JPH1012377A - アクティブマトリックス型有機el表示体の製造方法 - Google Patents
アクティブマトリックス型有機el表示体の製造方法Info
- Publication number
- JPH1012377A JPH1012377A JP8158671A JP15867196A JPH1012377A JP H1012377 A JPH1012377 A JP H1012377A JP 8158671 A JP8158671 A JP 8158671A JP 15867196 A JP15867196 A JP 15867196A JP H1012377 A JPH1012377 A JP H1012377A
- Authority
- JP
- Japan
- Prior art keywords
- light emitting
- organic light
- emitting layer
- organic
- thin film
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000011159 matrix material Substances 0.000 title claims abstract description 14
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 12
- 239000010409 thin film Substances 0.000 claims abstract description 22
- 239000011521 glass Substances 0.000 claims abstract description 13
- 238000002347 injection Methods 0.000 claims abstract description 13
- 239000007924 injection Substances 0.000 claims abstract description 13
- 238000000034 method Methods 0.000 claims description 19
- 239000000758 substrate Substances 0.000 claims description 13
- 230000015572 biosynthetic process Effects 0.000 claims description 5
- 239000000463 material Substances 0.000 abstract description 26
- -1 polyphenylene vinylene Polymers 0.000 abstract description 11
- 229920000553 poly(phenylenevinylene) Polymers 0.000 abstract description 7
- 239000002243 precursor Substances 0.000 abstract description 6
- 238000010438 heat treatment Methods 0.000 abstract description 3
- 238000001704 evaporation Methods 0.000 abstract description 2
- 230000008020 evaporation Effects 0.000 abstract 1
- 125000000843 phenylene group Chemical group C1(=C(C=CC=C1)*)* 0.000 abstract 1
- 238000006116 polymerization reaction Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
- 238000000059 patterning Methods 0.000 description 6
- 239000000975 dye Substances 0.000 description 3
- 229920000642 polymer Polymers 0.000 description 3
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 125000005678 ethenylene group Chemical group [H]C([*:1])=C([H])[*:2] 0.000 description 2
- 238000007641 inkjet printing Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000007740 vapor deposition Methods 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- RETDKIXQRINZEF-UHFFFAOYSA-N 1,3-benzoxazole;zinc Chemical compound [Zn].C1=CC=C2OC=NC2=C1 RETDKIXQRINZEF-UHFFFAOYSA-N 0.000 description 1
- 229910017073 AlLi Inorganic materials 0.000 description 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
- 229910052693 Europium Inorganic materials 0.000 description 1
- 229920000265 Polyparaphenylene Polymers 0.000 description 1
- NRCMAYZCPIVABH-UHFFFAOYSA-N Quinacridone Chemical class N1C2=CC=CC=C2C(=O)C2=C1C=C1C(=O)C3=CC=CC=C3NC1=C2 NRCMAYZCPIVABH-UHFFFAOYSA-N 0.000 description 1
- DGEZNRSVGBDHLK-UHFFFAOYSA-N [1,10]phenanthroline Chemical compound C1=CN=C2C3=NC=CC=C3C=CC2=C1 DGEZNRSVGBDHLK-UHFFFAOYSA-N 0.000 description 1
- 150000004984 aromatic diamines Chemical class 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- CHZWRIFDYXSVOD-UHFFFAOYSA-M chromenylium;perchlorate Chemical compound [O-]Cl(=O)(=O)=O.[O+]1=CC=CC2=CC=CC=C21 CHZWRIFDYXSVOD-UHFFFAOYSA-M 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 150000004696 coordination complex Chemical class 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000000539 dimer Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000007772 electrode material Substances 0.000 description 1
- OGPBJKLSAFTDLK-UHFFFAOYSA-N europium atom Chemical compound [Eu] OGPBJKLSAFTDLK-UHFFFAOYSA-N 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- AHLBNYSZXLDEJQ-FWEHEUNISA-N orlistat Chemical compound CCCCCCCCCCC[C@H](OC(=O)[C@H](CC(C)C)NC=O)C[C@@H]1OC(=O)[C@H]1CCCCCC AHLBNYSZXLDEJQ-FWEHEUNISA-N 0.000 description 1
- 238000000206 photolithography Methods 0.000 description 1
- 150000004032 porphyrins Chemical class 0.000 description 1
- 150000003219 pyrazolines Chemical class 0.000 description 1
- LISFMEBWQUVKPJ-UHFFFAOYSA-N quinolin-2-ol Chemical compound C1=CC=C2NC(=O)C=CC2=C1 LISFMEBWQUVKPJ-UHFFFAOYSA-N 0.000 description 1
- YYMBJDOZVAITBP-UHFFFAOYSA-N rubrene Chemical class C1=CC=CC=C1C(C1=C(C=2C=CC=CC=2)C2=CC=CC=C2C(C=2C=CC=CC=2)=C11)=C(C=CC=C2)C2=C1C1=CC=CC=C1 YYMBJDOZVAITBP-UHFFFAOYSA-N 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- JFLKFZNIIQFQBS-FNCQTZNRSA-N trans,trans-1,4-Diphenyl-1,3-butadiene Chemical class C=1C=CC=CC=1\C=C\C=C\C1=CC=CC=C1 JFLKFZNIIQFQBS-FNCQTZNRSA-N 0.000 description 1
- 150000003852 triazoles Chemical class 0.000 description 1
- 125000006617 triphenylamine group Chemical group 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K59/00—Integrated devices, or assemblies of multiple devices, comprising at least one organic light-emitting element covered by group H10K50/00
- H10K59/30—Devices specially adapted for multicolour light emission
- H10K59/35—Devices specially adapted for multicolour light emission comprising red-green-blue [RGB] subpixels
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K50/00—Organic light-emitting devices
- H10K50/10—OLEDs or polymer light-emitting diodes [PLED]
- H10K50/17—Carrier injection layers
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K85/00—Organic materials used in the body or electrodes of devices covered by this subclass
- H10K85/10—Organic polymers or oligomers
- H10K85/111—Organic polymers or oligomers comprising aromatic, heteroaromatic, or aryl chains, e.g. polyaniline, polyphenylene or polyphenylene vinylene
- H10K85/114—Poly-phenylenevinylene; Derivatives thereof
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K2102/00—Constructional details relating to the organic devices covered by this subclass
- H10K2102/301—Details of OLEDs
- H10K2102/302—Details of OLEDs of OLED structures
- H10K2102/3023—Direction of light emission
- H10K2102/3026—Top emission
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K59/00—Integrated devices, or assemblies of multiple devices, comprising at least one organic light-emitting element covered by group H10K50/00
- H10K59/10—OLED displays
- H10K59/12—Active-matrix OLED [AMOLED] displays
- H10K59/123—Connection of the pixel electrodes to the thin film transistors [TFT]
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K71/00—Manufacture or treatment specially adapted for the organic devices covered by this subclass
- H10K71/10—Deposition of organic active material
- H10K71/12—Deposition of organic active material using liquid deposition, e.g. spin coating
- H10K71/13—Deposition of organic active material using liquid deposition, e.g. spin coating using printing techniques, e.g. ink-jet printing or screen printing
- H10K71/135—Deposition of organic active material using liquid deposition, e.g. spin coating using printing techniques, e.g. ink-jet printing or screen printing using ink-jet printing
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K71/00—Manufacture or treatment specially adapted for the organic devices covered by this subclass
- H10K71/40—Thermal treatment, e.g. annealing in the presence of a solvent vapour
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Ink Jet (AREA)
- Electroluminescent Light Sources (AREA)
Abstract
機EL材料をインクジェット方式により形成および配列
することで、赤、緑、青の発光色を備える有機発光層を
画素毎に任意にパターニングすることが可能となった。
これにより、フルカラー表示のアクティブマトリックス
型有機EL表示体を実現した。 【効果】安価で大画面のフルカラー表示体が製造可能と
なり、効果は大である。
Description
を用いたアクティブマトリックス型のEL表示体のイン
クジェット方式を用いた製造方法に関する。
む薄膜を、陰極と陽極とで挟んだ構成を有し、前記薄膜
に電子および正孔(ホール)を注入して再結合させるこ
とにより励起子(エキシトン)を生成させ、このエキシ
トンが失活する際の光の放出(蛍光・燐光)を利用して
発光させる素子である。
低電圧で100〜100000 cd/m2 程度の高輝度の
面発光が可能であり、また蛍光物質の種類を選択するこ
とにより青色から赤色までの発光が可能なことである。
表示素子を実現するものとして注目を集めている(電子
情報通信学会技術報告、第89巻、NO.106、49
ページ、1989年)。報告によると、強い蛍光を発す
る有機色素を発光層に使用し、青、緑、赤色の明るい発
光を得ている。これは、薄膜状で強い蛍光を発し、ピン
ホール欠陥の少ない有機色素を用いたことで、高輝度な
フルカラー表示を実現できたと考えられている。
機発光層の成分が有機電荷材料と有機発光材料の混合物
からなる薄膜層を設け、濃度消光を防止して発光材料の
選択幅を広げ、高輝度なフルカラー素子とする旨が提案
されている。
ラー表示パネルの構成や製造方法については言及されて
いない。
た有機薄膜EL素子は、青、緑、赤の発光を示す。しか
し、よく知られているように、フルカラー表示体を実現
するためには、3原色を発光する有機発光層を画素毎に
配置する必要がある。従来、有機発光層をパターニング
する技術は非常に困難とされていた。原因は、一つは反
射電極材の金属表面が不安定であり、蒸着のパターニン
グ精度が出ないという点である。2つめは、正孔注入層
および有機発光層を形成するポリマーや前駆体がフォト
リソグラフィー等のパターニング工程に対して耐性が無
いという点である。
ものであり、その目的は、有機発光層をインクジェット
方式により画素毎にパターニングしたアクティブマトリ
ックス型EL表示体の製造方法を提供することにある。
ブマトリックス型有機EL表示体の製造方法は、薄膜ト
ランジスタを有するガラス基板に形成された透明画素電
極上層に正孔注入層が形成され、この上層に少なくとも
各画素毎に赤、緑、青より選択された発光色を有する有
機発光層が形成され、更にこの上層に反射電極が形成さ
れるアクティブマトリックス型有機EL表示体の製造方
法において、前記有機発光層の形成および配列がインク
ジェット方式によりなされることを特徴とし、また、薄
膜トランジスタを有するガラス基板に形成された透明画
素電極上層に少なくとも各画素毎に赤、緑、青より選択
された発光色を有する有機発光層が形成され、更にこの
上層に反射電極が形成されるアクティブマトリックス型
有機EL表示体の製造方法において、前記有機発光層の
形成および配列がインクジェット方式によりなされるこ
とを特徴とする。
板に形成された反射画素電極上層に少なくとも各画素毎
に赤、緑、青より選択された発光色を有する有機発光層
が形成され、この上層に正孔注入層が形成され、更にこ
の上層に透明電極が形成されるアクティブマトリックス
型有機EL表示体の製造方法において、前記有機発光層
の形成および配列がインクジェット方式によりなされる
ことを特徴とし、また、薄膜トランジスタを有するガラ
ス基板に形成された反射画素電極上層に少なくとも各画
素毎に赤、緑、青より選択された発光色を有する有機発
光層が形成され、更にこの上層に透明電極が形成される
アクティブマトリックス型有機EL表示体の製造方法に
おいて、前記有機発光層の形成および配列がインクジェ
ット方式によりなされることを特徴とする。
板上に形成された信号線301、ゲート線302、画素
電極303および薄膜トランジスタ304上に、インク
ジェット法により、赤、緑、青色の有機発光材料をパタ
ーニング塗布することで、フルカラー表示を実現するも
のである。
ついて図面を参照して説明する。
板101上に薄膜トランジスタ102を形成してから、
ITO透明画素電極103を形成する。
ポリテトラヒドロチオフェニルフェニレンをコーティン
グする。加熱により、前駆体はポリフェニレンビニレン
となり、厚さ0.05ミクロンの正孔注入層104が形
成される。
により赤、緑、青色を発色する発光材料をパターニング
塗布し、厚さ0.05ミクロンの発色層106、10
7、108を形成する。赤色発光材料にはシアノポリフ
ェニレンビニレン、緑色発光材料にはポリフェニレンビ
ニレン、青色発光材料にはポリフェニレンビニレンおよ
びポリアルキルフェニレンを使用する。これらの有機E
L材料はケンブリッジ・ディスプレイ・テクノロジー社
製であり、液状で入手可能である。
gAg反射電極109を蒸着法により形成する。
表示体が完成する。
板201上に薄膜トランジスタ202を形成してから、
AlLi反射画素電極203を形成する。
により赤、緑、青色を発色する発光材料をパターニング
塗布し、発色層204、205、206を形成する。赤
色発光材料にはシアノポリフェニレンビニレン、緑色発
光材料にはポリフェニレンビニレン、青色発光材料には
ポリフェニレンビニレンおよびポリアルキルフェニレン
を使用する。これらの有機EL材料はケンブリッジ・デ
ィスプレイ・テクノロジー社製であり、液状で入手可能
である。
ポリテトラヒドロチオフェニルフェニレンをキャスト法
により形成する。加熱により、前駆体はポリフェニレン
ビニレンとなり、正孔注入層208が形成される。
より形成する。
表示体が完成する。
して2,3,6,7-テトラヒドロ-11-オキソ−1H,5H,11H-(1)
ベンゾピラノ[6,7,8-ij]-キノリジン-10-カルボン酸を
用い、有機正孔注入層材料として1,1-ビス-(4-N,N-ジト
リルアミノフェニル)シクロヘキサンを用い、両者を混
合することで緑色の発光材料とする。
3',4'-ジヒドロキシフェニル)-3,5,7-トリヒドロキシ-1
-ベンゾピリリウムパークロレートを用いて正孔注入層
材料と混合する。
してトリス(8-ヒドロキシキノリノール)アルミニウムを
用い、有機発光材料として、2,3,6,7-テトラヒドロ-9-
メチル-11-オキソ-1H,5H,11H-(1)ベンゾピラノ[6,7,8-i
j]-キノリジンを混合し、発光材料を作成する。
各々の発光層をインクジェットプリンタ装置により局所
パターニングし、アクティブマトリックス型有機EL表
示体を作成する。
外にも、アロマティックジアミン誘導体(TDP)、オ
キシジアゾールダイマー(OXD)、オキシジアゾール
誘導体(PBD)、ジスチルアリーレン誘導体(DS
A)、キノリノール系金属錯体、ベリリウム−ベンゾキ
ノリノール錯体(Bebq)、トリフェニルアミン誘導
体(MTDATA)、ジスチリル誘導体、ピラゾリンダ
イマー、ルブレン、キナクリドン、トリアゾール誘導
体、ポリフェニレン、ポリアルキルフルオレン、ポリア
ルキルチオフェン、アゾメチン亜鉛錯体、ポリフィリン
亜鉛錯体、ベンゾオキサゾール亜鉛錯体、フェナントロ
リンユウロピウム錯体が使用できるが、これに限られる
物ではない。
有機EL材料をインクジェット方式により形成および配
列することでパターニングが可能となり、フルカラー表
示のアクティブマトリックス型有機EL表示体を実現し
た。これにより、安価で大画面のフルカラー表示体が製
造可能となり、効果は大である。
トリックス型有機EL表示体の工程を示す図である。
トリックス型有機EL表示体の工程を示す図である。
法により形成された発色層を示す図である。
Claims (4)
- 【請求項1】 薄膜トランジスタを有するガラス基板に
形成された透明画素電極上層に正孔注入層が形成され、
この上層に少なくとも各画素毎に赤、緑、青より選択さ
れた発光色を有する有機発光層が形成され、更にこの上
層に反射電極が形成されるアクティブマトリックス型有
機EL表示体の製造方法において、前記有機発光層の形
成および配列がインクジェット方式によりなされること
を特徴とするアクティブマトリックス型有機EL表示体
の製造方法。 - 【請求項2】 薄膜トランジスタを有するガラス基板に
形成された透明画素電極上層に少なくとも各画素毎に
赤、緑、青より選択された発光色を有する有機発光層が
形成され、更にこの上層に反射電極が形成されるアクテ
ィブマトリックス型有機EL表示体の製造方法におい
て、前記有機発光層の形成および配列がインクジェット
方式によりなされることを特徴とするアクティブマトリ
ックス型有機EL表示体の製造方法。 - 【請求項3】 薄膜トランジスタを有するガラス基板に
形成された反射画素電極上層に少なくとも各画素毎に
赤、緑、青より選択された発光色を有する有機発光層が
形成され、この上層に正孔注入層が形成され、更にこの
上層に透明電極が形成されるアクティブマトリックス型
有機EL表示体の製造方法において、前記有機発光層の
形成および配列がインクジェット方式によりなされるこ
とを特徴とするアクティブマトリックス型有機EL表示
体の製造方法。 - 【請求項4】 薄膜トランジスタを有するガラス基板に
形成された反射画素電極上層に少なくとも各画素毎に
赤、緑、青より選択された発光色を有する有機発光層が
形成され、更にこの上層に透明電極が形成されるアクテ
ィブマトリックス型有機EL表示体の製造方法におい
て、前記有機発光層の形成および配列がインクジェット
方式によりなされることを特徴とするアクティブマトリ
ックス型有機EL表示体の製造方法。
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP8158671A JP3036436B2 (ja) | 1996-06-19 | 1996-06-19 | アクティブマトリックス型有機el表示体の製造方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP8158671A JP3036436B2 (ja) | 1996-06-19 | 1996-06-19 | アクティブマトリックス型有機el表示体の製造方法 |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP11323845A Division JP2000123975A (ja) | 1999-11-15 | 1999-11-15 | アクティブマトリックス型有機el表示体 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH1012377A true JPH1012377A (ja) | 1998-01-16 |
JP3036436B2 JP3036436B2 (ja) | 2000-04-24 |
Family
ID=15676827
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP8158671A Expired - Lifetime JP3036436B2 (ja) | 1996-06-19 | 1996-06-19 | アクティブマトリックス型有機el表示体の製造方法 |
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