JPH11137973A - Separation membrane evaluating device - Google Patents

Separation membrane evaluating device

Info

Publication number
JPH11137973A
JPH11137973A JP32219897A JP32219897A JPH11137973A JP H11137973 A JPH11137973 A JP H11137973A JP 32219897 A JP32219897 A JP 32219897A JP 32219897 A JP32219897 A JP 32219897A JP H11137973 A JPH11137973 A JP H11137973A
Authority
JP
Japan
Prior art keywords
separation membrane
cell
separation
cells
liquid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP32219897A
Other languages
Japanese (ja)
Other versions
JP3080051B2 (en
Inventor
Yuji Nishida
祐二 西田
Shinichi Jizo
眞一 地蔵
Atsuto Takamoto
敦人 高本
Hajime Hisada
肇 久田
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nitto Denko Corp
Original Assignee
Nitto Denko Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nitto Denko Corp filed Critical Nitto Denko Corp
Priority to JP09322198A priority Critical patent/JP3080051B2/en
Publication of JPH11137973A publication Critical patent/JPH11137973A/en
Application granted granted Critical
Publication of JP3080051B2 publication Critical patent/JP3080051B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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  • Separation Using Semi-Permeable Membranes (AREA)

Abstract

PROBLEM TO BE SOLVED: To accurately evaluate plural separation membrane samples at the same time by providing each cell and cells of specific pieces or more capable of inserting a separation membrane between the cells, providing an original liquid introducing passage and a concentrated liquid discharge passage in one of the cells opposed to each other and providing a permeated liquid discharge passage in another cell. SOLUTION: The performance evaluating device for the separation membrane is constituted so that the separation membranes 11, 26, 34 different in kind from each other are attached every one piece among >=3 cells, the original liquid is supplied to the separation membranes 11, 26, 34 in parallel and the performance evaluation of the separation membranes 11, 26, 34 is performed at the same time. Relating to the cells, an attaching part 12 is provided at the center of the upper surface of a 1st stage cell 10 of the lowermost stage, a permeated liquid flow passage material 13 is placed thereon, the separation membrane 11 is placed thereon and a seal ring is built-up on the separation membrane 11. An original liquid introducing port 15 is provided at the side of the 1st stage cell 10 and the original liquid is fed to the separation membranes 11, 26, 34 through an original liquid flow passage 16. And the permeated liquid discharge passage 17 is provided below the attaching part 12 to discharge the permeated liquid from the separation membrane 11.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の分野】本発明は液体の分離、濃縮を行う逆浸透
膜、限外濾過膜、精密濾過膜などの分離膜の性能評価装
置に関する。
The present invention relates to an apparatus for evaluating the performance of a separation membrane such as a reverse osmosis membrane, an ultrafiltration membrane and a microfiltration membrane for separating and concentrating a liquid.

【0002】[0002]

【従来技術】処理原液に対する最適の分離膜を決定する
には、実際に分離膜を用いて原液を処理し評価する必要
がある。図4はこのような従来の分離膜評価装置の一具
体例を示す概略断面図である。かかる従来の分離膜評価
装置は上部セル100及び下部セル101が組み合わされて耐
圧セルを形成する。上部セル100は原液導入路102及び濃
縮液排出路103を備え、一方、下部セル101は透過液排出
路104を備える。下部セル100の上面中央には、分離膜10
5を装着する凹部である装着部106が設けられる。該装着
部106には、透過液流路材107が敷設された上に分離膜10
5が載置され、該分離膜105の上部にはシールリング108
が組み込まれる。また、下部セル101の装着部106下方に
は透過液排出路104が設けられる。上部セル100はその下
面が下部セル101の装着部106と嵌まり合うよう形成され
ており、ボルト、ナット等の締結手段を用いて前記シー
ルリング108を介して下部セル101との間に、評価すべき
分離膜105を液密に保持する。また、原液はポンプ等で
加圧されて原液導入路102より導入され、上部セル100の
下面と分離膜105との間の空間に供給される。ついで、
分離膜105上の原液は濃縮液排出路103より排出、循環さ
れ、一方濾過された透過液は透過液排出路104から外部
に取り出される。
2. Description of the Related Art In order to determine an optimum separation membrane for a processing stock solution, it is necessary to actually process and evaluate the stock solution using a separation membrane. FIG. 4 is a schematic sectional view showing a specific example of such a conventional separation membrane evaluation apparatus. In such a conventional separation membrane evaluation apparatus, the upper cell 100 and the lower cell 101 are combined to form a breakdown voltage cell. The upper cell 100 includes a stock solution introduction channel 102 and a concentrated solution discharge channel 103, while the lower cell 101 includes a permeate solution discharge channel 104. In the center of the upper surface of the lower cell 100, a separation membrane 10
A mounting portion 106, which is a recess for mounting 5, is provided. The mounting portion 106 has a permeated liquid channel material 107 laid thereon and
5 is placed, and a seal ring 108 is provided above the separation membrane 105.
Is incorporated. A permeated liquid discharge passage 104 is provided below the mounting portion 106 of the lower cell 101. The upper cell 100 is formed such that its lower surface is fitted with the mounting portion 106 of the lower cell 101, and is fastened between the lower cell 101 and the lower cell 101 through the seal ring 108 using fastening means such as bolts and nuts. The separation membrane 105 to be maintained is kept liquid-tight. The undiluted solution is pressurized by a pump or the like, introduced into the undiluted solution introduction passage 102, and supplied to the space between the lower surface of the upper cell 100 and the separation membrane 105. Then
The undiluted solution on the separation membrane 105 is discharged and circulated from the concentrated liquid discharge channel 103, while the filtered permeate is taken out from the permeated liquid discharge channel 104 to the outside.

【0003】[0003]

【発明が解決しようとする課題】処理原液に対して最適
な分離膜を選択するには、数多くの分離膜について検討
しなければならない。しかしながら、前記従来の分離膜
評価装置では1度に1枚の分離膜しか評価ができず、く
り返し交換して1枚ずつ分離膜を評価する必要がある。
このため、分離膜の交換作業に手間を要し、全体の評価
時間も長くなる。また、経時的に性質が変化する原液の
場合、時間を経て異なる分離膜を評価しても原液の変質
により評価結果の信頼性が乏しい。
In order to select an optimum separation membrane for a stock solution to be treated, a large number of separation membranes must be examined. However, the above-described conventional separation membrane evaluation apparatus can evaluate only one separation membrane at a time, and it is necessary to repeatedly replace and evaluate one separation membrane at a time.
For this reason, it takes time and effort to replace the separation membrane, and the overall evaluation time becomes longer. Further, in the case of a stock solution whose properties change with time, even if different separation membranes are evaluated over time, the reliability of the evaluation result is poor due to deterioration of the stock solution.

【0004】かかる問題点を解消するため、同じ分離膜
評価装置を複数台並べて同時に評価を行う方法もある。
しかしながら、このような方法では、ポンプからの接続
配管及び分離膜評価装置間の接続配管が長くなったり、
また複雑になるなど、評価の準備に時間を要し、また流
路抵抗が増大して運転条件の設定が困難となり好ましく
ない。また、従来の分離膜評価装置では、原液は原液導
入路から分離膜面上に広がった後濃縮液排出路に向かう
が、原液導入路と濃縮液排出路とを直線的に結ぶ部分の
流速が大きく、分離膜の周辺部分になるほど流速が低下
し、滞留部が生ずる場合もある。このように流速の差が
大きい場合、分離膜性能について信頼性の高いデータは
得られない。
[0004] In order to solve such a problem, there is a method of arranging a plurality of the same separation membrane evaluation devices and simultaneously evaluating them.
However, in such a method, the connection pipe from the pump and the connection pipe between the separation membrane evaluation device become long,
In addition, it takes time to prepare for evaluation, such as complexity, and the flow path resistance increases, which makes it difficult to set operating conditions, which is not preferable. In addition, in the conventional separation membrane evaluation device, the undiluted solution spreads from the undiluted solution introduction path onto the separation membrane surface and then flows to the concentrated liquid discharge path. In some cases, the flow velocity decreases as the distance from the periphery of the separation membrane increases, and a stagnation portion may occur. When the flow velocity difference is large as described above, highly reliable data on the performance of the separation membrane cannot be obtained.

【0005】本発明の目的は、かかる従来装置の欠点を
解消し複数の分離膜試料を一度に正確に評価することの
できる分離膜評価装置を提供することにある。本発明の
評価装置は、3つ以上のセルに分割された各セルの間
に、評価対象の分離膜を取り付け、同時に複数の分離膜
の性能を評価することができる。
SUMMARY OF THE INVENTION An object of the present invention is to provide a separation membrane evaluation apparatus capable of solving the drawbacks of the conventional apparatus and accurately evaluating a plurality of separation membrane samples at once. The evaluation apparatus of the present invention can attach a separation membrane to be evaluated between each cell divided into three or more cells, and can simultaneously evaluate the performance of a plurality of separation membranes.

【0006】[0006]

【課題を解決するための手段】すなわち、本発明は、複
数の平膜状の分離膜を装着し膜性能の評価を行う分離膜
評価装置であって、該装置は各セルとセルの間に分離膜
を挟むことのできる3つ以上のセルからなり、各対向す
るセルの一方には装着した各分離膜に対する原液導入路
および濃縮液排出路が設けられ、他方のセルには該分離
膜からの透過液排出路が設けられてなる分離膜評価装置
を提供するものである。
That is, the present invention relates to a separation membrane evaluation apparatus for evaluating a membrane performance by mounting a plurality of flat membrane separation membranes, wherein the apparatus is provided between each cell. It consists of three or more cells capable of sandwiching a separation membrane, and one of the opposed cells is provided with a stock solution introduction path and a concentrated solution discharge path for each of the mounted separation membranes, and the other cell is provided with the separation membrane from the separation membrane. The present invention also provides a separation membrane evaluation device provided with a permeated liquid discharge passage.

【0007】本発明の装置によれば、複数枚の分離膜を
容易に同時に評価することができる。また、本発明の他
の態様によれば分離膜面上の流速を均一にして信頼性の
高い評価を行うことができる。
According to the apparatus of the present invention, a plurality of separation membranes can be easily and simultaneously evaluated. Further, according to another aspect of the present invention, a highly reliable evaluation can be performed by making the flow velocity on the separation membrane surface uniform.

【0008】[0008]

【実施の態様】つぎに具体例を挙げ図面を参照しながら
本発明をさらに詳細に説明する。図1は、本発明の評価
装置の一具体例を示す概略断面図である。図1におい
て、評価装置は、ほぼ円筒形で偏平な4つのセルを縦に
積み重ねた形態をなし、各セルの間に第1〜3の異なる
種類の分離膜が各1枚ずつ装着される。原液はこれら各
分離膜に並列に供給され、第1〜3の3枚の分離膜の性
能評価を一度に行うことができる。
DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS The present invention will now be described in more detail with reference to the drawings and specific examples. FIG. 1 is a schematic sectional view showing a specific example of the evaluation device of the present invention. In FIG. 1, the evaluation apparatus has a form in which four cells having a substantially cylindrical flat shape are vertically stacked, and first to third different types of separation membranes are mounted between each cell. The stock solution is supplied in parallel to each of these separation membranes, and the performance evaluation of the first to third three separation membranes can be performed at once.

【0009】(i)1段目セル 最下段の1段目セル10の上面中央には、第1分離膜1
1を装填する凹部である第1装着部12が設けられ、こ
こには透過液流路材13が敷かれた上に第1分離膜11
が載置され、該分離膜11の上にシールリング21が組
み込まれる。一方、1段目セル10の側方には装置全体
への原液の導入口である原液導入口15が設けられ、原
液流路16を通じて第1〜3の分離膜への原液の供給が
行われる。また、前記、第1装着部12の凹部下方に
は、第1分離膜11からの透過液を排出する透過液排出
路17が設けられる。
(I) First-stage cell In the center of the upper surface of the lowest-stage first-stage cell 10, the first separation film 1
1 is provided with a first mounting portion 12 which is a concave portion in which the first separation membrane 11 is placed.
Is mounted, and a seal ring 21 is assembled on the separation membrane 11. On the other hand, on the side of the first-stage cell 10, an undiluted solution inlet 15 which is an inlet for undiluted solution to the entire apparatus is provided, and the undiluted solution is supplied to the first to third separation membranes through the undiluted solution channel 16. . A permeated liquid discharge passage 17 for discharging permeated liquid from the first separation membrane 11 is provided below the concave portion of the first mounting portion 12.

【0010】(ii)2段目セル 前記1段目セル10の上には、その下面がこれと嵌まり
合うよう形成された2段目セル20が配置される。2段
目セル20の下面は、前記1段目セル10上面の第1装
着部12と嵌まり合う形態に成形され、シールリング2
1を介して1段目セル10との間に第1分離膜11を液
密に保持する。
(Ii) Second-stage cell On the first-stage cell 10, a second-stage cell 20 whose lower surface is formed so as to fit therewith is arranged. The lower surface of the second-stage cell 20 is formed into a form that fits with the first mounting portion 12 on the upper surface of the first-stage cell 10, and the seal ring 2
The first separation membrane 11 is kept liquid-tight between the first separation cell 10 and the first-stage cell 10 via the first separation cell 1.

【0011】一方、2段目セル20の側方には、前記1
段目セル10の原液流路16に連通する原液流路22が
設けられ、これから分岐して第1分離膜の中央部に処理
原液を供給する第1原液導入路23が設けられる。ま
た、前記2段目セル20下面の側方からは第1分離膜1
1からの濃縮液を排出する濃縮液排出路24が設けられ
る。なお、2段目セル20の下面には、第1分離膜11
の中央に供給された原液が濃縮液排出路24に直接短絡
して流れないよう流路仕切り突起25が設けられる。
On the other hand, beside the second-stage cell 20,
An undiluted liquid flow path 22 communicating with the undiluted liquid flow path 16 of the stage cell 10 is provided, and a first undiluted liquid introduction path 23 for branching off from the undiluted liquid flow path 16 and supplying a processing undiluted liquid to a central portion of the first separation membrane is provided. In addition, the first separation membrane 1 is provided from the side of the lower surface of the second-stage cell 20.
A concentrate discharge path 24 for discharging the concentrate from 1 is provided. The first separation film 11 is provided on the lower surface of the second-stage cell 20.
A channel partition projection 25 is provided so that the undiluted solution supplied to the center of the does not directly flow into the concentrated solution discharge path 24 due to a short circuit.

【0012】図2はかかる突起の一具体例を示す概略図
である。図2に示すように流路仕切り突起25は、平面
方向から見てほぼ円形の仕切りを形成し一部に切り欠き
が設けられる。また、突起25の高さは分離膜に接しな
いぎりぎりの高さとするのが好ましい。したがって、装
着部の中央の原液導入路23より供給された原液は装着
部に装填された分離膜の膜面を同心円状に設けた突起2
5に沿って図中の矢印のように均一に移動したのち、濃
縮液排出路24より排出される。なお、流路仕切り突起
の数、断面形状、幅、高さ等は流体力学的手法で均一な
圧力損失及び流速さらには加工のやり易さを考慮して設
計することができる。
FIG. 2 is a schematic view showing a specific example of such a projection. As shown in FIG. 2, the flow path partitioning projection 25 forms a substantially circular partition when viewed from a plane direction, and is partially provided with a notch. Further, it is preferable that the height of the projection 25 is almost the same as the height that does not contact the separation membrane. Therefore, the undiluted solution supplied from the undiluted solution introduction passage 23 at the center of the mounting portion is formed by the projection 2 having the membrane surface of the separation membrane loaded in the mounting portion provided concentrically.
After moving uniformly along arrow 5 as shown by the arrow in the figure, the liquid is discharged from the concentrated liquid discharge path 24. The number, cross-sectional shape, width, height, and the like of the flow path partitioning projections can be designed by a hydrodynamic method in consideration of uniform pressure loss and flow rate, as well as ease of processing.

【0013】一方、2段目セルの上面中央には、前記1
段目セルと同様にして、第2分離膜26を装着するため
の凹部である第2装着部27が設けられる。第2装着部
には前記と同様透過液流路材が敷かれた上に第2分離膜
が載置され、その上にシールリングが組み込まれる。
On the other hand, at the center of the upper surface of the second cell,
Similarly to the stage cell, a second mounting portion 27 which is a concave portion for mounting the second separation membrane 26 is provided. A second separation membrane is placed on the permeated liquid flow path material on the second mounting portion in the same manner as described above, and a seal ring is assembled thereon.

【0014】なお、第2装着部の凹部下方には、第2分
離膜からの透過液を排出する透過液排出路(図示せず)が
設けられる。
A permeate discharge passage (not shown) for discharging the permeate from the second separation membrane is provided below the recess of the second mounting portion.

【0015】(iii)3段目セル 3段目セル30は、前記2段目セルとほぼ同一の構造を
なし、下面にて2段目セルとの間に第2分離膜26を保
持し、一方、上面にて4段目セルとの間に第3分離膜3
4を保持する。したがって、2段目セル20と同様に、
セルの側方には2段目セルの原液流路22に連通する原
液流路31、これから分岐して第2分離膜に処理原液を
供給する第2原液導入路32が設けられると共に第2分
離膜からの濃縮液を排出する第2濃縮液排出路33が設
けられる。なお、3段目セルの下面には、前記と同様に
流路仕切り突起が設けられる。
(Iii) Third-stage cell The third-stage cell 30 has substantially the same structure as that of the second-stage cell, and holds the second separation membrane 26 between the second-stage cell and the lower surface, On the other hand, the third separation membrane 3 is provided between the upper surface and the fourth cell.
Hold 4. Therefore, similar to the second-stage cell 20,
On the side of the cell, there is provided a stock solution flow path 31 communicating with the stock solution flow path 22 of the second-stage cell, and a second stock solution introduction passage 32 branched therefrom to supply a stock solution to be processed to the second separation membrane. A second concentrate discharge path 33 for discharging the concentrate from the membrane is provided. In addition, a flow path partitioning projection is provided on the lower surface of the third-stage cell as described above.

【0016】一方、3段目セルの上面中央には、第3分
離膜34を装着するため、前記と同様の第3装着部35
が設けられる。さらに、第3装着部の凹部下方に第3分
離膜からの透過液を排出する透過液導出路(図示せず)が
設けられる。
On the other hand, at the center of the upper surface of the third-stage cell, a third mounting portion 35 similar to the above is provided for mounting the third separation membrane 34.
Is provided. Further, a permeated liquid outlet (not shown) for discharging the permeated liquid from the third separation membrane is provided below the concave portion of the third mounting portion.

【0017】(iv)4段目セル 最上部の4段目セル40の下面は、基本的に前記2段目
セル及び3段目セルの下面と同様の形態を有しており、
3段目セル30との間で第3分離膜34を保持する。す
なわち、4段目セル40の下面は、3段目セル30上面
の第3装着部35と嵌まり合う形態に成形され、シール
リングを介して3段目セルとの間に第3分離膜を液密に
保持する。また、4段目セル40の側方には、3段目セ
ルの原液流路31につながる原液流路41が設けられ、
これから第3分離膜の中央部に原液を供給する第3原液
導入路42が設けられる。また、4段目セル下面の側方
には、第3分離膜34からの濃縮液を排出する濃縮液排
出路43が設けられる。なお、4段目セルの下面には、
第2及び第3セルの場合と同様の流路仕切り突起が設け
られる。
(Iv) Fourth cell The lower surface of the uppermost fourth cell 40 has basically the same form as the lower surfaces of the second and third cells.
The third separation film 34 is held between the third stage cell 30 and the third stage cell 30. That is, the lower surface of the fourth-stage cell 40 is formed so as to fit with the third mounting portion 35 on the upper surface of the third-stage cell 30, and a third separation membrane is provided between the third-stage cell and the third-stage cell via a seal ring. Keep liquid tight. In addition, on the side of the fourth-stage cell 40, a stock solution flow path 41 connected to the stock solution flow channel 31 of the third-stage cell is provided,
From this, a third undiluted solution introduction path 42 for supplying undiluted solution is provided at the center of the third separation membrane. On the side of the lower surface of the fourth cell, a concentrated liquid discharge passage 43 for discharging the concentrated liquid from the third separation membrane 34 is provided. In addition, on the lower surface of the fourth cell,
The same flow channel partitioning projection as in the case of the second and third cells is provided.

【0018】本発明の分離膜評価装置において、評価す
る分離膜は異なる種類を選んでもよく、また同種の分離
膜を選んでもよい。なお、各段セルの流路はシールリン
グにより液密にシールされる。
In the separation membrane evaluation apparatus of the present invention, different types of separation membranes to be evaluated may be selected, or the same type of separation membrane may be selected. The flow path of each cell is sealed in a liquid-tight manner by a seal ring.

【0019】本発明の評価装置は、耐圧強度や耐腐食性
を得るためステシレス等の金属やアクリル樹脂、硬質塩
化ビニル樹脂等のプラスチックで作製するのが好まし
い。
The evaluation device of the present invention is preferably made of a metal such as stesiless or a plastic such as an acrylic resin or a hard vinyl chloride resin in order to obtain pressure resistance and corrosion resistance.

【0020】各セルは順次重ね合わせてボルト・ナット
で締結して締め付けるか、油圧プレス等を用いて締め付
け、全体を液密な耐圧セルとする。
The cells are sequentially superimposed and fastened with bolts and nuts or tightened using a hydraulic press or the like, so that the whole is a liquid-tight pressure-resistant cell.

【0021】処理原液は、原液導入口15より導入さ
れ、各原液流路16、22、31、41から各々第1〜3
の原液導入路23、32、42に分岐されて分離膜面上に
導入され、各段の濃縮液排出路24、33、43に集まり
排出され循環される。一方、透過液は各段の透過液排出
路より取り出される。
The undiluted solution is introduced from the undiluted solution introduction port 15 and flows through the undiluted solution flow paths 16, 22, 31, 41 from the first to third, respectively.
Are concentrated on the surface of the separation membrane, and are collected, discharged and circulated in the concentrated liquid discharge paths 24, 33, 43 of each stage. On the other hand, the permeated liquid is taken out from the permeated liquid discharge passage of each stage.

【0022】各セルに流れる原液の液量は、流体力学的
手法により均一な圧力損失及び流速になるよう調整され
る。すなわち、原液流路の径を順次小さく、濃縮液流路
の径を順次大きくすることによって均等にすることがで
きる。
The amount of the undiluted solution flowing through each cell is adjusted by a hydrodynamic method so as to obtain a uniform pressure loss and a uniform flow rate. That is, the diameters of the undiluted liquid flow paths can be made smaller and the diameters of the concentrated liquid flow paths can be made larger by making the diameters larger.

【0023】なお、本具体例では3枚の分離膜を同時に
評価できるが、2、3段目セルと同型のセルを増減する
ことにより、2枚以上、適宜の枚数の分離膜を同時に評
価できる。
In this example, three separation membranes can be evaluated at the same time. However, by increasing or decreasing the number of cells of the same type as the second and third cells, two or more and an appropriate number of separation membranes can be simultaneously evaluated. .

【0024】また、図3はセルを4段重ね合わせて、試
験分離膜に対する原液流れが直列となるように構成し
て、3枚の分離膜を同時に評価できるようにした分離膜
評価装置の概略断面図である。各セルの構成は原液が分
離膜に並列に供給される図1の場合と基本的に同じであ
り、第1分離膜における濃縮液が次の第2分離膜の原液
となる。
FIG. 3 is a schematic diagram of a separation membrane evaluation apparatus in which cells are stacked in four stages so that the stock solution flows in series with the test separation membrane so that three separation membranes can be evaluated simultaneously. It is sectional drawing. The configuration of each cell is basically the same as the case of FIG. 1 in which the stock solution is supplied in parallel to the separation membrane, and the concentrated solution in the first separation membrane becomes the stock solution for the next second separation membrane.

【0025】なお、前記具体例においてはセルの平面形
態は略円筒形であるが、これに限らず、四角形、六角形
などの多角形であってもよい。さらに、前記具体例にお
いては、各段セルの上下いずれか一方に原液流路及び濃
縮液排出路を設け、他方に透過液排出路を設けて、セル
を組み立てることによりこれら流路をセルの上下方向に
交互に配置し、各分離膜に対して同じ方向から液の導
入、排出を行っているが、これに限定されるものではな
く、例えば、同一セルの両側の分離膜に対して、各々原
液流路を設けてもよい。
In the above example, the planar shape of the cell is substantially cylindrical, but is not limited to this, and may be a polygon such as a square or a hexagon. Further, in the above specific example, a stock solution flow path and a concentrated solution discharge path are provided on one of the upper and lower sides of each cell, and a permeate discharge path is provided on the other side. The liquids are alternately arranged in the direction and the liquid is introduced and discharged from the same direction for each separation membrane.However, the present invention is not limited to this.For example, for the separation membranes on both sides of the same cell, A stock solution flow path may be provided.

【0026】[0026]

【発明の効果】平膜状の分離膜を収納して性能評価する
分離膜評価装置において、セルを少なくとも3段以上重
ね合わせて2枚以上の分離膜を同時に評価できるように
したことにより、評価作業の簡略化と時間短縮が可能と
なった。また、分離膜面上の流れを均一にする流路仕切
凸部を設けたことによって分離膜性能を高い精度で短時
間に評価できる。
As described above, in a separation membrane evaluation apparatus for storing a flat separation membrane and evaluating its performance, two or more separation membranes can be simultaneously evaluated by stacking at least three or more cells. Work can be simplified and time can be reduced. In addition, by providing the flow path partitioning convex portion for making the flow on the separation membrane surface uniform, the performance of the separation membrane can be evaluated with high accuracy in a short time.

【図面の簡単な説明】[Brief description of the drawings]

【図1】 本発明装置の一具体例を示す概略断面図であ
る。
FIG. 1 is a schematic sectional view showing a specific example of the device of the present invention.

【図2】 本発明装置における分離膜上の原液の流路を
示す模式図である。
FIG. 2 is a schematic diagram showing a flow path of a stock solution on a separation membrane in the apparatus of the present invention.

【図3】 本発明装置の他の具体例を示す概略断面図で
ある。
FIG. 3 is a schematic sectional view showing another specific example of the device of the present invention.

【図4】 従来の評価装置の概略断面図である。FIG. 4 is a schematic sectional view of a conventional evaluation device.

【符号の説明】[Explanation of symbols]

10 1段目セル 11 第1分離膜 12 第1装着部 20 2段目セル 26 第2分離膜 27 第2装着部 30 3段目セル 34 第3分離膜 35 第3装着部 40 4段目セル 10 First-stage cell 11 First separation membrane 12 First mounting unit 20 Second-stage cell 26 Second separation membrane 27 Second mounting unit 30 Third-stage cell 34 Third separation membrane 35 Third mounting unit 40 Fourth-stage cell

───────────────────────────────────────────────────── フロントページの続き (72)発明者 久田 肇 大阪府茨木市下穂積1丁目1番2号 日東 電工株式会社内 ────────────────────────────────────────────────── ─── Continued on the front page (72) Inventor Hajime Hisada 1-1-2 Shimohozumi, Ibaraki-shi, Osaka Nitto Denko Corporation

Claims (5)

【特許請求の範囲】[Claims] 【請求項1】 複数の平膜状の分離膜を装着し膜性能の
評価を行う分離膜評価装置であって、該装置は各セルと
セルの間に分離膜を挟むことのできる3つ以上のセルか
らなり、各対向するセルの一方には装着した各分離膜に
対する原液導入路および濃縮液排出路が設けられ、他方
のセルには該分離膜からの透過液排出路が設けられてな
る分離膜評価装置。
1. A separation membrane evaluation apparatus for mounting a plurality of flat membrane-shaped separation membranes and evaluating membrane performance, the apparatus comprising at least three separation membranes capable of sandwiching a separation membrane between cells. One of the opposed cells is provided with a stock solution introduction path and a concentrated solution discharge path for each of the mounted separation membranes, and the other cell is provided with a permeate discharge path from the separation membrane. Separation membrane evaluation device.
【請求項2】 分離膜に供給された原液が、セル内部に
おいて分離膜表面のほぼ中心部に供給され同心円状に流
れる請求項1の分離膜評価装置。
2. The separation membrane evaluation apparatus according to claim 1, wherein the stock solution supplied to the separation membrane is supplied to a substantially central portion of the surface of the separation membrane inside the cell and flows concentrically.
【請求項3】 各セルへの原液流れを並列に行う請求項
1又は2の分離膜評価装置。
3. The separation membrane evaluation apparatus according to claim 1, wherein the undiluted solution flows to each cell in parallel.
【請求項4】 セルの原液流路径が順次小さくなり、一
方濃縮流路径が順次大きくなる請求項1〜3のいずれか
の分離膜評価装置。
4. The separation membrane evaluation apparatus according to claim 1, wherein the diameter of the raw solution flow path of the cell gradually decreases, while the diameter of the concentration flow path gradually increases.
【請求項5】 各セルの原液流れを直列に行う請求項1
又は2の分離膜評価装置。
5. The method according to claim 1, wherein the undiluted solution flows in each cell in series.
Or the separation membrane evaluation device of 2.
JP09322198A 1997-11-07 1997-11-07 Separation membrane evaluation device Expired - Fee Related JP3080051B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP09322198A JP3080051B2 (en) 1997-11-07 1997-11-07 Separation membrane evaluation device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP09322198A JP3080051B2 (en) 1997-11-07 1997-11-07 Separation membrane evaluation device

Publications (2)

Publication Number Publication Date
JPH11137973A true JPH11137973A (en) 1999-05-25
JP3080051B2 JP3080051B2 (en) 2000-08-21

Family

ID=18141054

Family Applications (1)

Application Number Title Priority Date Filing Date
JP09322198A Expired - Fee Related JP3080051B2 (en) 1997-11-07 1997-11-07 Separation membrane evaluation device

Country Status (1)

Country Link
JP (1) JP3080051B2 (en)

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Publication number Priority date Publication date Assignee Title
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WO2015142011A1 (en) * 2014-03-17 2015-09-24 한국기계연구원 Cross-flow membrane test cell and membrane test apparatus having same
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Cited By (6)

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Publication number Priority date Publication date Assignee Title
JP2015120111A (en) * 2013-12-24 2015-07-02 日立造船株式会社 Porous film evaluation device and porous film evaluation method
WO2015142011A1 (en) * 2014-03-17 2015-09-24 한국기계연구원 Cross-flow membrane test cell and membrane test apparatus having same
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