharge decreases and the yarn runs more stably. In comparison, the upper limit speed of movement increases dramatically.
本発明になる紡糸口金の一例の平面図及び直角断面図を
各々矛１図ａ及び、１−１図すに示す。符号ｌは口金の
保持用つげ、２は吐出孔径減少、３は４を中心とする円
周を表わし、吐出孔はこの円周３上にのるように配列し
て穿孔される。円周３の直径を通常Ｐ、Ｃ８Ｄ、（Ｐｉ
ｔｃｈ ｏｆ Ｃ１ｒｃｌｅ Ｄｉａｍｅｔｅｒ）と呼
ぶ。A plan view and a right-angle sectional view of an example of the spinneret according to the present invention are shown in Figure 1A and Figure 1-1, respectively. Reference numeral 1 represents a boxwood for holding the cap, 2 represents a reduction in the diameter of the discharge hole, and 3 represents a circumference centered on 4, and the discharge holes are arranged and drilled on this circumference 3. The diameter of circumference 3 is usually P, C8D, (Pi
tch of C1rcle Diameter).
従来形の多重配列紡糸口金にあっては、中心４を等しく
する複数の同心円上に、吐出孔を穿孔している。In conventional multi-array spinnerets, the discharge holes are drilled on a plurality of concentric circles with equal centers 4.
〕・２図に本発明に用いるのが好ましい泥沼紡糸方法の
一例を図示する。]・Figure 2 illustrates an example of the quagmire spinning method preferably used in the present invention.
ビスコースはビスコース供給口５から供給され、凝固浴
供給口６から供給された後、凝固浴整流部品７を通って
整流された凝固浴と、紡糸口金保持具８に保持された紡
糸口金９から吐出されて出会い、吐出糸条１１となり、
−緒に流管１０内を通過する。流管１０を出た後、糸条
１１は、例えば糸道１３により向きをかえることにより
噴出凝固浴１２と分離されて、適当な後工程へと導かれ
る。本発明において泥沼の方向は上向、横向、下向いず
れであっても好ましい結果を得る。Viscose is supplied from a viscose supply port 5 , and after being supplied from a coagulation bath supply port 6 , the coagulation bath is rectified through a coagulation bath rectification component 7 and a spinneret 9 held in a spinneret holder 8 . They are discharged from each other, meet each other, and become discharged yarn 11.
- pass through the flow tube 10 together. After exiting the flow tube 10, the yarn 11 is separated from the jet coagulation bath 12, for example by being turned around by a yarn channel 13, and is led to a suitable subsequent process. In the present invention, favorable results can be obtained regardless of whether the direction of the quagmire is upward, sideways, or downward.
次に本発明を実施例により更に説明する。当然のことな
がら、本発明は記載された実施例にのみ限定されるもの
ではない。Next, the present invention will be further explained by examples. Naturally, the invention is not limited only to the described embodiments.
実施例１
通常の方法にて製造したセルロース濃度＆０重量％、ア
ルカリ濃度５．５重量％のビスコースを、通常の方法に
て製造したＨ２ＳＯ，１５０ｆｌ／４３ 、 Ｎａ２Ｓ
Ｏ４２８０ｉ／−ｇ、Ｚｎ５Ｏ４１５）／−ｇ （１）
５５℃の凝固浴中に、ツ・２図に示した紡糸方法を上
向に用いて、紡糸速度１７０ｍ／分にて、１２０デニー
ル８０フイラメントの糸を紡糸した。紡糸口金の径はｌ
Ｑｌｌｒｌｌｌφであり、Ｐ、Ｃ，Ｄ、７−の円周上
に等間隔に吐出孔径Ｑ、Ｑ５１１１１３φの吐出孔が８
０個穿孔されており、吐出孔間最短距離は０．２７１１
１１であり、ドラフトは１３０となる。これらの条件を
矛１表に示す。流管は内径５ｗＭφ、長さ２００１ｍの
ガラス管を用い、紡糸口金面から流管人口までの距離を
５０−にし凝固浴の流管内速度は１２ＯＦＦＩ／分に設
定した。凝固糸条はこのローラーを経て遠心ポットに巻
取り通常の後処理を施こし℃製品フィラメントにした。Example 1 Viscose with a cellulose concentration &0% by weight and an alkali concentration of 5.5% by weight, produced by a conventional method, was mixed with H2SO, 150fl/43, Na2S, produced by a conventional method.
O4280i/-g, Zn5O415)/-g (1)
A yarn of 120 denier and 80 filaments was spun in a coagulation bath at 55°C at a spinning speed of 170 m/min using the spinning method shown in Figure 2 in an upward direction. The diameter of the spinneret is l
Qllrllllφ, and there are 8 discharge holes with discharge hole diameters Q and Q511113φ at equal intervals on the circumference of P, C, D, and 7-.
0 holes are drilled, and the shortest distance between discharge holes is 0.2711
11, and the draft is 130. These conditions are shown in Table 1. A glass tube with an inner diameter of 5 wMφ and a length of 2001 m was used as the flow tube, the distance from the spinneret surface to the flow tube population was set to 50 -, and the flow tube speed of the coagulation bath was set to 12 OFFI/min. The coagulated yarn passed through this roller, was wound into a centrifugal pot, and subjected to usual post-treatment to form a product filament at °C.
大毛羽数はワーノく−型毛羽検知装置にて肉眼で検定し
た。更に紡糸口金の孔詰りによる交換頻度を示すために
交換から次の交換までの周期日数を飼った。いずれもそ
の結果を、１−２表に示す。The number of large fluffs was determined visually using a Warno-type fluff detector. Furthermore, the number of cycle days from one exchange to the next exchange was recorded to indicate the frequency of exchange due to spinneret hole clogging. The results are shown in Table 1-2.
比較例１
１・１表に記載した紡糸口金を用いた他は、実施全く同
様にして７５デニール、３３フイラメントの糸を紡糸し
、実施例１と全く同様にして評価した。その結果な牙２
表に示す。Comparative Example 1 A 75 denier, 33 filament yarn was spun in exactly the same manner as in Example 1, except that the spinneret shown in Table 1.1 was used, and evaluated in the same manner as in Example 1. The resulting fang 2
Shown in the table.
矛 １ 表
矛２表
実施例４及び比較例４
矛２図に示した紡糸方法を下向きに用い、実施例１と全
く同様のビスコース及び凝固浴により。Table 1 Table 2 Table Example 4 and Comparative Example 4 Table 2 Using the spinning method shown in Figure 2 in a downward direction, and using the same viscose and coagulation bath as in Example 1.
矛３表記載の紡糸口金にて、７５デニールの糸を紡糸し
た。１時間以上の間切断せずに巻取る事の出来た速度を
可動最高速度とし、１・３表に、その時の流管内磁高流
速と併せ℃記す。A 75 denier yarn was spun using the spinneret shown in Table 3. The maximum movable speed is the speed at which the coil can be wound without cutting for more than 1 hour, and is recorded in degrees Celsius in Tables 1 and 3 along with the magnetic high flow speed in the flow tube at that time.
（以下余色）
矛 ３ 表
以上の実施例１〜４及び比較例１〜４かも分るように、
本発明になる泥沼紡糸方法が従来法に比べて、極めて良
好な品質並びに工程性能を示す事がり」臼である。(Hereinafter, extra color) Spear 3 As can be seen from Examples 1 to 4 and Comparative Examples 1 to 4 in the table above,
The bog spinning method of the present invention exhibits extremely good quality and process performance compared to conventional methods.
３□ １図は本発明の紡糸口金を示し、（ＡＪ図は平面
図、Ｂ図は直角断面図である。
牙２図は本発明に好ましく用いられる泥沼紡糸方法の一
例を図示したものである。
ｌは口金の保持用つげ、２は吐出孔穿孔面、３は４を中
心とする吐出孔穿孔円周、５はビスコース供給口、６は
凝固浴供給口、７は凝固浴整流部品、８は紡糸口金保持
具、９は紡糸口金、１０は流管、１１は吐出糸条、１２
は噴出凝固浴、１３は糸道。
特許出願人 旭化成工業株式会社
第１
（Ａ）
第２図3 □ Figure 1 shows the spinneret of the present invention (Figure AJ is a plan view, Figure B is a right-angled sectional view. Figure 2 is a diagram illustrating an example of the bog spinning method preferably used in the present invention). .l is a boxwood for holding the cap, 2 is a discharge hole perforation surface, 3 is a discharge hole perforation circumference centered on 4, 5 is a viscose supply port, 6 is a coagulation bath supply port, 7 is a coagulation bath rectification part, 8 is a spinneret holder, 9 is a spinneret, 10 is a flow tube, 11 is a discharge yarn, 12
1 is a jet coagulation bath, and 13 is a thread path. Patent applicant: Asahi Kasei Industries, Ltd. No. 1 (A) Figure 2
Claims (1)
めるビスコースレーヨンの泥沼紡糸方法にオ６いて、全
ての吐出孔がひとつの円周上にのるように配置して穿孔
した紡糸口金を用いる事を特徴とするビスコースレーヨ
ンの泥沼紡糸方法（２）凝固浴を流動供給せしめる凝固
浴供給口が、吐出糸条の進行方向に対して、紡糸口金の
以前にある事を特徴とする特許請求の範囲矛１１１項に
記載のビスコースレーヨンの泥沼紡糸方法（３） 吐
出時のビスコースに凝固浴を流動供給せしめるにあたり
、流管を用いる事を特徴とする特許請求範囲矛（１）項
乃至矛（２）項に記載のビスコースレーヨンの泥沼紡糸
方法 （４）吐出時のビスコースに流動供給せしめられる凝固
浴が整流用部品を通過して整流されている事を特徴とす
る特許請求の範囲矛（１）項乃至矛（３）項に記載のビ
スコースレーヨンの泥沼紡糸方法 （５）穿孔された吐出孔間の最短距離が２謂以下である
事を特徴とする特許請求の範囲矛（１１乃至、）１１（
４）項に記載のビスコースレーヨンの泥沼紡糸方法[Claims] (1) A viscose rayon bog spinning method in which a coagulating bath is fluidly supplied to viscose during discharge, and all discharge holes are arranged on one circumference. (2) A coagulation bath supply port for supplying a coagulation bath in a flowing manner is located in front of the spinneret with respect to the traveling direction of the discharged yarn. A viscose rayon quagmire spinning method (3) according to claim 111, characterized in that a flow tube is used to supply the coagulation bath to the viscose at the time of discharge. Scope (1) to (2) of the viscose rayon quagmire spinning method (4) The coagulation bath that is fluidly supplied to the viscose at the time of discharge is rectified by passing through a rectifying component. A viscose rayon quagmire spinning method according to claims (1) to (3), characterized in that (5) the shortest distance between the drilled discharge holes is less than or equal to 2. Claims (11 to 11)
Quagmire spinning method for viscose rayon described in section 4)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10170083A JPS59228013A (en) | 1983-06-09 | 1983-06-09 | Flowing bath spinning of viscose rayon |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10170083A JPS59228013A (en) | 1983-06-09 | 1983-06-09 | Flowing bath spinning of viscose rayon |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS59228013A true JPS59228013A (en) | 1984-12-21 |
Family
ID=14307593
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP10170083A Pending JPS59228013A (en) | 1983-06-09 | 1983-06-09 | Flowing bath spinning of viscose rayon |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS59228013A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01132817A (en) * | 1987-11-11 | 1989-05-25 | Kuraray Co Ltd | Ultrafine viscose rayon filament yarn and production thereof |
| EP0362825A2 (en) * | 1988-10-05 | 1990-04-11 | Asahi Kasei Kogyo Kabushiki Kaisha | Viscose rayon fiber having superior appearance |
| EP0442405A2 (en) * | 1990-02-16 | 1991-08-21 | Akzo Nobel N.V. | Process and apparatus for the preparation of moulded articles |
| US5254303A (en) * | 1990-02-16 | 1993-10-19 | Akzo N.V. | Method and device for manufacturing molded bodies |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS54131022A (en) * | 1978-03-30 | 1979-10-11 | Asahi Chem Ind Co Ltd | Wet spinning device |
| JPS56128312A (en) * | 1980-02-12 | 1981-10-07 | Du Pont | Production of filament |
-
1983
- 1983-06-09 JP JP10170083A patent/JPS59228013A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS54131022A (en) * | 1978-03-30 | 1979-10-11 | Asahi Chem Ind Co Ltd | Wet spinning device |
| JPS56128312A (en) * | 1980-02-12 | 1981-10-07 | Du Pont | Production of filament |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01132817A (en) * | 1987-11-11 | 1989-05-25 | Kuraray Co Ltd | Ultrafine viscose rayon filament yarn and production thereof |
| EP0362825A2 (en) * | 1988-10-05 | 1990-04-11 | Asahi Kasei Kogyo Kabushiki Kaisha | Viscose rayon fiber having superior appearance |
| EP0362825A3 (en) * | 1988-10-05 | 1990-12-27 | Asahi Kasei Kogyo Kabushiki Kaisha | Viscose rayon fiber having superior appearance |
| EP0442405A2 (en) * | 1990-02-16 | 1991-08-21 | Akzo Nobel N.V. | Process and apparatus for the preparation of moulded articles |
| US5254303A (en) * | 1990-02-16 | 1993-10-19 | Akzo N.V. | Method and device for manufacturing molded bodies |
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