JPS59115721A - Separator in spary dryer - Google Patents

Separator in spary dryer

Info

Publication number
JPS59115721A
JPS59115721A JP23158683A JP23158683A JPS59115721A JP S59115721 A JPS59115721 A JP S59115721A JP 23158683 A JP23158683 A JP 23158683A JP 23158683 A JP23158683 A JP 23158683A JP S59115721 A JPS59115721 A JP S59115721A
Authority
JP
Japan
Prior art keywords
flow
guide
container
product
ring space
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP23158683A
Other languages
Japanese (ja)
Inventor
フリ−ドベルト・ホフマン
グンタ−・アイパ−
ハンス・ランゲンフエルダ−
ハンス−ヨヘン・バイゼ
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of JPS59115721A publication Critical patent/JPS59115721A/en
Pending legal-status Critical Current

Links

Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B3/00Drying solid materials or objects by processes involving the application of heat
    • F26B3/02Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air
    • F26B3/10Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour carrying the materials or objects to be dried with it
    • F26B3/12Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour carrying the materials or objects to be dried with it in the form of a spray, i.e. sprayed or dispersed emulsions or suspensions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/16Evaporating by spraying
    • B01D1/18Evaporating by spraying to obtain dry solids

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Microbiology (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Separating Particles In Gases By Inertia (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Drying Of Solid Materials (AREA)

Abstract

(57)【要約】本公報は電子出願前の出願データであるた
め要約のデータは記録されません。
(57) [Summary] This bulletin contains application data before electronic filing, so abstract data is not recorded.

Description

【発明の詳細な説明】 およびその間に配置さ・れかつガス放出のため1つまた
は複数の出口開口を備えたリング空間が設けられており
,その際リング空間の範囲の容器内部に,生成物/ガス
流用のガイド装Nが設けられている,噴霧乾燥器におけ
る生成物/ガス流用分離装置。
DETAILED DESCRIPTION OF THE INVENTION A ring space is provided between and provided with one or more outlet openings for gas discharge, with the product being inside the vessel in the area of the ring space. /Product/gas flow separation device in a spray dryer, which is provided with a guide arrangement N for the gas flow.

噴霧乾燥器においてミクロ粒子から処理すべき懸濁液ま
たは溶液,例えばピグメント懸濁液を得るようにし.乾
燥容器においてほとんとの場合単方向流動作で熱いガス
流中に散布し,このカスT)’+trが懸濁液の湿気を
吸取し,かつその際乾燥した生酸物粒子を残す。これら
乾燥粒子は、下側容器端部においてガス流から分離され
、かつ収容容器に入り、ここから取出される。
A suspension or solution to be treated, for example a pigment suspension, is obtained from the microparticles in a spray dryer. In a drying container, the residue T)'+tr, which is dispersed in a hot gas stream in most cases in a unidirectional flow motion, absorbs the moisture of the suspension and leaves behind dried bioacid particles. These dry particles are separated from the gas stream at the lower vessel end and enter the receiving vessel from which they are removed.

生成物/ガス流の分離のため通常乾燥容器と収容容器の
間にリング空間がはめ込まれており、このリング空間を
介してカスは加圧または負圧により取出される。その際
まだガス流中に残留した生成物粒子は後続の分離装置に
おいて大部分粉砕されほこりになるので、できるたけ完
全に分難することが望ましい。
For the separation of the product/gas stream, a ring space is usually inserted between the drying vessel and the receiving vessel, through which the waste is removed by means of pressure or underpressure. Since the product particles still remaining in the gas stream are then mostly crushed to dust in the subsequent separation device, it is desirable to separate them as completely as possible.

それ故に専門書I−スプレィ、ドライング、ハンドブッ
ク」第3版、 19’79年、第9章「セパレイジョン
、アンド、リカバリー、オブ、ドライド、プロダクト」
に記載されたように、乾燥容器の端部においてリング空
間の範囲に、流れ断面を収縮するガイド板が設けられ、
それによりガス流は、流速を増加され、かつこれに続い
てリング空間の方に強力に転向させられる。
Therefore, Specialized Book I - Spray, Drying, Handbook, 3rd Edition, 19'79, Chapter 9, ``Separation, and, Recovery, of, Drying, Products.''
As described in , a guide plate is provided in the region of the ring space at the end of the drying container, which constricts the flow cross section;
The gas flow is thereby increased in flow velocity and subsequently deflected strongly towards the ring space.

粗い生成物についてはこれら構造処置で十分であるが、
それに反してミクロ粒子において固体の収量は満足すべ
きものではない。
These structural treatments are sufficient for coarse products, but
On the other hand, the solids yield in microparticles is not satisfactory.

それ故に本発明の課題は、噴霧乾燥において乾燥生成物
を、これまで利用できた装置によるものより多くの収量
でガス流から分離できる乾燥装置を開発することにある
It is therefore an object of the present invention to develop a drying device which makes it possible to separate the dried product from the gas stream in spray drying with a higher yield than with devices available hitherto.

本発明によればこの課題は、初めに述べたような分離装
置により次のようにして解決される。すなわちガイド装
置が、直接連続した2つの流れガイド部材から成り、こ
れら流れガイド部材のうち流れの方向において第1のも
のか、乾燥容器の端部において流れ断面の収縮を行い、
かつ第2のものが、リング空間の高さのところで流れ断
面の拡大を行う。
According to the invention, this problem is solved by means of a separation device of the type mentioned at the outset, as follows. That is, the guide device consists of two flow guide elements in direct succession, of which the first one in the direction of flow causes a contraction of the flow cross section at the end of the drying container;
and the second one carries out an enlargement of the flow cross section at the level of the ring space.

本発明の実施例を以下図面によって説明する。Embodiments of the present invention will be described below with reference to the drawings.

乾燥容器1と収容容器、ここでは収容円すい体2との間
にあるリング空間3の範囲に、生成物/ガス流のガイド
装置が設けられており、この方イド装置は、乾燥容器の
端部において流れ断面を収縮する第1の流れガイド部材
、およびこれにすぐ続きかつリング空間の高さのところ
で流れ断IT4jを拡大する第2の流れガイド部材から
成る(第1図)。
In the area of the annular space 3 between the drying container 1 and the receiving container, here the receiving cone 2, a guide device for the product/gas flow is provided, which guide device is arranged at the end of the drying container. It consists of a first flow guide member that constricts the flow cross section and a second flow guide member that immediately follows this and widens the flow break IT4j at the level of the ring space (FIG. 1).

分離装置の有利な構成において第1の流れガイド部材は
、流れ断面をじょうごのように収縮するガイド板5から
成り、また第2のものは、流れ断面をじょうごのように
拡大するガイド板6から成る。その際収縮したガイド板
5が収容円すい体2と同じ傾斜を有し、かつこのガイド
板の下側縁が拡大ガイド板6の始まる高さで終っており
、その際この拡大ガイド板か他方においてI1g容円す
い体の始端部にまで達している場合、非常に多くの固体
収量が得られることがわかった。装置部分の幾何学的(
117造および大きさおよび相互配置に応して。
In an advantageous embodiment of the separation device, the first flow guide element consists of a guide plate 5 which constricts the flow cross section like a funnel, and the second one consists of a guide plate 6 which expands the flow cross section like a funnel. Become. In this case, the retracted guide plate 5 has the same slope as the receiving cone 2 and the lower edge of this guide plate ends at the level at which the enlarged guide plate 6 begins, with this enlarged guide plate on the other hand. It has been found that very high solids yields are obtained when reaching the beginning of the I1 g cone. The geometry of the equipment part (
117 depending on the structure and size and mutual arrangement.

別の組込み状態が最適なこともあることは明らかである
It is clear that other embedded states may be optimal.

第2図に示すように流れ収縮は、第2のガイド板6のす
ぐ上にこれに対して同心的に配置されたリング管7によ
って行うこともできる。そのためこのリング管は1周に
わたって分配されかつ乾燥容器lの中心に向けられた噴
射開口8を有し、かつ圧力源に接続されている。
As shown in FIG. 2, the flow contraction can also be effected by means of a ring tube 7 arranged directly above the second guide plate 6 and concentrically thereto. For this purpose, this ring tube has an injection opening 8 distributed over one circumference and directed toward the center of the drying vessel l, and is connected to a pressure source.

流れガイド部材を配置することにより、生成物/ガス流
は、まず収束され、かつそれから側方に転向され、ガス
流またその一部が、収束の直後に両方の流れガイド部材
の間で高い流速を生じるリング空間に達することはない
By arranging the flow guide elements, the product/gas stream is first focused and then diverted to the side, such that the gas stream or a portion of it has a high flow velocity between both flow guide elements immediately after convergence. It never reaches the ring space that causes it.

工業規阜における実験によれは9本発明による分離装置
により92%の固体収量が得られ、一方公知技術による
装置では75%であることがわかった。
Experiments in an industrial setting have shown that a solids yield of 92% can be obtained with the separation apparatus according to the invention, compared to 75% with the apparatus according to the prior art.

【図面の簡単な説明】 第1図は、乾燥容器の下部、ここに接続されたリング空
間および収容容器の上部を含む分離装置の長手断面図、
第2図は、流れガイド部材として噴射量りを有するリン
グ管を示す図である。 1・・・・・・乾燥容器、2・・・・・・収容容器、3
・・・・・リング空nL  5,6.7・・・・・・流
れガイド部材特許出願人   パスフ ァクチェンゲゼ
ルシャフト代理人弁理士   1)代 力k 泊
BRIEF DESCRIPTION OF THE DRAWINGS FIG. 1 is a longitudinal sectional view of the separation device including the lower part of the drying container, the ring space connected thereto and the upper part of the receiving container;
FIG. 2 shows a ring tube with an injection meter as a flow guide element. 1... Drying container, 2... Storage container, 3
...Ring empty nL 5,6.7...Flow guide member patent applicant Passfachchengesellschaft representative patent attorney 1) Power K Tomari

Claims (1)

【特許請求の範囲】 (1)乾燥容器(1)に続く生成物用収容容器(2)、
およびその間に配置されかつガス放出のため1つまたは
複数の出11開1−1をf+iffえたリング空間(3
)が設けられており、その際リング空間の範囲の容器内
部に。 生成物/カス流用のガイド装置が設けられている。 噴霧乾燥器における生成物/ガス流用分離装置において
。 カイト装RV、が、IU接連続した2つの流れガイド部
vJ’C5,6,’/)から成り、これら流れガイド部
材のうち流れの方向において第1のもの(5゜7)が、
乾燥容器(1)の端部において流れ断面の収縮を行い、
かつ第2のもの(6)が、リング空間(3)の高さのと
ころで流れ断u7jの拡大を行うことを特徴とする。噴
霧乾燥器における分離装置。 (,2)流れカイト部材が、流れ断面をじょうごのよう
に収縮する第1のガイド板(5)と流れ断面をじょうご
のように拡大する第2のガイド板(6)とから成る。特
許請求の範囲第1項記載の分離装置。 (3)第1の流れガイド部材が、第2のガイド部材のす
ぐ上にこれに対して同心的に配置されたリング管(7)
から成り、このリングw’ i; 、周にわたって分散
されかつ乾燥容器(1)の中心に向けられた複数の噴射
量D (8)を有し、かつ圧力源に接続されている。特
8′[請求の範囲第1項記載の分離装置。
[Claims] (1) A product storage container (2) following the drying container (1);
and a ring space (3
) inside the container in the area of the ring space. A guide device for product/waste flow is provided. In product/gas stream separation devices in spray dryers. The kite rig RV consists of two continuous flow guide parts vJ'C5,6,'/) in contact with the IU, of which the first one (5°7) in the flow direction is
performing a contraction of the flow cross section at the end of the drying container (1);
And the second one (6) is characterized in that it performs an expansion of the flow cutoff u7j at the level of the ring space (3). Separation device in spray dryer. (, 2) The flow kite member consists of a first guide plate (5) whose flow cross section contracts like a funnel and a second guide plate (6) whose flow cross section expands like a funnel. A separation device according to claim 1. (3) a ring tube (7) in which the first flow guide member is arranged directly above and concentrically with respect to the second guide member;
, which has a plurality of injection volumes D (8) distributed over its circumference and directed towards the center of the drying container (1), and is connected to a pressure source. Part 8' [separation device according to claim 1].
JP23158683A 1982-12-11 1983-12-09 Separator in spary dryer Pending JPS59115721A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE3245954 1982-12-11
DE32459548 1982-12-11

Publications (1)

Publication Number Publication Date
JPS59115721A true JPS59115721A (en) 1984-07-04

Family

ID=6180466

Family Applications (1)

Application Number Title Priority Date Filing Date
JP23158683A Pending JPS59115721A (en) 1982-12-11 1983-12-09 Separator in spary dryer

Country Status (3)

Country Link
JP (1) JPS59115721A (en)
CH (1) CH662410A5 (en)
DK (1) DK157505C (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NO20022016L (en) * 2002-04-26 2003-10-27 Norsk Hydro As Method and equipment for separating solid particles from a gas stream

Also Published As

Publication number Publication date
DK567083A (en) 1984-06-12
DK567083D0 (en) 1983-12-09
DK157505B (en) 1990-01-15
DK157505C (en) 1990-06-25
CH662410A5 (en) 1987-09-30

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