JPH0394897A - Initial operating method for anaerobic treatment device - Google Patents

Initial operating method for anaerobic treatment device

Info

Publication number
JPH0394897A
JPH0394897A JP1228268A JP22826889A JPH0394897A JP H0394897 A JPH0394897 A JP H0394897A JP 1228268 A JP1228268 A JP 1228268A JP 22826889 A JP22826889 A JP 22826889A JP H0394897 A JPH0394897 A JP H0394897A
Authority
JP
Japan
Prior art keywords
sludge
anaerobic treatment
treatment device
anaerobic
seeding
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP1228268A
Other languages
Japanese (ja)
Inventor
Haruki Akega
明賀 春樹
Hironori Niwa
博則 丹羽
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Organo Corp
Original Assignee
Organo Corp
Japan Organo Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Organo Corp, Japan Organo Co Ltd filed Critical Organo Corp
Priority to JP1228268A priority Critical patent/JPH0394897A/en
Publication of JPH0394897A publication Critical patent/JPH0394897A/en
Pending legal-status Critical Current

Links

Classifications

    • Y02W10/12

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  • Purification Treatments By Anaerobic Or Anaerobic And Aerobic Bacteria Or Animals (AREA)

Abstract

PURPOSE:To obtain an initial operating method for an anaerobic treatment device which can start the device at a lower cost by using an excess sludge which is produced in the other anaerobic treatment device already under working and is subjected to a dehydration treatment as the sludge for seeding. CONSTITUTION:The excess sludge which is produced in the other anaerobic treatment device already under working and is subjected to the dehydration treatment is used as the sludge for seeding in the method for obtaining the sludge for seeding from the outside and starting the operation by charging this sludge into the anaerobic treatment device at the time of starting the operation of the anaerobic treatment device which treats waste water contg. org. matter by an anaerobic fermentation method. Since the starting of the anaerobic treatment device is executed by using the sludge which is subjected to the dehydration treatment and is thereby reduced in volume and, therefore, the amt. of the sludge for seeding to be obtd. from the outside at the time of starting the operation is drastically decreased as compared to heretofore.

Description

【発明の詳細な説明】 《産業上の利用分野〉 本発明はし尿、下水、各種産業廃水等の有機物を含む廃
水を、嫌気性発酵法によって処理する際の装置の初期運
転方法、すなわち立ち上げ方法に関するものである. く従来の技術冫 嫌気性発酵法による廃水処理は、処理装0内に存在する
嫌気性微生物の働きによって廃水中の有機物をメタンガ
スと炭酸ガスに分解して処理する技術であり、活性汚泥
法のように空気で曝気して酸素を供給する必要がないこ
とから運転経費が安く、また発虫するメタンガスをエネ
ルギー源として利用できる等の利点を有し、現在、し尿
処理場、下水処理場、および各種産業廃水処理装置等で
実用化されている. ところで、上述のような働きをする嫌気性微生物は、活
性汚泥のような好気性微生物に比べてその増殖速度が非
常に遅いため、たとえば嫌気性処理装置を新たに設置し
たような場合の運転開始、いわゆる装置の立ち上げに際
しては、処理すべき廃水に適した嫌気性微生物を所定の
量まで、かつ速やかに馴養すべく、外部より植種用の汚
泥を入手してこれを新設の装置内に投入し、しかる後に
当該装置の立ち上げを行うようにしている。
[Detailed Description of the Invention] <Industrial Application Field> The present invention relates to an initial operation method, that is, startup, of an apparatus for treating wastewater containing organic matter such as human waste, sewage, and various industrial wastewater by an anaerobic fermentation method. It concerns the method. Conventional technology Wastewater treatment using anaerobic fermentation is a technology that decomposes organic matter in wastewater into methane gas and carbon dioxide gas by the action of anaerobic microorganisms present in the treatment equipment.Activated sludge method As there is no need to aerate with air to supply oxygen, operating costs are low, and the methane gas generated by insects can be used as an energy source. It has been put into practical use in various industrial wastewater treatment equipment. By the way, the anaerobic microorganisms that work as described above have a much slower growth rate than aerobic microorganisms such as activated sludge, so for example, when starting up a newly installed anaerobic treatment device, When starting up the equipment, in order to quickly incubate the wastewater with anaerobic microorganisms suitable for the wastewater to a predetermined amount, it is necessary to obtain sludge for seeding from outside and introduce it into the newly installed equipment. After that, the device is started up.

そして、前記植種用汚泥としては、通常、既に稼動して
いる他の嫌気性処理装置にて嫌気性微生物の増薙によっ
て発生した、汚泥濃度2〜4%程度のスラリー状の余剰
汚泥が使用されていた。
The sludge for seeding is usually surplus sludge in the form of slurry with a sludge concentration of about 2 to 4%, which is generated by the growth of anaerobic microorganisms in other anaerobic treatment equipment that is already in operation. It had been.

すなわち、稼動巾の他の嫌気性処理装置から発生した余
剰汚泥を、これから運転を開始しようとする嫌気性処理
装置の設置場所までスラリー状のまま輸送し、当該汚泥
を装置内に投入して立ち上げを行っていたのである。
In other words, surplus sludge generated from other anaerobic treatment equipment within the operating range is transported in the form of a slurry to the installation site of the anaerobic treatment equipment that is about to start operation, and the sludge is put into the equipment and placed in a standing position. They were raising their prices.

く発明が解決しようεする問題点〉 しかしながら、上述のような従来の立ち上げ方法では、
植種用汚泥こしてスラリー状のまま輸送された余剰汚泥
を使用するので、以下に述べるような問題点がある。
However, in the conventional startup method as described above,
Since surplus sludge that has been strained and transported as a slurry for planting is used, there are problems as described below.

すなわち、嫌気性処理装置の立ち上げに際しては、たと
えば汚泥濃度2〜4%のスラリー状余剰汚泥を、通常当
該装置容量の174〜3/4程度投入しなければならな
いが、嫌気性処理装置の容量は一般的に数百〜数千一、
あるいはそれ以上の規模である場合が多い。従って、嫌
気性処理装置の立ち上げに際して輸送すべき余剰汚泥の
容量は極めて大景乙なり、かつスラリー状で輸送するた
めにタンクローリー等の特殊な輸送手段が必要であるこ
とから、当該余剰汚泥の輸送費は極めて莫大なものとな
り、この点が嫌気性処理装置を立ち上げる際の経費増大
の大きな要因となっていた。
In other words, when starting up an anaerobic treatment device, for example, surplus sludge in the form of slurry with a sludge concentration of 2 to 4% must be input, usually about 174 to 3/4 of the capacity of the device, but the capacity of the anaerobic treatment device is generally several hundred to several thousand one,
Or, in many cases, even larger. Therefore, the volume of surplus sludge that must be transported when starting up an anaerobic treatment facility is extremely large, and special transport means such as tank trucks are required to transport it in slurry form. The transportation costs were extremely high, and this point was a major factor in the increase in costs when setting up an anaerobic treatment facility.

本発明は上述の問題点を解決し、少ない経費で装置の立
ち上げを行うことができる、嫌気性処理装置の初期運転
方法を提供することを目的とするものである。
SUMMARY OF THE INVENTION An object of the present invention is to provide an initial operation method for an anaerobic treatment device that solves the above-mentioned problems and allows startup of the device at low cost.

く問題点を解決するための千段) かかる目的を達戒するためになされた本発明は、有機物
を含む廃水を嫌気性発酵法によって処理する嫌気性処理
装蓋の運転開始に際して、外部より植種用の汚泥を入手
し、当該汚泥を前記嫌気性処理装置に投入して運転を開
始する方法において、前記植種用汚泥として、既に稼動
中の他の嫌気性処理装置の余剰汚泥であって、か・つ脱
水処理されたものを使用することを特徴とする嫌気性処
理装置の初期運転方法である。
The present invention, which has been made to achieve the above object, is designed to provide an environment in which plants are removed from the outside at the start of operation of an anaerobic treatment unit that processes wastewater containing organic matter by an anaerobic fermentation method. In the method of obtaining sludge for seeding and introducing the sludge into the anaerobic treatment device to start operation, the sludge for seeding is surplus sludge from another anaerobic treatment device already in operation. This is an initial operating method for an anaerobic treatment equipment, characterized in that it uses anaerobic treatment equipment that has been dehydrated.

以下に本発明を詳細に説明する。The present invention will be explained in detail below.

嫌気性処理装置から発生するスラリー状の余剰汚泥は、
通常各種の脱水機によって脱水処理され、輸送の容易な
、かつ減容化された形態の脱水なーキとされた後に廃棄
処分される。
Slurry-like surplus sludge generated from anaerobic treatment equipment is
Usually, it is dehydrated using various types of dehydrators, and then it is disposed of after it is made into a dehydrated nake that is easy to transport and has a reduced volume.

従って、当該脱水ケーキを、これから運転を開始しよう
とする嫌気性処理装置の植種用汚泥として使用すること
ができれば、汚泥輸送に係わる前述のような問題点を解
決することができる。
Therefore, if the dehydrated cake can be used as sludge for seeding in an anaerobic treatment device that is about to start operation, the above-mentioned problems related to sludge transportation can be solved.

しかしながら、従来は前記余剰汚泥を構威している、メ
タン菌に代表される嫌気性菌の酸素に対する耐性が極め
て弱いとされており、従って脱水処理がなされ、大気中
に暴露された状態に蓋かれた脱水ケーキは、当該脱水な
ーキ中に存在する嫌気性菌が死滅したり、あるいはその
活性が著しく低下したりしているために、植種用汚泥と
して不適であると考えられていた.事実、今日に至るま
で脱水ケー牛を植種用汚泥として使用したという事例は
拷無であり、前述のごεく従来は余剰汚泥をスラリー状
のまま、たとえばタンクローリーに入れて密閉状態を保
持して輸送し、これを植種用の汚泥として使用していた
のである。
However, conventionally, the anaerobic bacteria such as methane bacteria that make up the excess sludge are said to have extremely low resistance to oxygen, so dehydration treatment is performed and the sludge is capped when exposed to the atmosphere. The dehydrated cake was thought to be unsuitable as sludge for seed planting because the anaerobic bacteria present in the dehydrated cake have died or their activity has significantly decreased. In fact, to this day, there have been no cases of using dehydrated sludge as seed sludge, and as mentioned above, in the past, surplus sludge was placed in a slurry form, for example, in a tank truck and kept in an airtight state. This was used as sludge for planting seeds.

しかしながら、本発明者等の研究結果によれば、余剰汚
泥中に存在するメタン菌の中にも、たとえば当該余剰汚
泥中に比較的多量に存在するメタノスリンクス(Met
har+othriX)属に属するメタン菌のように、
酸素に対する耐性の非常に強いものが存在し、たとえ曝
気等の操作を施しても死滅しない菌が存在することが明
らかとなった。
However, according to the research results of the present inventors, among the methane bacteria present in surplus sludge, for example, methanoshrynx (Methanoshrynx), which is present in a relatively large amount in the surplus sludge,
Like methane bacteria belonging to the genus har + othriX),
It has become clear that there are bacteria that are extremely resistant to oxygen and cannot be killed even by aeration and other operations.

このような知見のもとに、本発明者等は脱水処理された
余剰汚泥を嫌気性処理の植種用汚泥として使用すること
を試みたところ、後述の実施例に示すごとく、スラリー
状の余剰汚泥を使用した場合とほとんど変わりなく、極
めて順調に嫌気性微生物の馴養を行うことができた。
Based on this knowledge, the present inventors attempted to use dehydrated surplus sludge as sludge for seeding in anaerobic treatment, and as shown in the examples below, the surplus sludge in the form of a slurry was obtained. Anaerobic microorganisms were able to acclimatize very smoothly, almost the same as when using sludge.

本発明でいう脱水処理された余剰汚泥とは、たεえばし
尿、下水処理場の嫌気性消化槽から発生ずるスラリー状
の余剰汚泥や、各種産業廃水の処理に使用されている嫌
気性処理装置から発生するスラリー状の余剰汚泥を、何
らかの手段によって脱水処理したものを意味し、前記脱
水手段の例としては、遠心分離機、真空脱水機、濾布走
行型脱水機、あるいはフィルタープレス等の公知の脱水
手段を挙げるこεができる。
In the present invention, dewatered surplus sludge refers to, for example, human waste, slurry-like surplus sludge generated from anaerobic digestion tanks in sewage treatment plants, and anaerobic treatment equipment used to treat various industrial wastewater. This refers to surplus sludge in the form of slurry generated from sludge that has been dehydrated by some means, and examples of the dehydration means include a centrifugal separator, a vacuum dehydrator, a filter cloth running type dehydrator, or a filter press. Dehydration means can be listed here.

また、上記脱水汚泥は脱水処理の過程において凝集剤等
の薬品を何ら添加されていない、いわゆる無薬注脱水汚
泥が最も好ましいが、薬品を添加して脱水した汚泥を用
いる場合は、石灰や塩化第二鉄等の無機系凝集剤を添加
したものよりも、有機系の、いわゆる高分子凝集剤を添
加したものω方が、嫌気性菌の死滅や活性低下の問題が
より少ないという点で好ましい。
In addition, the most preferable dehydrated sludge is so-called chemical-free dehydrated sludge, in which no chemicals such as flocculants are added during the dewatering process. Rather than those containing inorganic flocculants such as ferric iron, organic flocculants containing so-called polymer flocculants are preferable because they cause fewer problems of killing anaerobic bacteria and decreasing activity. .

なお、脱水汚泥を、これから運転を開始しようとする嫌
気性処理装置内に投入するに際しては、当該汚泥を直接
投入しても差し支えないが、通常は当該脱水汚泥に水や
被処理水を加えて再びスラリー状に戻し、しかる後に投
入するのがよい。
When introducing dehydrated sludge into the anaerobic treatment equipment that is about to start operation, it is okay to directly introduce the sludge, but usually water or water to be treated is added to the dehydrated sludge. It is best to reconstitute it into a slurry and then add it.

本発明方法は浮遊式、固定床式、流動床弐、あるいは上
昇流スラッジブランケット式(一般にUASB法と呼ば
れる)等あらゆる方式の嫌気性処理装遣に適用ずること
ができるが、特に固定床式、流動床式、および上昇流ス
ラフジブランケット式の嫌気性処理装置に好適である.
その理由は、これらの装置においては前述した酸素に対
する酎牲が強いMe thano tlxr ix属に
属するメタン菌が優先種となって廃水中の有機物の分解
がなされるからである。
The method of the present invention can be applied to all types of anaerobic treatment equipment such as floating type, fixed bed type, fluidized bed type, and upflow sludge blanket type (generally called UASB method), but in particular fixed bed type, Suitable for fluidized bed type and upflow sludge blanket type anaerobic treatment equipment.
The reason for this is that in these devices, the above-mentioned methane bacteria belonging to the genus Methano tlxrix, which are highly addictive to oxygen, become the priority species and decompose the organic matter in the wastewater.

(実施例〉 以下に本発明の実施例を説明する。(Example> Examples of the present invention will be described below.

容量3lの上昇流スラソジブランケット式嫌気性処理装
置を用いて、以下のような立ち挙げ実験を行った。
The following start-up experiment was conducted using an upflow sludge blanket type anaerobic treatment device with a capacity of 3 liters.

すなわち、某下水処理場から入手した嫌気性消化槽の余
剰汚泥の脱水ケーキ(固形分濃度23%、含水率77%
)を大気中に24時間放置後植種用汚泥として使用し、
当該脱水ケーキの200gを1lの水道水を入れた容器
中に投入、攪拌してスラリー状の汚泥となし、当該スラ
リー状汚泥を一夜放置した後に前記嫌気性処理装置内に
投入した。
In other words, a dehydrated cake of excess sludge from an anaerobic digestion tank obtained from a certain sewage treatment plant (solid content 23%, moisture content 77%)
) was left in the atmosphere for 24 hours and then used as sludge for seeding.
200 g of the dehydrated cake was put into a container containing 1 liter of tap water and stirred to form a slurry-like sludge. The slurry-like sludge was left overnight and then put into the anaerobic treatment apparatus.

次いで、当該嫌気性処理装置向に、グルコース3,00
0g/Il、グルタaン酸ナトリウムl,000■/l
,NHaC 1 1 0 0■N/6、K H 2P 
0 ,30■P/6、および酵母エキス100■/lを
含む合戒廃水を流入させ、反応温度を36℃に保ちなが
ら当該装置の運転を開始した。
Next, 3,00 g of glucose was added to the anaerobic treatment device.
0g/Il, sodium glutamate l,000■/l
, NHaC 1 1 0 0 ■N/6, K H 2P
0.0, 30 μP/6 and yeast extract 100 μ/l were introduced into the reactor, and operation of the apparatus was started while maintaining the reaction temperature at 36°C.

運転当初は容積負荷O.5kg”COD〜/ポ/Bの低
負荷で運転を行い、処理が良好であることを確認しなが
ら徐々に容積負荷を上げていったところ、65日経過後
には目標負荷である10kg−CODc,/n{/日に
到達した。
At the beginning of operation, the volumetric load is O. We operated at a low load of 5kg-COD~/Po/B, and gradually increased the volumetric load while confirming that the treatment was good. After 65 days, the target load was 10kg-CODc, Reached /n{/ day.

比較のため、植種用汚泥として前記実施例の場合と同じ
下水処理場の脱水前のスラリー状余剰汚泥(固形分濃度
260%)であって、密閉状態を保持して移送したもの
を使用し、当該汚泥の2.37!を実施例に用いたと同
じ容量の上昇流スラフジブランケンE式嫌気性処理装置
内に投入(装置内の固形分量は実施例の場合と同じとな
る)して実施例と同じ条件で立ち上げ実験を行ったとこ
ろ、530経過後に目標負荷である1 0kg−COD
,,/ボ/日に到達した。
For comparison, surplus slurry sludge (solid content concentration 260%) from the same sewage treatment plant as in the previous example was used as the seeding sludge, and was transported while being kept in a sealed state. , 2.37 of the sludge! was put into an upflow slough diblanken E-type anaerobic treatment device with the same capacity as used in the example (the amount of solids in the device is the same as in the example), and a start-up experiment was conducted under the same conditions as in the example. When 530 minutes passed, the target load of 10kg-COD was reached.
,, reached /bo/day.

以上の結果から明らかなように、植種用汚泥として脱水
ケーキを用いた場合も、スラリー状の余剰汚泥を用いる
従来法とほぼ同様に順調に嫌気性処理装置の立ち上げを
行うことができた。
As is clear from the above results, even when dehydrated cake was used as the seeding sludge, the anaerobic treatment equipment could be started up as smoothly as in the conventional method using surplus sludge in the form of slurry. .

く効果〉 以上詳述したごとく、本発明方法によれば脱水処理され
て滅容化された汚泥を用いて、スラリー状汚泥を用いる
従来法と同様に順調に嫌気性処理装置の立ち上げを行う
ことができるので、運転開始に際して外部より入手すべ
き植種用汚泥の量を従来に比べて著しく少なくすること
ができる。
Effect> As detailed above, according to the method of the present invention, using sludge that has been dehydrated and sterilized, the anaerobic treatment equipment can be started up smoothly in the same way as the conventional method using slurry sludge. Therefore, the amount of seeding sludge that must be obtained from outside at the start of operation can be significantly reduced compared to the conventional method.

すなわち、従来は植種用汚泥として固形分濃度2〜4%
程度のスラリー状汚泥を用いていたのに対して、本発明
の場合は固形分濃度がたとえば15〜40%というよう
に極めて高い脱水汚泥を使用するので、入手すべき汚泥
の容量は従来法の約1/5〜1/10程度で済み、従っ
て汚泥の輸送費用も従来の約1/5〜1/10程度に軽
減される。
In other words, conventionally, the solid content concentration of sludge for seeding was 2 to 4%.
In contrast, in the case of the present invention, dewatered sludge with an extremely high solid content concentration of, for example, 15 to 40% is used, so the volume of sludge to be obtained is smaller than that of the conventional method. The cost for transporting sludge is reduced to about 1/5 to 1/10 of the conventional cost.

また、脱水処理された汚泥は、タンクローリー等の費用
の高い輸送手段を用いずとも、費用の安い通常のトラッ
クに直接積載して、あるいは汚泥を簡単なオーブン容器
に入れて水分が外部に葡出しない状態にしてからトラソ
クに積載する等して、要するにEラソク等の通常の輸送
手段を用いて輸送することができるので汚泥輸送に係わ
る費用は更に軽減され、よって本発明の実用的価値は極
めて大である。
In addition, the dehydrated sludge can be loaded directly onto a low-cost regular truck, without using expensive means of transportation such as a tank truck, or the sludge can be placed in a simple oven container and the water is drained outside. The cost of transporting sludge can be further reduced because it can be transported using ordinary means of transportation such as E-rasok by loading it onto a truck after it has been brought into a dry state, and therefore the practical value of the present invention is extremely high. It's large.

Claims (1)

【特許請求の範囲】[Claims] 有機物を含む廃水を嫌気性発酵法によって処理する嫌気
性処理装置の運転開始に際して、外部より植種用の汚泥
を入手し、当該汚泥を前記嫌気性処理装置に投入して運
転を開始する方法において、前記植種用汚泥として、既
に稼動中の他の嫌気性処理装置の余剰汚泥であって、か
つ脱水処理されたものを使用することを特徴とする嫌気
性処理装置の初期運転方法。
In a method of starting operation of an anaerobic treatment device for treating wastewater containing organic matter by an anaerobic fermentation method, obtaining sludge for seeding from outside, and introducing the sludge into the anaerobic treatment device to start operation. . An initial operating method for an anaerobic treatment device, characterized in that the seeding sludge is surplus sludge from another anaerobic treatment device that is already in operation and has been subjected to dewatering treatment.
JP1228268A 1989-09-05 1989-09-05 Initial operating method for anaerobic treatment device Pending JPH0394897A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP1228268A JPH0394897A (en) 1989-09-05 1989-09-05 Initial operating method for anaerobic treatment device

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JP1228268A JPH0394897A (en) 1989-09-05 1989-09-05 Initial operating method for anaerobic treatment device

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JPH0394897A true JPH0394897A (en) 1991-04-19

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009011993A (en) * 2007-07-09 2009-01-22 Takuma Co Ltd Method for starting up anaerobic digestion system
CN102910732A (en) * 2012-11-09 2013-02-06 北京桑德环境工程有限公司 Method for rapidly starting anaerobic reactor by high-concentration organic wastewater
CN104445610A (en) * 2014-12-23 2015-03-25 长春建筑学院 Method for treating lignite upgrading wastewater by anaerobic co-metabolism
JP2015097994A (en) * 2013-11-19 2015-05-28 住友理工株式会社 Method for processing glycol-containing waste water, device for processing glycol-containing waste water, and sludge for use therein

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61125499A (en) * 1984-11-22 1986-06-13 Matsushita Electric Ind Co Ltd Method for supplying methane fermentation microorganism

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61125499A (en) * 1984-11-22 1986-06-13 Matsushita Electric Ind Co Ltd Method for supplying methane fermentation microorganism

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009011993A (en) * 2007-07-09 2009-01-22 Takuma Co Ltd Method for starting up anaerobic digestion system
CN102910732A (en) * 2012-11-09 2013-02-06 北京桑德环境工程有限公司 Method for rapidly starting anaerobic reactor by high-concentration organic wastewater
JP2015097994A (en) * 2013-11-19 2015-05-28 住友理工株式会社 Method for processing glycol-containing waste water, device for processing glycol-containing waste water, and sludge for use therein
CN104445610A (en) * 2014-12-23 2015-03-25 长春建筑学院 Method for treating lignite upgrading wastewater by anaerobic co-metabolism
CN104445610B (en) * 2014-12-23 2016-10-19 长春建筑学院 Anaerobic co-metabolism processes the method for brown coal upgrading waste water

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