JPS5629573A - Preparation of halogeno-trifluoromethyl-pyridine - Google Patents
Preparation of halogeno-trifluoromethyl-pyridineInfo
- Publication number
- JPS5629573A JPS5629573A JP10486679A JP10486679A JPS5629573A JP S5629573 A JPS5629573 A JP S5629573A JP 10486679 A JP10486679 A JP 10486679A JP 10486679 A JP10486679 A JP 10486679A JP S5629573 A JPS5629573 A JP S5629573A
- Authority
- JP
- Japan
- Prior art keywords
- pyridine
- trifluoromethyl
- chloro
- halogeno
- hydrogen fluoride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Pyridine Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
PURPOSE: To prepare a 2-halogeno-5-trifluoromethyl-pyridine useful as an intermediate of herbicide, without leaving solid residue, by reacting 2-chloro-5-trichloromethyl-pyridine with hydrogen fluoride in the presence of a solid catalyst.
CONSTITUTION: 2-Fluoro- or 2-chloro-5-trifluoromethyl-pyridine is prepared by reacting (A) 2-chloro-5-trichloromethyl-pyridine (1mol) with (B) hydrogen fluoride (3W30mol) in the presence of (C) a solid fluorinating catalyst at 250W400°C. The fluorinating catalyst is pref. aluminum fluoride, chromium (III) oxyfluoride or their mixture, or chromium (III) oxyfluoride supported on aluminum fluoride. The reaction is pref. carried out by introducing the (A) component as a solution in hydrogen fluoride or an inert solvent into the reaction zone.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP10486679A JPS5629573A (en) | 1979-08-16 | 1979-08-16 | Preparation of halogeno-trifluoromethyl-pyridine |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP10486679A JPS5629573A (en) | 1979-08-16 | 1979-08-16 | Preparation of halogeno-trifluoromethyl-pyridine |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP17047186A Division JPS6212758A (en) | 1986-07-19 | 1986-07-19 | Production of halogeno-trifluoromethyl-pyridine |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5629573A true JPS5629573A (en) | 1981-03-24 |
JPS625425B2 JPS625425B2 (en) | 1987-02-04 |
Family
ID=14392148
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP10486679A Granted JPS5629573A (en) | 1979-08-16 | 1979-08-16 | Preparation of halogeno-trifluoromethyl-pyridine |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5629573A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS56100764A (en) * | 1980-01-14 | 1981-08-12 | Ishihara Sangyo Kaisha Ltd | Preparation of beta-trifluoromethylpyridines |
CN106748981A (en) * | 2016-11-29 | 2017-05-31 | 大连九信精细化工有限公司 | A kind of residual recoverying and utilizing method of fluoromethyl pyridine reactor |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5432479A (en) * | 1977-08-12 | 1979-03-09 | Ici Ltd | Herbicidal pyridine compound |
JPS5461183A (en) * | 1977-10-21 | 1979-05-17 | Ishihara Sangyo Kaisha Ltd | 2-substituted-5-trifluoromethyl pyridine compounds |
JPS5585564A (en) * | 1978-12-22 | 1980-06-27 | Ishihara Sangyo Kaisha Ltd | Preparation of beta-trifluoromethylpyridine |
JPS55124762A (en) * | 1979-03-19 | 1980-09-26 | Ishihara Sangyo Kaisha Ltd | Preparation of beta-trifluoromethylpyridine |
-
1979
- 1979-08-16 JP JP10486679A patent/JPS5629573A/en active Granted
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5432479A (en) * | 1977-08-12 | 1979-03-09 | Ici Ltd | Herbicidal pyridine compound |
JPS5461183A (en) * | 1977-10-21 | 1979-05-17 | Ishihara Sangyo Kaisha Ltd | 2-substituted-5-trifluoromethyl pyridine compounds |
JPS5585564A (en) * | 1978-12-22 | 1980-06-27 | Ishihara Sangyo Kaisha Ltd | Preparation of beta-trifluoromethylpyridine |
JPS55124762A (en) * | 1979-03-19 | 1980-09-26 | Ishihara Sangyo Kaisha Ltd | Preparation of beta-trifluoromethylpyridine |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS56100764A (en) * | 1980-01-14 | 1981-08-12 | Ishihara Sangyo Kaisha Ltd | Preparation of beta-trifluoromethylpyridines |
JPS6134416B2 (en) * | 1980-01-14 | 1986-08-07 | Ishihara Sangyo Kaisha | |
CN106748981A (en) * | 2016-11-29 | 2017-05-31 | 大连九信精细化工有限公司 | A kind of residual recoverying and utilizing method of fluoromethyl pyridine reactor |
Also Published As
Publication number | Publication date |
---|---|
JPS625425B2 (en) | 1987-02-04 |
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