JPS5473753A - Preparation of urethane - Google Patents
Preparation of urethaneInfo
- Publication number
- JPS5473753A JPS5473753A JP13973577A JP13973577A JPS5473753A JP S5473753 A JPS5473753 A JP S5473753A JP 13973577 A JP13973577 A JP 13973577A JP 13973577 A JP13973577 A JP 13973577A JP S5473753 A JPS5473753 A JP S5473753A
- Authority
- JP
- Japan
- Prior art keywords
- compound
- vanadium
- palladium
- per gram
- gram atom
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To obtain urethane which is a raw material for polyurethane, by reacting an aromatic nitro compound with an OH group-containing organic compound and CO, using a catalyst consisting of metallic palladium or its compound, a vanadium compound, a tertiary amine and hydrogen chloride.
CONSTITUTION: An aromatic compound is reacted with an OH group-containing organic compound, e.g. a mono-or polyhydric alcohol or phenol, and CO in the presence of a catalyst consisting of metallic palladium or its compound, e.g. a palladium halide, etc. in an amount calculated as 0.001W1wt.% of simple palladium, 10W100 gram atoms per gram atom. of Pd of a vanadium compound, e.g. vanadium pentoxide, etc., and 1W50 moles per gram atom Pd of tertiary amine, e.g. pyridine, etc., and 1W10 moles per gram atom of vanadium of hydrogen chloride under a partial pressure of CO of 1W500 kglcm2 at 100W240°C for 10 minW6 hr to give urethane.
COPYRIGHT: (C)1979,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP13973577A JPS5473753A (en) | 1977-11-21 | 1977-11-21 | Preparation of urethane |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP13973577A JPS5473753A (en) | 1977-11-21 | 1977-11-21 | Preparation of urethane |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5473753A true JPS5473753A (en) | 1979-06-13 |
JPS6115868B2 JPS6115868B2 (en) | 1986-04-26 |
Family
ID=15252148
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP13973577A Granted JPS5473753A (en) | 1977-11-21 | 1977-11-21 | Preparation of urethane |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5473753A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS56131557A (en) * | 1980-03-19 | 1981-10-15 | Mitsubishi Chem Ind Ltd | Preparation of aromatic carbamic acid ester |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH03140086A (en) * | 1989-10-26 | 1991-06-14 | Matsushita Electric Works Ltd | Telephone system |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5198240A (en) * | 1975-01-30 | 1976-08-30 |
-
1977
- 1977-11-21 JP JP13973577A patent/JPS5473753A/en active Granted
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5198240A (en) * | 1975-01-30 | 1976-08-30 |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS56131557A (en) * | 1980-03-19 | 1981-10-15 | Mitsubishi Chem Ind Ltd | Preparation of aromatic carbamic acid ester |
Also Published As
Publication number | Publication date |
---|---|
JPS6115868B2 (en) | 1986-04-26 |
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