JPH11226952A - Resin impregnation device and resin impregnation method using the device - Google Patents

Resin impregnation device and resin impregnation method using the device

Info

Publication number
JPH11226952A
JPH11226952A JP3464198A JP3464198A JPH11226952A JP H11226952 A JPH11226952 A JP H11226952A JP 3464198 A JP3464198 A JP 3464198A JP 3464198 A JP3464198 A JP 3464198A JP H11226952 A JPH11226952 A JP H11226952A
Authority
JP
Japan
Prior art keywords
resin
base material
fiber base
impregnation
resin impregnation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP3464198A
Other languages
Japanese (ja)
Inventor
Shigehiro Konno
繁宏 近野
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Showa Denko Materials Co Ltd
Original Assignee
Hitachi Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hitachi Chemical Co Ltd filed Critical Hitachi Chemical Co Ltd
Priority to JP3464198A priority Critical patent/JPH11226952A/en
Publication of JPH11226952A publication Critical patent/JPH11226952A/en
Pending legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29BPREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B15/00Pretreatment of the material to be shaped, not covered by groups B29B7/00 - B29B13/00
    • B29B15/08Pretreatment of the material to be shaped, not covered by groups B29B7/00 - B29B13/00 of reinforcements or fillers
    • B29B15/10Coating or impregnating independently of the moulding or shaping step
    • B29B15/12Coating or impregnating independently of the moulding or shaping step of reinforcements of indefinite length
    • B29B15/122Coating or impregnating independently of the moulding or shaping step of reinforcements of indefinite length with a matrix in liquid form, e.g. as melt, solution or latex
    • B29B15/125Coating or impregnating independently of the moulding or shaping step of reinforcements of indefinite length with a matrix in liquid form, e.g. as melt, solution or latex by dipping

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Reinforced Plastic Materials (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)

Abstract

PROBLEM TO BE SOLVED: To provide a resin impregnation device which is capable of improving the impregnation properties of a liquid resin with a fiber base material at a low cost, and a resin impregnation method using the device. SOLUTION: This resin impregnation device is equipped with a supply roll for supplying a fiber base material 2, a feed device for paying off the fiber base material 2, an impregnation roll 7 for bringing a liquid resin 3 into contact with the fiber base material 2 paid off and a resin impregnation tank 4 for supplying the liquid resin 3 to the fiber base material 2. In addition, the resin impregnation device has the resin impregnation tank 4 installed on an ultrasonic vibration device in a freely vibration manner. Further, the resin impregnation device drives the supply roll for supplying the fiber base material 2 to pay off the fiber base material 2 with the help of the feed device and at the same time, makes the fiber base material 2 come into contact with the liquid resin 3 stored in the resin impregnation tank 4. Then the resin impregnation device applies an ultrasonic vibration to the liquid resin 3 while impregnating the fiber base material 2 with the liquid resin 3 using the impregnation roll 7.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は、プリプレグの製造
工程における繊維基材の樹脂含浸装置とその装置を用い
た樹脂含浸方法に関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to an apparatus for impregnating a fiber substrate with a resin in a prepreg manufacturing process and a method for impregnating a resin using the apparatus.

【0002】[0002]

【従来の技術】プリント配線板に用いられるプリプレグ
は、紙、ガラス布、合成繊維または天然繊維などの織布
や不織布などの繊維基材に、フェノール樹脂、エポキシ
樹脂、ポリイミド樹脂、ポリアミド樹脂などの液状の熱
硬化性樹脂(以下、液状樹脂という)を含浸させ、この
液状樹脂の付着量をスクイズロールなどで調整し、加熱
・乾燥により液状樹脂を半硬化状態にしている。従来、
液状樹脂の含浸方法として、液状樹脂に繊維基材を直接
浸漬して含浸させる浸漬法や液状樹脂を付着させたロー
ルに繊維基材を接触させ、ロールを介して間接的に含浸
させるキス法などが知られている。
2. Description of the Related Art A prepreg used for a printed wiring board is formed on a fiber base material such as woven or non-woven fabric such as paper, glass cloth, synthetic fiber or natural fiber, and phenol resin, epoxy resin, polyimide resin or polyamide resin. A liquid thermosetting resin (hereinafter, referred to as a liquid resin) is impregnated, the amount of the liquid resin adhered is adjusted by a squeeze roll or the like, and the liquid resin is semi-cured by heating and drying. Conventionally,
Examples of the method of impregnating the liquid resin include a dipping method in which the fiber base material is directly immersed in the liquid resin and impregnation, and a kiss method in which the fiber base material is brought into contact with a roll to which the liquid resin is adhered and indirectly impregnated through the roll. It has been known.

【0003】[0003]

【発明が解決しようとする課題】ところで、従来の含浸
方法では、プリプレグ中に気泡が残ると、硬化後にプリ
プレグの表面が平滑にならず、凹凸面が形成されてしま
い、耐熱性などに劣り性能的に安定したプリプレグが得
られないという課題がある。この課題を解決するために
は、繊維基材への液状樹脂の含浸性を向上させるのに、
液状樹脂に浸漬させる時間や距離を長く設定したり、塗
工速度を遅く設定したりしている。しかし、このような
方法では、生産性が低く、気泡除去の効果も不十分で、
プリプレグ表面の平滑性も困難であると共に、粘度を低
下するため溶剤量を多くしなければならず、コスト高に
なるなどの課題がある。
However, in the conventional impregnation method, if air bubbles remain in the prepreg, the surface of the prepreg will not be smooth after curing and an uneven surface will be formed, resulting in poor heat resistance. There is a problem that a stable prepreg cannot be obtained. In order to solve this problem, to improve the impregnation of the liquid resin into the fiber base material,
The time and distance of immersion in the liquid resin are set long, and the coating speed is set low. However, with such a method, productivity is low and the effect of removing bubbles is insufficient,
The surface smoothness of the prepreg is difficult, and the amount of the solvent must be increased in order to lower the viscosity.

【0004】本発明は、低コストで、繊維基材への液状
樹脂の含浸性を向上させることが可能な樹脂含浸装置と
その装置を用いた樹脂含浸方法を提供することを目的と
する。
An object of the present invention is to provide a resin impregnating apparatus capable of improving the impregnation property of a liquid resin into a fiber base material at low cost, and a resin impregnating method using the apparatus.

【0005】[0005]

【課題を解決するための手段】本発明の樹脂含浸装置
は、繊維基材を供給する供給ロールと、繊維基材を巻き
出す送り装置と、巻き出された繊維基材に液状樹脂を接
触させる含浸ロールと、繊維基材に液状樹脂を供給する
樹脂含浸槽とを備え、その樹脂含浸槽を超音波振動装置
に振動可能に取り付けたことを特徴とする。
According to the present invention, there is provided a resin impregnating apparatus for supplying a fiber base material, a feeding device for unwinding the fiber base material, and bringing a liquid resin into contact with the unwound fiber base material. An impregnating roll and a resin impregnation tank for supplying a liquid resin to the fiber base material are provided, and the resin impregnation tank is attached to an ultrasonic vibrator so as to be able to vibrate.

【0006】このような装置を用いれば、繊維基材を供
給する供給ロールから、送り装置によって繊維基材を巻
き出しながら、樹脂含浸槽に貯えられた液状樹脂に接触
させて含浸ロールによって液状樹脂を含浸させながら、
超音波振動を与えることができる。
[0006] With such an apparatus, the fiber base is unwound from the supply roll for supplying the fiber base while being fed by the feeder, and is brought into contact with the liquid resin stored in the resin impregnation tank. While impregnating
Ultrasonic vibration can be given.

【0007】[0007]

【発明の実施の形態】図1に示すように、基材供給装置
1から送りロール6によって送り出された紙、ガラス
布、合成繊維または天然繊維などの織布や不織布などの
繊維基材2は、超音波振動装置に振動可能に取り付けら
れた樹脂含浸槽4に貯えられた液状樹脂3に接触させな
がら、含浸ロール7で液状樹脂を含浸しながら、超音波
振動を与えて所定のスピードで通過させ、この振動によ
り繊維基材2が樹脂含浸槽4を通過する過程において、
繊維基材2内の気泡、繊維基材2表面の付着物を除去
し、繊維基材2に対する液状樹脂3の含浸が図れる。ま
た、樹脂含浸槽4内で除去された異物を濾過し、液状樹
脂3を循環することでより効果的である。樹脂含浸槽4
から出た繊維基材2は、乾燥機5により熱乾燥処理が施
され半硬化状態のプリプレグとなる。図1に示す樹脂含
浸装置を用い、繊維基材2に厚さ200μmのガラス布
を用いた。また、振動による静電気発生を除去するため
にアースを取った。この状態で、塗工速度を10m/分
とし、液状のエポキシ樹脂を含浸させた。この樹脂含浸
装置により得られたプリプレグは、上面から見た際の単
位面積当たりに占める気泡の割合、つまりプリプレグの
気泡面積率は28%であった。比較例として、超音波振
動装置を停止して、同じ条件でプリプレグを製造した結
果、得られたプリプレグの気泡面積率は48%であっ
た。このことから明らかなように、本発明に係わる含浸
装置によると、従来よりも液状樹脂の含有率が高まって
いることが確認できた。
DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS As shown in FIG. 1, a fiber substrate 2 such as woven or non-woven fabric such as paper, glass cloth, synthetic fiber or natural fiber sent from a substrate supply device 1 by a feed roll 6 is used. While being in contact with the liquid resin 3 stored in the resin impregnating tank 4 attached to the ultrasonic vibrating device so as to vibrate, the liquid resin is impregnated with the impregnating roll 7 while applying ultrasonic vibration to pass at a predetermined speed. In the process in which the fiber base material 2 passes through the resin impregnation tank 4 due to this vibration,
Bubbles in the fiber base material 2 and deposits on the surface of the fiber base material 2 are removed, so that the fiber base material 2 can be impregnated with the liquid resin 3. Further, it is more effective to filter foreign matter removed in the resin impregnation tank 4 and circulate the liquid resin 3. Resin impregnation tank 4
Is subjected to a heat drying treatment by a dryer 5 to be a semi-cured prepreg. Using a resin impregnating apparatus shown in FIG. In addition, a ground was taken to eliminate the generation of static electricity due to vibration. In this state, the coating speed was set to 10 m / min and the liquid epoxy resin was impregnated. In the prepreg obtained by this resin impregnating apparatus, the proportion of bubbles per unit area when viewed from the top, that is, the bubble area ratio of the prepreg was 28%. As a comparative example, the ultrasonic vibration device was stopped, and a prepreg was manufactured under the same conditions. As a result, the bubble area ratio of the obtained prepreg was 48%. As is apparent from this, it was confirmed that the impregnating apparatus according to the present invention had a higher content of the liquid resin than the conventional one.

【0008】[0008]

【発明の効果】以上に説明したとおり、本発明によっ
て、低コストで、繊維基材への液状樹脂の含浸性を向上
させることが可能な樹脂含浸装置とその装置を用いた樹
脂含浸方法を提供することができる。
As described above, the present invention provides a resin impregnating apparatus capable of improving the impregnation property of a liquid resin into a fiber base material at low cost and a resin impregnating method using the apparatus. can do.

【図面の簡単な説明】[Brief description of the drawings]

【図1】本発明における樹脂含浸装置を示す説明図であ
る。
FIG. 1 is an explanatory view showing a resin impregnating apparatus according to the present invention.

【符号の説明】[Explanation of symbols]

1.基材供給装置 2.繊維基材 3.液状樹脂 4.樹脂含浸
槽 5.乾燥機 6.送りロー
ル 7.含浸ロール
1. Substrate supply device 2. Fiber base material 3. Liquid resin 4. Resin impregnation tank 5. Dryer 6. Feed roll 7. Impregnating roll

Claims (2)

【特許請求の範囲】[Claims] 【請求項1】繊維基材を供給する供給ロールと、繊維基
材を巻き出す送り装置と、巻き出された繊維基材に液状
樹脂を接触させる含浸ロールと、含浸ロールと繊維基材
に液状樹脂を供給する樹脂含浸槽とを備え、その樹脂含
浸槽を超音波振動装置に振動可能に取り付けたことを特
徴とする樹脂含浸装置。
1. A supply roll for supplying a fiber base material, a feeding device for unwinding the fiber base material, an impregnating roll for bringing a liquid resin into contact with the unwound fiber base material, and a liquid impregnating roll and the fiber base material A resin impregnating apparatus comprising: a resin impregnating tank for supplying a resin; and the resin impregnating tank is attached to an ultrasonic vibrator so as to be able to vibrate.
【請求項2】繊維基材を供給する供給ロールから、送り
装置によって繊維基材を巻き出しながら、樹脂含浸槽に
貯えた液状樹脂に接触させて含浸ロールによって液状樹
脂を含浸させながら、超音波振動を与えることを特徴と
する樹脂含浸方法。
2. An ultrasonic wave while the fiber base material is unwound from the supply roll for supplying the fiber base material while being brought into contact with the liquid resin stored in the resin impregnation tank while being unwound by the feeder. A resin impregnation method characterized by applying vibration.
JP3464198A 1998-02-17 1998-02-17 Resin impregnation device and resin impregnation method using the device Pending JPH11226952A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP3464198A JPH11226952A (en) 1998-02-17 1998-02-17 Resin impregnation device and resin impregnation method using the device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP3464198A JPH11226952A (en) 1998-02-17 1998-02-17 Resin impregnation device and resin impregnation method using the device

Publications (1)

Publication Number Publication Date
JPH11226952A true JPH11226952A (en) 1999-08-24

Family

ID=12420067

Family Applications (1)

Application Number Title Priority Date Filing Date
JP3464198A Pending JPH11226952A (en) 1998-02-17 1998-02-17 Resin impregnation device and resin impregnation method using the device

Country Status (1)

Country Link
JP (1) JPH11226952A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2016203397A (en) * 2015-04-15 2016-12-08 東邦テナックス株式会社 Method for producing prepreg
CN111263289A (en) * 2018-11-30 2020-06-09 大原博 Method for manufacturing elastic wave by using auxiliary material to assist impregnation

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2016203397A (en) * 2015-04-15 2016-12-08 東邦テナックス株式会社 Method for producing prepreg
CN111263289A (en) * 2018-11-30 2020-06-09 大原博 Method for manufacturing elastic wave by using auxiliary material to assist impregnation

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