JPS5553227A - Preparation of beta-phenethyl alcohol - Google Patents
Preparation of beta-phenethyl alcoholInfo
- Publication number
- JPS5553227A JPS5553227A JP12519778A JP12519778A JPS5553227A JP S5553227 A JPS5553227 A JP S5553227A JP 12519778 A JP12519778 A JP 12519778A JP 12519778 A JP12519778 A JP 12519778A JP S5553227 A JPS5553227 A JP S5553227A
- Authority
- JP
- Japan
- Prior art keywords
- solvent
- promide
- phenylethyl
- under normal
- beta
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Abstract
PURPOSE: To obtain the title compound in high purity and yield through simple procedures under normal pressures, by hydrolyzing β-phenylethyl promide in the presence of a specific solvent and a catalyst in an aqueous alkali.
CONSTITUTION: One part by wt. of with β-phenylethyl promide is hydrolyzed with an ankali salt, e.g. sodium or potassium corbonate, and water in the presence of a formate or γ-hydroxydutyrate in 0.3 part by wt. or more, preferably 0.5W10 parts by wt., of a polyethylene glycol, e.g. diethylene, thriethylene, or tetraethylene glycol as a solvent at 100W150°C, preferably 110W140°C, under normal pressures. The formed alkali metal bromide is separated by filtration, and the high-purity objective compound is obtained by distilling off a high-boiling solvent.
COPYRIGHT: (C)1980,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP12519778A JPS5553227A (en) | 1978-10-13 | 1978-10-13 | Preparation of beta-phenethyl alcohol |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP12519778A JPS5553227A (en) | 1978-10-13 | 1978-10-13 | Preparation of beta-phenethyl alcohol |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS5553227A true JPS5553227A (en) | 1980-04-18 |
Family
ID=14904313
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP12519778A Pending JPS5553227A (en) | 1978-10-13 | 1978-10-13 | Preparation of beta-phenethyl alcohol |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5553227A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2007059169A (en) * | 2005-08-24 | 2007-03-08 | Matsushita Electric Ind Co Ltd | Dial rotation transmission structure |
-
1978
- 1978-10-13 JP JP12519778A patent/JPS5553227A/en active Pending
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2007059169A (en) * | 2005-08-24 | 2007-03-08 | Matsushita Electric Ind Co Ltd | Dial rotation transmission structure |
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