JP7464233B2 - Non-aqueous hair oil - Google Patents
Non-aqueous hair oil Download PDFInfo
- Publication number
- JP7464233B2 JP7464233B2 JP2016248054A JP2016248054A JP7464233B2 JP 7464233 B2 JP7464233 B2 JP 7464233B2 JP 2016248054 A JP2016248054 A JP 2016248054A JP 2016248054 A JP2016248054 A JP 2016248054A JP 7464233 B2 JP7464233 B2 JP 7464233B2
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- mass
- oil
- hair
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- 239000003921 oil Substances 0.000 claims description 63
- 229920001296 polysiloxane Polymers 0.000 claims description 36
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 26
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- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims description 24
- 238000006116 polymerization reaction Methods 0.000 claims description 13
- 125000004122 cyclic group Chemical group 0.000 claims description 11
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- 239000010696 ester oil Substances 0.000 claims description 8
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- 125000000217 alkyl group Chemical group 0.000 description 2
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- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
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- 238000000926 separation method Methods 0.000 description 1
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- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 1
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Landscapes
- Cosmetics (AREA)
Description
本発明は、洗い流さない非水系ヘアオイルに関する。 The present invention relates to a non-aqueous hair oil that is not rinsed off.
一般に、損傷を受けた毛髪に対して適用するヘアトリートメント剤が知られている。それらの中で髪に塗布してそのまま乾かして仕上げる洗い流さないタイプのトリートメント剤が知られている。特に損傷が大きい毛髪に対しては、シリコーン誘導体や炭化水素を主成分とするオイルタイプ又はオイルゲルタイプのものが用いられ、損傷した毛髪に対し滑らかな指通り、まとまり感等の適度なセット力を付与している。 Generally, hair treatment agents that are applied to damaged hair are known. Among these, leave-in type treatment agents are known, which are applied to the hair and then left to dry. For hair that is particularly damaged, oil or oil gel types that contain silicone derivatives or hydrocarbons as the main ingredients are used, which give damaged hair a smooth feel and moderate setting power, such as manageability.
例えば、特許文献１は、特定のポリエーテル変性シリコーン等を含有する油中水型の乳化化粧料について開示する。かかる乳化化粧料は、外相が油分であることから、潤い、しっとり感を向上させている。また、特許文献２は、ジメチコノール、アミノ変性シリコーン、環状シリコーン等を含有する非水系毛髪処理剤について開示する。非水系毛髪処理剤は、環状シリコーンにより使用感を向上させている。 For example, Patent Document 1 discloses a water-in-oil type emulsion cosmetic that contains a specific polyether-modified silicone, etc. Such an emulsion cosmetic improves moisturizing and moisturizing feeling because the external phase is oil. Furthermore, Patent Document 2 discloses a non-aqueous hair treatment agent that contains dimethiconol, amino-modified silicone, cyclic silicone, etc. The non-aqueous hair treatment agent improves the feeling of use by using the cyclic silicone.
ところが、それらの処理剤は、使用感、まとまり感等の効果の持続性、及び毛髪の柔らかさの観点においてまだ十分に満足できるものではなかった。
本発明の目的は、洗い流さないタイプの非水系ヘアオイルにおいて、使用感、効果の持続性、及び柔らかさを向上できる非水系ヘアオイルを提供することにある。
However, these treatments have not yet been fully satisfactory in terms of feel upon use, durability of effects such as manageability, and softness of hair.
An object of the present invention is to provide a leave-in type non-aqueous hair oil that can improve the feel during use, the durability of the effect, and the softness of hair.
本発明は、所定量のジメチコン及びジメチコノールとイソドデカンを併用することにより、使用感、効果の持続性、及び柔らかさを向上できることを見出したことに基づくものである。尚、成分の含有量を示す質量％の数値は、有機溶剤等の可溶化剤を使用する場合、それらも含めた剤型中における数値である。 The present invention is based on the discovery that the use of a specified amount of dimethicone and dimethiconol in combination with isododecane can improve usability, duration of effect, and softness. Note that the mass % values indicating the content of the components are values in the formulation including solubilizers such as organic solvents, if any.
上記目的を達成するために、本発明の一態様では、（Ａ）成分として（Ａ１）ジメチコン及び（Ａ２）ジメチコノールを含有し、（Ａ）成分の含有量が６０質量％以上、並びに（Ｂ）イソドデカンを１～４０質量％を含有し、実質的に環状シリコーンを含有しない洗い流さない非水系ヘアオイルを要旨とする。前記（Ａ）成分は、少なくとも（Ａ２－１）高重合ジメチコノールを含み、前記（Ａ）成分の全含有量に対して（Ａ２－１）高重合ジメチコノールが１～３０質量％含有してもよい。更に（Ｃ）アミノ変性シリコーンを含有してもよい。更に（Ｄ）２５℃で液状のジカルボン酸系エステル油を含有してもよい。 In order to achieve the above object, one aspect of the present invention is a leave-on non-aqueous hair oil that contains (A1) dimethicone and (A2) dimethiconol as component (A), contains 60% by mass or more of component (A), and contains 1 to 40% by mass of (B) isododecane, and is substantially free of cyclic silicone. Component (A) contains at least (A2-1) highly polymerized dimethiconol, and may contain 1 to 30% by mass of highly polymerized dimethiconol (A2-1) relative to the total content of component (A). It may further contain (C) amino-modified silicone. It may further contain (D) dicarboxylic acid ester oil that is liquid at 25°C.
本発明によれば、使用感、効果の持続性、及び柔らかさを向上できる。 The present invention improves usability, durability of effect, and softness.
以下、本発明の非水系ヘアオイル（以下、単に「ヘアオイル」という）を具体化した一実施形態を説明する。本実施形態のヘアオイルは、（Ａ）成分として（Ａ１）ジメチコン及び（Ａ２）ジメチコノールを含有し、（Ａ）成分の含有量が６０質量％以上、並びに（Ｂ）イソドデカンを１～４０質量％を含有する。さらに、例えば（Ｃ）アミノ変性シリコーン及び（Ｄ）２５℃で液状のジカルボン酸系エステル油を含有してもよい。 One embodiment of the non-aqueous hair oil (hereinafter simply referred to as "hair oil") of the present invention will be described below. The hair oil of this embodiment contains (A1) dimethicone and (A2) dimethiconol as component (A), with the content of component (A) being 60% by mass or more, and (B) isododecane being 1 to 40% by mass. It may further contain, for example, (C) amino-modified silicone and (D) dicarboxylic acid-based ester oil that is liquid at 25°C.
（Ａ）成分は、まとまり感、つや等の効果の持続性を向上させる。ヘアオイル中における（Ａ）成分の含有量の下限は、６０質量％以上、好ましくは６５質量％以上、より好ましくは７０質量％以上である。（Ａ）成分の含有量が６０質量％以上であると、まとまり感、つや等の効果の持続性を向上できる。 Component (A) improves the durability of effects such as manageability and shine. The lower limit of the content of component (A) in the hair oil is 60% by mass or more, preferably 65% by mass or more, and more preferably 70% by mass or more. When the content of component (A) is 60% by mass or more, the durability of effects such as manageability and shine can be improved.
ヘアオイル中における（Ａ）成分の含有量の上限は、適宜設定されるが、好ましくは９０質量％以下、より好ましくは８５質量％以下、さらに好ましくは８０質量％以下である。（Ａ）成分の含有量が９０質量％以下であると、伸び等の使用感をより向上させる。 The upper limit of the content of component (A) in the hair oil is set appropriately, but is preferably 90% by mass or less, more preferably 85% by mass or less, and even more preferably 80% by mass or less. When the content of component (A) is 90% by mass or less, the feel when used, such as stretchiness, is further improved.
（Ａ）成分は、少なくとも（Ａ２－１）高重合ジメチコノールを含むことが好ましい。（Ａ２－１）高重合ジメチコノールを含むことにより、毛髪の柔らかさをより向上させる。なお、本実施形態において、（Ａ２－１）高重合ジメチコノールの平均重合度の下限は、好ましくは１０００以上、より好ましくは２０００以上である。（Ａ２－１）高重合ジメチコノールの平均重合度の上限は、好ましくは２００００以下、より好ましくは１００００以下である。（Ａ２－１）高重合ジメチコノールの平均重合度をかかる範囲内に規定することにより、毛髪の柔らかさをより向上させる。 The (A) component preferably contains at least (A2-1) highly polymerized dimethiconol. By containing (A2-1) highly polymerized dimethiconol, the softness of hair is further improved. In this embodiment, the lower limit of the average polymerization degree of (A2-1) highly polymerized dimethiconol is preferably 1000 or more, more preferably 2000 or more. The upper limit of the average polymerization degree of (A2-1) highly polymerized dimethiconol is preferably 20000 or less, more preferably 10000 or less. By specifying the average polymerization degree of (A2-1) highly polymerized dimethiconol within this range, the softness of hair is further improved.
ヘアオイル中における（Ａ２－１）高重合ジメチコノールの含有量の下限は、適宜設定されるが、好ましくは１質量％以上、より好ましくは３質量％以上である。（Ａ２－１）高重合ジメチコノールの含有量が１質量％以上であると、柔らかさをより向上させる。 The lower limit of the content of (A2-1) highly polymerized dimethiconol in the hair oil is set appropriately, but is preferably 1% by mass or more, and more preferably 3% by mass or more. When the content of (A2-1) highly polymerized dimethiconol is 1% by mass or more, softness is further improved.
ヘアオイル中における（Ａ２－１）高重合ジメチコノールの含有量の上限は、適宜設定されるが、好ましくは２０質量％以下、より好ましくは１５質量％以下である。（Ａ２－１）高重合ジメチコノールの含有量が２０質量％以下であると、伸び等の使用感をより向上させる。 The upper limit of the content of (A2-1) highly polymerized dimethiconol in the hair oil is set appropriately, but is preferably 20% by mass or less, and more preferably 15% by mass or less. If the content of (A2-1) highly polymerized dimethiconol is 20% by mass or less, the feel when used, such as stretchiness, is further improved.
（Ａ）成分の全含有量中における（Ａ２－１）高重合ジメチコノールの含有量の下限は、適宜設定されるが、好ましくは１質量％以上、より好ましくは３質量％以上である。かかる（Ａ２－１）高重合ジメチコノールの含有量を１質量％以上に規定することにより、柔らかさをより向上させる。 The lower limit of the content of highly polymerized dimethiconol (A2-1) in the total content of component (A) is set appropriately, but is preferably 1% by mass or more, and more preferably 3% by mass or more. By setting the content of highly polymerized dimethiconol (A2-1) to 1% by mass or more, softness is further improved.
（Ａ）成分の全含有量中における（Ａ２－１）高重合ジメチコノールの含有量の上限は、適宜設定されるが、好ましくは３０質量％以下、より好ましくは２０質量％以下である。かかる（Ａ２－１）高重合ジメチコノールの含有量を３０質量％以下に規定することにより、伸び等の使用感をより向上させる。 The upper limit of the content of (A2-1) highly polymerized dimethiconol in the total content of component (A) is set appropriately, but is preferably 30% by mass or less, and more preferably 20% by mass or less. By setting the content of (A2-1) highly polymerized dimethiconol at 30% by mass or less, the feel when used, such as stretchability, is further improved.
（Ａ）成分は、（Ａ１－１）高重合ジメチコンを含んでもよい。（Ａ１－１）高重合ジメチコンを含むことにより、まとまり感、つや等の効果の持続性を向上させる。なお、本実施形態において、（Ａ１－１）高重合ジメチコンの平均重合度の下限は、好ましくは１０００以上、より好ましくは２０００以上である。（Ａ１－１）高重合ジメチコンの平均重合度の上限は、好ましくは２００００以下、より好ましくは１００００以下である。平均重合度をかかる範囲内に規定することにより、まとまり感、つや等の効果の持続性をより向上させる。 Component (A) may contain (A1-1) highly polymerized dimethicone. By containing (A1-1) highly polymerized dimethicone, the durability of effects such as manageability and gloss is improved. In this embodiment, the lower limit of the average polymerization degree of (A1-1) highly polymerized dimethicone is preferably 1000 or more, more preferably 2000 or more. The upper limit of the average polymerization degree of (A1-1) highly polymerized dimethicone is preferably 20000 or less, more preferably 10000 or less. By specifying the average polymerization degree within this range, the durability of effects such as manageability and gloss is further improved.
ヘアオイル中における（Ａ１－１）高重合ジメチコンの含有量の下限は、適宜設定されるが、好ましくは０．５質量％以上、より好ましくは１質量％以上である。（Ａ１－１）高重合ジメチコンの含有量が０．５質量％以上であると、つやの持続性をより向上させる。 The lower limit of the content of (A1-1) highly polymerized dimethicone in the hair oil is set appropriately, but is preferably 0.5% by mass or more, and more preferably 1% by mass or more. If the content of (A1-1) highly polymerized dimethicone is 0.5% by mass or more, the durability of luster is further improved.
ヘアオイル中における（Ａ１－１）高重合ジメチコンの含有量の上限は、適宜設定されるが、好ましくは１０質量％以下、より好ましくは８質量％以下である。（Ａ１－１）高重合ジメチコンの含有量が１０質量％以下であると、伸び等の使用感をより損なわない。 The upper limit of the content of (A1-1) highly polymerized dimethicone in the hair oil is set appropriately, but is preferably 10% by mass or less, and more preferably 8% by mass or less. If the content of (A1-1) highly polymerized dimethicone is 10% by mass or less, the feeling of use, such as stretchiness, is not impaired.
（Ａ）成分は、（Ａ１－２）低重合ジメチコン及び（Ａ２－２）低重合ジメチコノールから選ばれる少なくとも一種を含んでもよい。（Ａ１－２）低重合ジメチコン及び（Ａ２－２）低重合ジメチコノールから選ばれる少なくとも一種を含むことにより、伸び等の使用感を向上させる。なお、本実施形態において、（Ａ１－２）低重合ジメチコン及び（Ａ２－２）低重合ジメチコノールの平均重合度の下限は、それぞれ好ましく１以上、より好ましくは２以上である。（Ａ１－２）低重合ジメチコン及び（Ａ２－２）低重合ジメチコノールの平均重合度の上限は、それぞれ好ましくは１００以下、より好ましくは９０以下である。平均重合度をかかる範囲内に規定することにより、伸び等の使用感をより向上させる。 The (A) component may contain at least one selected from (A1-2) low-polymerized dimethicone and (A2-2) low-polymerized dimethiconol. By containing at least one selected from (A1-2) low-polymerized dimethicone and (A2-2) low-polymerized dimethiconol, the feeling of use such as stretchability is improved. In this embodiment, the lower limit of the average polymerization degree of (A1-2) low-polymerized dimethicone and (A2-2) low-polymerized dimethiconol is preferably 1 or more, more preferably 2 or more. The upper limit of the average polymerization degree of (A1-2) low-polymerized dimethicone and (A2-2) low-polymerized dimethiconol is preferably 100 or less, more preferably 90 or less. By specifying the average polymerization degree within such range, the feeling of use such as stretchability is further improved.
ヘアオイル中における（Ａ１－２）低重合ジメチコン及び（Ａ２－２）低重合ジメチコノールから選ばれる少なくとも一種の含有量の下限は、適宜設定されるが、好ましくは４０質量％以上、より好ましくは５０質量％以上である。かかる含有量が４０質量％以上であると、伸び等の使用感をより向上させる。 The lower limit of the content of at least one selected from (A1-2) low polymerized dimethicone and (A2-2) low polymerized dimethiconol in the hair oil is set appropriately, but is preferably 40% by mass or more, and more preferably 50% by mass or more. If the content is 40% by mass or more, the feel when used, such as stretchiness, is further improved.
ヘアオイル中における（Ａ１－２）低重合ジメチコン及び（Ａ２－２）低重合ジメチコノールから選ばれる少なくとも一種の含有量の上限は、適宜設定されるが、好ましくは８０質量％以下、より好ましくは７０質量％以下である。かかる含有量が８０質量％以下であると、効果の持続性をより向上させる。 The upper limit of the content of at least one selected from (A1-2) low polymerized dimethicone and (A2-2) low polymerized dimethiconol in the hair oil is set appropriately, but is preferably 80% by mass or less, and more preferably 70% by mass or less. If the content is 80% by mass or less, the durability of the effect is further improved.
（Ｂ）イソドデカンは、柔らかさを損なわず、かつ伸び（使用感）を向上させる。ヘアオイル中における（Ｂ）イソドデカンの含有量の下限は、１質量％以上、好ましくは５質量％以上、より好ましくは１０質量％以上である。（Ｂ）イソドデカンの含有量が１質量％以上であると、柔らかさを損なわず、かつ伸び（使用感）を向上させる。また、効果の持続性をより向上させる。 (B) Isododecane improves the stretch (feel when used) without impairing softness. The lower limit of the content of (B) Isododecane in the hair oil is 1% by mass or more, preferably 5% by mass or more, and more preferably 10% by mass or more. When the content of (B) Isododecane is 1% by mass or more, the softness is not impaired and the stretch (feel when used) is improved. In addition, the durability of the effect is further improved.
ヘアオイル中における（Ｂ）イソドデカンの含有量の上限は、４０質量％以下、好ましくは３８質量％以下、より好ましくは３５質量％以下である。（Ｂ）イソドデカンの含有量が４０質量％以下であると、効果の持続性を損なわない。また、伸び等の使用感をより向上させる。 The upper limit of the content of (B) isododecane in the hair oil is 40% by mass or less, preferably 38% by mass or less, and more preferably 35% by mass or less. If the content of (B) isododecane is 40% by mass or less, the durability of the effect is not impaired. In addition, the feel of use, such as stretchiness, is further improved.
（Ｃ）アミノ変性シリコーンは、根元の新生部から毛先のダメージ部への均一な指通り等の使用感をより向上させる。（Ｃ）アミノ変性シリコーンとは、（－Ｓｉ－Ｏ－）の繰り返しからなるポリシロキサン骨格を持ち、そのケイ素原子のアルキル側鎖の一部がアミノ変性されたものである。（Ｃ）アミノ変性シリコーンの具体例としては、例えばアミノプロピルメチルシロキサン・ジメチルシロキサン共重合体（アミノプロピルジメチコン（ＩＮＣＩ名称））、アミノエチルアミノプロピルメチルシロキサン・ジメチルシロキサン共重合体（アモジメチコン）、（ビスイソブチルＰＥＧ－１４／アモジメチコン）コポリマー等が挙げられる。好ましくは、アミノエチルアミノプロピルメチルシロキサン・ジメチルシロキサン共重合体が挙げられる。これらの具体例は、一種類のみであってもよいし、二種類以上を組み合わせて使用してもよい。 (C) Amino-modified silicone improves the feel of the hair, such as smooth finger-combing from the newly grown part at the root to the damaged part at the tip. (C) Amino-modified silicone has a polysiloxane skeleton consisting of a repeating (-Si-O-) structure, and a part of the alkyl side chain of the silicon atom is amino-modified. Specific examples of (C) amino-modified silicone include aminopropylmethylsiloxane-dimethylsiloxane copolymer (aminopropyl dimethicone (INCI name)), aminoethylaminopropylmethylsiloxane-dimethylsiloxane copolymer (amodimethicone), (bisisobutylPEG-14/amodimethicone) copolymer, etc. Preferably, aminoethylaminopropylmethylsiloxane-dimethylsiloxane copolymer is used. These specific examples may be used alone or in combination of two or more.
（Ｃ）アミノ変性シリコーンのアミノ当量の下限は、適宜設定されるが、好ましくは８００ｇ／ｍｏｌ以上、より好ましくは１０００ｇ／ｍｏｌ以上である。（Ｃ）アミノ変性シリコーンのアミノ当量の上限は、適宜設定されるが、好ましくは３０００ｇ／ｍｏｌ以下、より好ましくは２０００ｇ／ｍｏｌ以下である。アミノ当量をかかる範囲内に規定することにより、使用感をより向上させる。アミノ当量とは、アミノ基又はアンモニウム基１個当たりのシロキサン骨格の質量を意味している。表記単位のｇ／ｍｏｌはアミノ基又はアンモニウム基１ｍｏｌ当たりに換算した値を示す。 The lower limit of the amino equivalent of (C) amino-modified silicone is set appropriately, but is preferably 800 g/mol or more, more preferably 1000 g/mol or more. The upper limit of the amino equivalent of (C) amino-modified silicone is set appropriately, but is preferably 3000 g/mol or less, more preferably 2000 g/mol or less. By setting the amino equivalent within this range, the feeling of use is further improved. The amino equivalent means the mass of the siloxane skeleton per amino group or ammonium group. The unit of g/mol indicates the value converted into 1 mol of amino groups or ammonium groups.
ヘアオイル中における（Ｃ）アミノ変性シリコーンの含有量の下限は、適宜設定されるが、好ましくは０．０１質量％以上、より好ましくは０．１質量％以上である。（Ｃ）アミノ変性シリコーンの含有量が０．０１質量％以上であると、均一な指通り等の使用感をより向上させる。 The lower limit of the content of (C) amino-modified silicone in the hair oil is set appropriately, but is preferably 0.01% by mass or more, and more preferably 0.1% by mass or more. When the content of (C) amino-modified silicone is 0.01% by mass or more, the feel when used, such as a smooth feel when running the fingers through the hair, is further improved.
ヘアオイル中における（Ｃ）アミノ変性シリコーンの含有量の上限は、適宜設定されるが、好ましくは５質量％以下、より好ましくは３質量％以下である。（Ｃ）アミノ変性シリコーンの含有量が５質量％以下であると、べたつき等を抑制し、使用感をより向上させる。 The upper limit of the content of (C) amino-modified silicone in the hair oil is set appropriately, but is preferably 5% by mass or less, and more preferably 3% by mass or less. When the content of (C) amino-modified silicone is 5% by mass or less, stickiness and the like are suppressed, and the feeling of use is further improved.
（Ｄ）２５℃で液状のジカルボン酸系エステル油は、根元の新生部から毛先のダメージ部への均一な指通り等の使用感をより向上させる。（Ｄ）成分の具体例としては、例えばコハク酸ジエステル、アジピン酸ジエステル、セバシン酸ジエステル、リンゴ酸ジエステル等が挙げられる。コハク酸ジエステルの具体例としては、例えばコハク酸ジエチルヘキシル、コハク酸ジエトキシエチル、コハク酸ビスエトキシジグリコール、コハク酸ジオクチル等が挙げられる。アジピン酸ジエステルの具体例としては、例えばアジピン酸ジイソブチル、アジピン酸ジイソプロピル、アジピン酸ジヘプチルウンデシル、アジピン酸ジブチル、アジピン酸ジエトキシエチル等が挙げられる。セバシン酸ジエステルの具体例としては、例えばセバシン酸ジイソプロピル、セバシン酸ジエチル、セバシン酸ジオクチル等が挙げられる。リンゴ酸ジエステルの具体例としては、例えばリンゴ酸ジイソステアリル等が挙げられる。これらの具体例は、一種類のみであってもよいし、二種類以上を組み合わせて使用してもよい。これらの中で、均一な指通り等の使用感を向上させる効果に優れる観点から分岐のアルキル基を有するジカルボン酸系エステル油が好ましい。 (D) Dicarboxylic acid ester oil that is liquid at 25°C improves the feel of use, such as smooth fingering from the new roots to the damaged ends. Specific examples of the (D) component include succinic acid diester, adipic acid diester, sebacic acid diester, malic acid diester, etc. Specific examples of succinic acid diester include diethylhexyl succinate, diethoxyethyl succinate, bisethoxydiglycol succinate, dioctyl succinate, etc. Specific examples of adipic acid diester include diisobutyl adipate, diisopropyl adipate, diheptylundecyl adipate, dibutyl adipate, diethoxyethyl adipate, etc. Specific examples of sebacic acid diester include diisopropyl sebacate, diethyl sebacate, dioctyl sebacate, etc. Specific examples of malic acid diester include diisostearyl malate, etc. These specific examples may be used alone or in combination of two or more. Among these, dicarboxylic acid ester oils having branched alkyl groups are preferred from the viewpoint of their excellent effect of improving the feel of use, such as a smooth feel when running through the fingers.
ヘアオイル中における（Ｄ）成分の含有量の下限は、適宜設定されるが、好ましくは０．１質量％以上、より好ましくは１質量％以上である。（Ｄ）成分の含有量が０．１質量％以上であると、均一な指通り等の使用感をより向上させる。 The lower limit of the content of component (D) in the hair oil is set appropriately, but is preferably 0.1% by mass or more, and more preferably 1% by mass or more. When the content of component (D) is 0.1% by mass or more, the feel when using the hair oil, such as a smooth feel when running your fingers through it, is further improved.
ヘアオイル中における（Ｄ）成分の含有量の上限は、適宜設定されるが、好ましくは１０質量％以下、より好ましくは５質量％以下である。（Ｄ）成分の含有量が１０質量％以下であると、べたつき等を抑制し、使用感をより向上させる。 The upper limit of the content of component (D) in the hair oil is set as appropriate, but is preferably 10% by mass or less, and more preferably 5% by mass or less. When the content of component (D) is 10% by mass or less, stickiness and the like are suppressed, and the feel of use is further improved.
本実施形態のヘアオイルは、実質的に環状シリコーンを含有しない。本実施形態における「実質的に環状シリコーンを含有しない」とは、「別途、環状シリコーンを含有させることはしない」という意味であり、各配合成分に含まれる少量の環状シリコーンまで除外するものではない。ヘアオイルが環状シリコーンを実質的に含有しないため、（Ａ）成分等の含有量を増加させることができ、効果の持続性を向上できる。 The hair oil of this embodiment does not substantially contain cyclic silicone. In this embodiment, "substantially does not contain cyclic silicone" means "no additional cyclic silicone is added" and does not exclude small amounts of cyclic silicone contained in each blended ingredient. Because the hair oil does not substantially contain cyclic silicone, the content of component (A) etc. can be increased, improving the durability of the effect.
本実施形態のヘアオイルは、剤型が非水系のため、実質的に水を含有しない。本実施形態における「実質的に水を含有しない」とは、「別途、水を含有させることはしない」という意味であり、各配合成分に含まれる微量の水の配合まで除外するものではない。ヘアオイルの剤型が非水系のため、効果の持続性を付与することができる。また、濁りや各種油剤の分離及び沈殿を抑制し、安定性を向上させる。 The hair oil of this embodiment is non-aqueous in formulation and therefore does not substantially contain water. In this embodiment, "substantially does not contain water" means "water is not added separately" and does not exclude the inclusion of trace amounts of water contained in each blended ingredient. Since the hair oil is non-aqueous in formulation, it can provide a sustained effect. It also improves stability by suppressing turbidity and separation and precipitation of various oils.
本実施形態のヘアオイルは、必要に応じて、前述した成分以外の成分、例えば可溶化剤、上記以外の油性成分、多価アルコール、界面活性剤、糖、防腐剤、安定剤、植物抽出物、生薬抽出物、ビタミン、香料、酸化防止剤、キレート化剤、紫外線吸収剤等をさらに含有してもよい。 The hair oil of this embodiment may further contain ingredients other than those mentioned above, such as solubilizers, oily ingredients other than those mentioned above, polyhydric alcohols, surfactants, sugars, preservatives, stabilizers, plant extracts, herbal extracts, vitamins, fragrances, antioxidants, chelating agents, UV absorbers, etc., as necessary.
可溶化剤は、例えば、ヘアオイルの粘度を調整する場合に配合される。使用される可溶化剤の例としては、例えば有機溶媒（溶剤）が挙げられる。有機溶媒の具体例としては、例えばエタノール、ｎ－プロパノール、イソプロパノール、メチルセロソルブ、エチルセロソルブ、メチルカルビトール、エチルカルビトール、ベンジルアルコール、フェネチルアルコール、γ－フェニルプロピルアルコール、ケイ皮アルコール、アニスアルコール、ｐ－メチルベンジルアルコール、α－ジメチルフェネチルアルコール、α－フェニルエタノール、エチレングリコールフェニルエーテル（フェノキシエタノール）、フェノキシイソプロパノール、２－ベンジルオキシエタノール、Ｎ－アルキルピロリドン、炭酸アルキレン、アルキルエーテル等が挙げられる。これらの可溶化剤のうち、一種のみが単独で含有されてもよいし、二種以上が組み合わされて含有されてもよい。 Solubilizers are blended, for example, when adjusting the viscosity of hair oil. Examples of solubilizers used include organic solvents (solvents). Specific examples of organic solvents include ethanol, n-propanol, isopropanol, methyl cellosolve, ethyl cellosolve, methyl carbitol, ethyl carbitol, benzyl alcohol, phenethyl alcohol, γ-phenylpropyl alcohol, cinnamic alcohol, anise alcohol, p-methylbenzyl alcohol, α-dimethylphenethyl alcohol, α-phenylethanol, ethylene glycol phenyl ether (phenoxyethanol), phenoxyisopropanol, 2-benzyloxyethanol, N-alkylpyrrolidone, alkylene carbonate, alkyl ether, etc. Among these solubilizers, only one may be contained alone, or two or more may be contained in combination.
上記以外の油性成分は、毛髪にうるおい感を付与する。そのため、ヘアオイルは、本発明の効果を阻害しない範囲内において油性成分を含有してもよい。油性成分としては、例えば油脂、ロウ類、上記以外の炭化水素、上記以外のエステル油、高級アルコール、高級脂肪酸、アルキルグリセリルエーテル、上記以外のシリコーン等が挙げられる。 Oily components other than those mentioned above impart a moisturizing feel to hair. Therefore, hair oil may contain oily components within a range that does not impair the effects of the present invention. Examples of oily components include fats and oils, waxes, hydrocarbons other than those mentioned above, ester oils other than those mentioned above, higher alcohols, higher fatty acids, alkyl glyceryl ethers, silicones other than those mentioned above, etc.
油脂の具体例としては、例えばアルガニアスピノサ核油、オリーブ油（オリブ油）、ツバキ油、シア脂、アーモンド油、サフラワー油、ヒマワリ油、大豆油、綿実油、ゴマ油、トウモロコシ油、ナタネ油、コメヌカ油、コメ胚芽油、ブドウ種子油、アボカド油、マカダミアナッツ油、ヒマシ油、ヤシ油、月見草油、杏仁油、パーシック油、桃仁油、パーム油、卵黄油等が挙げられる。ロウ類の具体例としては、例えばラノリン、ミツロウ、キャンデリラロウ、カルナウバロウ、ホホバ油等が挙げられる。炭化水素の具体例としては、例えばパラフィン、オレフィンオリゴマー、ポリイソブテン、水添ポリイソブテン、ミネラルオイル、スクワラン、ポリブテン、ポリエチレン、マイクロクリスタリンワックス、ワセリン、流動パラフィン、軽質イソパラフィン、軽質流動イソパラフィン、イソパラフィン、α－オレフィンオリゴマー、合成スクワラン等が挙げられる。 Specific examples of fats and oils include, for example, Argania spinosa kernel oil, olive oil, camellia oil, shea butter, almond oil, safflower oil, sunflower oil, soybean oil, cottonseed oil, sesame oil, corn oil, rapeseed oil, rice bran oil, rice germ oil, grape seed oil, avocado oil, macadamia nut oil, castor oil, coconut oil, evening primrose oil, apricot kernel oil, persic oil, peach kernel oil, palm oil, egg yolk oil, etc. Specific examples of waxes include, for example, lanolin, beeswax, candelilla wax, carnauba wax, jojoba oil, etc. Specific examples of hydrocarbons include paraffin, olefin oligomer, polyisobutene, hydrogenated polyisobutene, mineral oil, squalane, polybutene, polyethylene, microcrystalline wax, petrolatum, liquid paraffin, light isoparaffin, light liquid isoparaffin, isoparaffin, α-olefin oligomer, synthetic squalane, etc.
エステル油の具体例としては、例えばミリスチン酸イソプロピル、オクタン酸セチル、イソノナン酸イソノニル、ミリスチン酸オクチルドデシル、パルミチン酸イソプロピル、ステアリン酸ステアリル、ミリスチン酸ミリスチル、ミリスチン酸イソトリデシル、パルミチン酸２－エチルへキシル、リシノール酸オクチルドデシル、１０～３０の炭素数を有する脂肪酸コレステリル／ラノステリル、乳酸セチル、酢酸ラノリン、ジ－２－エチルヘキサン酸エチレングリコール、ペンタエリスリトール脂肪酸エステル、ジペンタエリスリトール脂肪酸エステル、カプリン酸セチル、トリカプリル酸グリセリル、２－エチルヘキサン酸セチル、イソステアリン酸硬化ヒマシ油、パラメトキシケイ皮酸２－エチルヘキシル等が挙げられる。 Specific examples of ester oils include isopropyl myristate, cetyl octanoate, isononyl isononanoate, octyldodecyl myristate, isopropyl palmitate, stearyl stearate, myristyl myristate, isotridecyl myristate, 2-ethylhexyl palmitate, octyldodecyl ricinoleate, cholesteryl/lanosteryl fatty acids having 10 to 30 carbon atoms, cetyl lactate, lanolin acetate, ethylene glycol di-2-ethylhexanoate, pentaerythritol fatty acid esters, dipentaerythritol fatty acid esters, cetyl caprate, glyceryl tricaprylate, cetyl 2-ethylhexanoate, hydrogenated castor oil isostearate, and 2-ethylhexyl paramethoxycinnamate.
高級アルコールの具体例としては、例えばセチルアルコール（セタノール）、２－ヘキシルデカノール、ステアリルアルコール、イソステアリルアルコール、セトステアリルアルコール、オレイルアルコール、アラキルアルコール、ベヘニルアルコール、２－オクチルドデカノール、ラウリルアルコール、ミリスチルアルコール、デシルテトラデカノール、ラノリンアルコール等が挙げられる。 Specific examples of higher alcohols include cetyl alcohol (cetanol), 2-hexyldecanol, stearyl alcohol, isostearyl alcohol, cetostearyl alcohol, oleyl alcohol, arachyl alcohol, behenyl alcohol, 2-octyldodecanol, lauryl alcohol, myristyl alcohol, decyltetradecanol, lanolin alcohol, etc.
高級脂肪酸の具体例としては、例えばラウリン酸、ミリスチン酸、パルミチン酸、ステアリン酸、ベヘニン酸、イソステアリン酸、１２－ヒドロキシステアリン酸、オレイン酸、ラノリン脂肪酸等が挙げられる。アルキルグリセリルエーテルの具体例としては、例えばバチルアルコール、キミルアルコール、セラキルアルコール、イソステアリルグリセリルエーテル等が挙げられる。 Specific examples of higher fatty acids include lauric acid, myristic acid, palmitic acid, stearic acid, behenic acid, isostearic acid, 12-hydroxystearic acid, oleic acid, lanolin fatty acid, etc. Specific examples of alkyl glyceryl ethers include batyl alcohol, chimyl alcohol, selachyl alcohol, isostearyl glyceryl ether, etc.
シリコーンの具体例としては、例えばメチルフェニルポリシロキサン、ポリエーテル変性シリコーン（例えば、（ＰＥＧ／ＰＰＧ／ブチレン／ジメチコン）コポリマー）、ベタイン変性シリコーン、アルキル変性シリコーン、アルコキシ変性シリコーン、メルカプト変性シリコーン、カルボキシ変性シリコーン、フッ素変性シリコーン等が挙げられる。これらの油性成分のうち、一種のみが単独で含有されてもよいし、二種以上が組み合わされて含有されてもよい。 Specific examples of silicones include methylphenylpolysiloxane, polyether-modified silicone (e.g., (PEG/PPG/butylene/dimethicone) copolymer), betaine-modified silicone, alkyl-modified silicone, alkoxy-modified silicone, mercapto-modified silicone, carboxy-modified silicone, and fluorine-modified silicone. Of these oily components, only one may be contained alone, or two or more may be contained in combination.
多価アルコールとしては、例えばグリコール、グリセリン等が挙げられる。グリコールとしては、例えばエチレングリコール、ジエチレングリコール、トリエチレングリコール、ポリエチレングリコール、高重合ポリエチレングリコール、プロピレングリコール、ジプロピレングリコール、ポリプロピレングリコール、イソプレングリコール、１，３－ブチレングリコール等が挙げられる。グリセリンとしては、例えばグリセリン、ジグリセリン、ポリグリセリン等が挙げられる。これらの多価アルコールのうち、一種のみが単独で含有されてもよいし、二種以上が組み合わされて含有されてもよい。 Examples of polyhydric alcohols include glycol and glycerin. Examples of glycols include ethylene glycol, diethylene glycol, triethylene glycol, polyethylene glycol, highly polymerized polyethylene glycol, propylene glycol, dipropylene glycol, polypropylene glycol, isoprene glycol, and 1,3-butylene glycol. Examples of glycerin include glycerin, diglycerin, and polyglycerin. Only one of these polyhydric alcohols may be contained alone, or two or more may be contained in combination.
糖の具体例としては、例えばグルコース、ガラクトース等の単糖、マルトース、スクロース、フルクトース、トレハロース等の二糖、糖アルコール等が挙げられる。防腐剤の具体例としては、例えばパラベン、メチルパラベン、安息香酸ナトリウム等が挙げられる。安定剤の具体例としては、例えばフェナセチン、８－ヒドロキシキノリン、アセトアニリド、ピロリン酸ナトリウム、バルビツール酸、尿酸、タンニン酸等が挙げられる。酸化防止剤の具体例としては、例えばアスコルビン酸類及び亜硫酸塩等が挙げられる。キレート化剤の具体例としては、例えばエデト酸（エチレンジアミン四酢酸（ＥＤＴＡ））、エデト酸二ナトリウム、エデト酸四ナトリウム、ジエチレントリアミン五酢酸及びその塩類、エチレンジアミンヒドロキシエチル三酢酸及びその塩類、並びにヒドロキシエタンジホスホン酸（ＨＥＤＰ）及びその塩類等が挙げられる。 Specific examples of sugars include monosaccharides such as glucose and galactose, disaccharides such as maltose, sucrose, fructose, and trehalose, and sugar alcohols. Specific examples of preservatives include paraben, methylparaben, and sodium benzoate. Specific examples of stabilizers include phenacetin, 8-hydroxyquinoline, acetanilide, sodium pyrophosphate, barbituric acid, uric acid, and tannic acid. Specific examples of antioxidants include ascorbic acids and sulfites. Specific examples of chelating agents include edetic acid (ethylenediaminetetraacetic acid (EDTA)), disodium edetate, tetrasodium edetate, diethylenetriaminepentaacetic acid and its salts, ethylenediaminehydroxyethyltriacetic acid and its salts, and hydroxyethanediphosphonic acid (HEDP) and its salts.
ヘアオイルの剤型は特に限定されず、具体例として、２５℃における剤型が、例えば液状、ゲル状、フォーム状、クリーム状、ペースト状等が挙げられる。また、エアゾール、ノンエアゾール等とすることもでき、ノンエアゾールの場合、更にスクイズフォーマー式及びポンプフォーマー式等の種々の形態をとることができる。また、エアゾールの場合、公知の噴射剤及び発泡剤を適用することができる。噴射剤又は発泡剤の具体例としては、例えば液化石油ガス（ＬＰＧ）、ジメチルエーテル（ＤＭＥ）、窒素ガス、炭酸ガス等が挙げられる。 The formulation of the hair oil is not particularly limited, and specific examples thereof include, at 25°C, liquid, gel, foam, cream, paste, etc. Furthermore, it can be an aerosol or non-aerosol, and in the case of a non-aerosol, it can take various forms such as a squeeze foamer type and a pump foamer type. In the case of an aerosol, known propellants and foaming agents can be used. Specific examples of propellants or foaming agents include liquefied petroleum gas (LPG), dimethyl ether (DME), nitrogen gas, carbon dioxide gas, etc.
本実施形態のヘアオイルによれば、以下のような効果を得ることができる。
（１）本実施形態のヘアオイルでは、（Ａ）成分として（Ａ１）ジメチコン及び（Ａ２）ジメチコノールを含有し、（Ａ）成分の含有量が６０質量％以上、並びに（Ｂ）イソドデカンを１～４０質量％を含有し、実質的に環状シリコーンを含有しない洗い流さない非水系ヘアオイルとして構成される。したがって、まとまり感、つや等の効果の持続性を向上できる。また、柔らかさを向上できる。また、製剤の伸びを改善し、使用感を向上できる。
The hair oil of the present embodiment has the following effects.
(1) The hair oil of this embodiment contains (A1) dimethicone and (A2) dimethiconol as the component (A), contains 60% by mass or more of the component (A), and contains 1 to 40% by mass of (B) isododecane, and is configured as a non-aqueous hair oil that does not substantially contain cyclic silicone and is not rinsed off. Therefore, it is possible to improve the durability of effects such as manageability and gloss. In addition, it is possible to improve softness. In addition, it is possible to improve the spreadability of the formulation and improve the feel when used.
（２）（Ａ）成分は、少なくとも（Ａ２－１）高重合ジメチコノールを含み、（Ａ）成分の全含有量に対して（Ａ２－１）高重合ジメチコノールが１～３０質量％含有する場合、毛髪の柔らかさを向上できる。また、伸び等の使用感をより向上できる。 (2) Component (A) contains at least (A2-1) highly polymerized dimethiconol. When the content of (A2-1) highly polymerized dimethiconol is 1 to 30% by mass based on the total content of component (A), it is possible to improve hair softness. In addition, it is possible to further improve the feel of use, such as stretchiness.
（３）更に（Ｃ）アミノ変性シリコーンを含有する場合、根元の新生部から毛先のダメージ部への均一な指通り等の使用感をより向上できる。
（４）更に（Ｄ）２５℃で液状のジカルボン酸系エステル油を含有する場合、根元の新生部から毛先のダメージ部への均一な指通り等の使用感をより向上できる。
(3) When the hair further contains (C) amino-modified silicone, the feel when using the hair, such as the smoothness of the hair running from the newly grown hair at the roots to the damaged hair at the tips, can be further improved.
(4) When the hair further contains (D) a dicarboxylic acid ester oil that is liquid at 25°C, the feel when using the hair, such as the smoothness of the hair running from the newly grown part at the root to the damaged part at the tip, can be further improved.
なお、上記実施形態は以下のように変更してもよい。
・上記実施形態のヘアオイルの使用方法は、特に限定されず、髪に塗布してそのまま乾かして仕上げる方法を適用することができる。損傷が大きい毛先に塗布してもよく、新生毛に塗布してもよい。また、毛髪全体に塗布しても、部分的に塗布してもよい。また、手で塗布してもよく、コーム（櫛）又は刷毛に付着されて毛髪に塗布してもよい。
The above embodiment may be modified as follows.
The method of using the hair oil of the above embodiment is not particularly limited, and can be a method of applying it to hair and drying it as it is. It can be applied to the ends of hair that are highly damaged, or to new hair. It can also be applied to the entire hair or to parts of the hair. It can also be applied by hand, or attached to a comb or brush and applied to the hair.
・上記実施形態のヘアオイルは、使用時に各成分が混合して存在すればよく、上述したヘアオイルを構成する各剤に含有される各成分の一部を別剤として保存してもよい。かかる構成においても、本願発明の効果を得ることができる。 - The hair oil of the above embodiment only needs to have the components present in a mixed state when used, and some of the components contained in the components that make up the hair oil described above may be stored as separate agents. Even with such a configuration, the effects of the present invention can be obtained.
次に、実施例及び比較例を挙げて前記実施形態を更に具体的に説明する。尚、本発明は、実施例欄記載の構成に限定されるものではない。
表１，２に示す各成分を含有する、ヘアオイルをそれぞれ調製した。表１，２における各成分を示す欄中の数値は当該欄の成分の含有量を示し、その単位は質量％である。尚、表中「成分」欄におけるＡ～Ｄの表記は、本願請求項記載の各成分に対応する化合物を示す。表中「成分」欄における「ａ，ｂ」の表記は、本願請求項記載の対比化合物を示す。
Next, the above-mentioned embodiment will be described in more detail with reference to examples and comparative examples. Note that the present invention is not limited to the configurations described in the examples section.
Hair oils were prepared containing the components shown in Tables 1 and 2. The numerical value in the column showing each component in Tables 1 and 2 indicates the content of the component in that column, and the unit is mass %. The notations A to D in the "Component" column in the tables indicate compounds corresponding to each component described in the claims of the present application. The notations "a, b" in the "Component" column in the tables indicate comparative compounds described in the claims of the present application.
まず、ストレートなヒト毛髪ウィッグ（以下、単にウィッグという。）を準備した。そのウィッグを脱色剤（ホーユー社製、商品名：プロマスターＥＸ ＬＴ）で１回脱色処理し、水洗した後、乾燥させた。この操作により脱色されたウィッグを評価用ウィッグとした。この評価用ウィッグに各例のヘアオイルを塗布し、使用感、ウィッグのまとまり感及びつやの持続性、柔らかさについて、下記に示す方法に従い評価を行った。 First, a straight human hair wig (hereinafter simply referred to as a wig) was prepared. The wig was bleached once with a bleaching agent (manufactured by Hoyu Co., Ltd., product name: Promaster EX LT), washed with water, and then dried. The wig bleached through this procedure was used as the evaluation wig. Each example of hair oil was applied to this evaluation wig, and the feel of use, wig manageability, luster durability, and softness were evaluated according to the methods described below.
（使用感）
ウィッグの根元から毛先への塗布操作を複数回繰り返した際のヘアオイルの伸びについて、パネラー５名が、以下の基準で判断することにより使用感を評価した。ヘアオイルの伸びが、優れる（５点）、良好（４点）、可（３点）、やや不良（２点）及び不良（１点）の５段階で採点し、各パネラーの採点結果について平均値を算出した。平均値が４．６点以上を「優れる：５」、３．６点以上４．６点未満を「良好：４」、２．６点以上３．６点未満を「可：３」、１．６点以上２．６点未満を「やや不良：２」、及び１．６点未満を「不良：１」とし、評価結果とした。
(Usage)
Five panelists evaluated the spread of the hair oil when the application operation from the roots to the ends of the wig was repeated several times, judging the feel of use according to the following criteria. The spread of the hair oil was scored on a five-point scale of excellent (5 points), good (4 points), fair (3 points), slightly poor (2 points), and poor (1 point), and the average score of each panelist was calculated. The average score of 4.6 points or more was determined as "excellent: 5", 3.6 points or more but less than 4.6 points was determined as "good: 4", 2.6 points or more but less than 3.6 points was determined as "fair: 3", 1.6 points or more but less than 2.6 points was determined as "slightly poor: 2", and less than 1.6 points was determined as "poor: 1".
（まとまり感の持続性）
ヘアオイルをウィッグに塗布した後のまとまり感の持続性について、パネラー５名が、以下の基準で判断した。ヘアオイルをウィッグに塗布した後、２５℃で２４時間放置した後、まとまり感について、優れる（５点）、良好（４点）、可（３点）、やや不良（２点）及び不良（１点）の５段階で採点し、各パネラーの採点結果について平均値を算出した。平均値が４．６点以上を「優れる：５」、３．６点以上４．６点未満を「良好：４」、２．６点以上３．６点未満を「可：３」、１．６点以上２．６点未満を「やや不良：２」、及び１．６点未満を「不良：１」とし、評価結果とした。
(Sustained cohesiveness)
Five panelists judged the duration of manageability after applying the hair oil to the wig according to the following criteria. After applying the hair oil to the wig and leaving it at 25°C for 24 hours, the manageability was scored on a five-point scale of excellent (5 points), good (4 points), fair (3 points), slightly poor (2 points), and poor (1 point), and the average of the scores from each panelist was calculated. The average score of 4.6 points or more was determined as "excellent: 5", 3.6 points or more but less than 4.6 points was determined as "good: 4", 2.6 points or more but less than 3.6 points was determined as "fair: 3", 1.6 points or more but less than 2.6 points was determined as "slightly poor: 2", and less than 1.6 points was determined as "poor: 1". These were the evaluation results.
（つやの持続性）
ヘアオイルをウィッグに塗布した後のつやの持続性について、パネラー５名が、以下の基準で判断した。ヘアオイルをウィッグに塗布した後、２５℃で２４時間放置した後、つやについて、優れる（５点）、良好（４点）、可（３点）、やや不良（２点）及び不良（１点）の５段階で採点し、各パネラーの採点結果について平均値を算出した。平均値が４．６点以上を「優れる：５」、３．６点以上４．６点未満を「良好：４」、２．６点以上３．６点未満を「可：３」、１．６点以上２．６点未満を「やや不良：２」、及び１．６点未満を「不良：１」とし、評価結果とした。
(Lust lasting)
Five panelists judged the durability of the luster after applying the hair oil to the wig according to the following criteria. After applying the hair oil to the wig and leaving it at 25°C for 24 hours, the luster was scored on a five-point scale of excellent (5 points), good (4 points), fair (3 points), slightly poor (2 points) and poor (1 point), and the average of the scores from each panelist was calculated. The average score of 4.6 points or more was determined as "excellent: 5", 3.6 points or more but less than 4.6 points was determined as "good: 4", 2.6 points or more but less than 3.6 points was determined as "fair: 3", 1.6 points or more but less than 2.6 points was determined as "slightly poor: 2", and less than 1.6 points was determined as "poor: 1". These were the evaluation results.
（柔らかさ）
ヘアオイルをウィッグに塗布した後のウィッグの柔らかさについて、パネラー５名が、以下の基準で判断した。ウィッグの柔らかさについて、優れる（５点）、良好（４点）、可（３点）、やや不良（２点）及び不良（１点）の５段階で採点し、各パネラーの採点結果について平均値を算出した。平均値が４．６点以上を「優れる：５」、３．６点以上４．６点未満を「良好：４」、２．６点以上３．６点未満を「可：３」、１．６点以上２．６点未満を「やや不良：２」、及び１．６点未満を「不良：１」とし、評価結果とした。
(soft)
Five panelists judged the wig's softness after applying the hair oil to the wig according to the following criteria. The wig's softness was scored on a five-point scale: excellent (5 points), good (4 points), fair (3 points), slightly poor (2 points), and poor (1 point), and the average of the scores from each panelist was calculated. The average score of 4.6 points or more was determined as "excellent: 5", 3.6 points or more but less than 4.6 points was determined as "good: 4", 2.6 points or more but less than 3.6 points was determined as "fair: 3", 1.6 points or more but less than 2.6 points was determined as "slightly poor: 2", and less than 1.6 points was determined as "poor: 1". These were the evaluation results.
＜非水系ヘアオイルの処方例＞
下記表４，５に示される処方例１，２の非水系ヘアオイルを調製した。実施例１と同様の処理方法において、毛髪処理を行った。その結果、各実施例と同等の評価が得られることを確認した。
<Formulation example of non-aqueous hair oil>
Non-aqueous hair oils were prepared according to Formulation Examples 1 and 2 shown in Tables 4 and 5 below. Hair treatment was carried out in the same manner as in Example 1. As a result, it was confirmed that the same evaluations as those of the respective Examples were obtained.
Claims (4)
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