JP7440215B2 - 水素ラジカルを使用するための装置およびその使用方法 - Google Patents
水素ラジカルを使用するための装置およびその使用方法 Download PDFInfo
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- JP7440215B2 JP7440215B2 JP2019083810A JP2019083810A JP7440215B2 JP 7440215 B2 JP7440215 B2 JP 7440215B2 JP 2019083810 A JP2019083810 A JP 2019083810A JP 2019083810 A JP2019083810 A JP 2019083810A JP 7440215 B2 JP7440215 B2 JP 7440215B2
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- coating
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- 239000001257 hydrogen Substances 0.000 title claims description 48
- 229910052739 hydrogen Inorganic materials 0.000 title claims description 48
- 239000007789 gas Substances 0.000 claims description 116
- 238000000576 coating method Methods 0.000 claims description 58
- 239000000758 substrate Substances 0.000 claims description 54
- 238000000034 method Methods 0.000 claims description 51
- 239000011248 coating agent Substances 0.000 claims description 47
- 238000009826 distribution Methods 0.000 claims description 45
- 238000006243 chemical reaction Methods 0.000 claims description 41
- 230000008569 process Effects 0.000 claims description 18
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 12
- 238000000231 atomic layer deposition Methods 0.000 claims description 11
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims description 7
- 238000007743 anodising Methods 0.000 claims description 4
- 229910052782 aluminium Inorganic materials 0.000 claims description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 3
- 239000012530 fluid Substances 0.000 claims 2
- 230000003746 surface roughness Effects 0.000 claims 1
- 210000002381 plasma Anatomy 0.000 description 45
- 239000000463 material Substances 0.000 description 26
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- 229910052799 carbon Inorganic materials 0.000 description 21
- 239000000356 contaminant Substances 0.000 description 19
- 239000001301 oxygen Substances 0.000 description 11
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- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 10
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 9
- 229910052731 fluorine Inorganic materials 0.000 description 9
- 239000011737 fluorine Substances 0.000 description 9
- 238000010438 heat treatment Methods 0.000 description 9
- 239000002243 precursor Substances 0.000 description 9
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 8
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- 230000008901 benefit Effects 0.000 description 7
- 229910044991 metal oxide Inorganic materials 0.000 description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 6
- YZCKVEUIGOORGS-IGMARMGPSA-N Protium Chemical compound [1H] YZCKVEUIGOORGS-IGMARMGPSA-N 0.000 description 6
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 6
- 229910052593 corundum Inorganic materials 0.000 description 6
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- 229910052736 halogen Inorganic materials 0.000 description 6
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- 238000004519 manufacturing process Methods 0.000 description 6
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- 230000006798 recombination Effects 0.000 description 6
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- 238000005260 corrosion Methods 0.000 description 5
- 230000007797 corrosion Effects 0.000 description 5
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- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 4
- 229910000577 Silicon-germanium Inorganic materials 0.000 description 4
- 238000002048 anodisation reaction Methods 0.000 description 4
- 229910052786 argon Inorganic materials 0.000 description 4
- 239000004035 construction material Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- SIWVEOZUMHYXCS-UHFFFAOYSA-N oxo(oxoyttriooxy)yttrium Chemical compound O=[Y]O[Y]=O SIWVEOZUMHYXCS-UHFFFAOYSA-N 0.000 description 4
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 229910052710 silicon Inorganic materials 0.000 description 4
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- 238000000859 sublimation Methods 0.000 description 4
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- 229910001928 zirconium oxide Inorganic materials 0.000 description 4
- LEVVHYCKPQWKOP-UHFFFAOYSA-N [Si].[Ge] Chemical compound [Si].[Ge] LEVVHYCKPQWKOP-UHFFFAOYSA-N 0.000 description 3
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- 150000002431 hydrogen Chemical class 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000004065 semiconductor Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- JNDMLEXHDPKVFC-UHFFFAOYSA-N aluminum;oxygen(2-);yttrium(3+) Chemical compound [O-2].[O-2].[O-2].[Al+3].[Y+3] JNDMLEXHDPKVFC-UHFFFAOYSA-N 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 2
- -1 ammonium-hexafluorosilicate compounds Chemical class 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229910052732 germanium Inorganic materials 0.000 description 2
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000009827 uniform distribution Methods 0.000 description 2
- 229910019901 yttrium aluminum garnet Inorganic materials 0.000 description 2
- XTFIVUDBNACUBN-UHFFFAOYSA-N 1,3,5-trinitro-1,3,5-triazinane Chemical compound [O-][N+](=O)N1CN([N+]([O-])=O)CN([N+]([O-])=O)C1 XTFIVUDBNACUBN-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 101100328843 Dictyostelium discoideum cofB gene Proteins 0.000 description 1
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 1
- 229910017843 NF3 Inorganic materials 0.000 description 1
- 229910017855 NH 4 F Inorganic materials 0.000 description 1
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 1
- 229910052581 Si3N4 Inorganic materials 0.000 description 1
- 229910020177 SiOF Inorganic materials 0.000 description 1
- 229910010041 TiAlC Inorganic materials 0.000 description 1
- SLODBEHWNYQCRC-UHFFFAOYSA-N [La+3].[O-2].[Zr+4] Chemical compound [La+3].[O-2].[Zr+4] SLODBEHWNYQCRC-UHFFFAOYSA-N 0.000 description 1
- CHBIYWIUHAZZNR-UHFFFAOYSA-N [Y].FOF Chemical compound [Y].FOF CHBIYWIUHAZZNR-UHFFFAOYSA-N 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical group [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- IYRWEQXVUNLMAY-UHFFFAOYSA-N carbonyl fluoride Chemical compound FC(F)=O IYRWEQXVUNLMAY-UHFFFAOYSA-N 0.000 description 1
- 239000012159 carrier gas Substances 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000005137 deposition process Methods 0.000 description 1
- OSIVBHBGRFWHOS-UHFFFAOYSA-N dicarboxycarbamic acid Chemical compound OC(=O)N(C(O)=O)C(O)=O OSIVBHBGRFWHOS-UHFFFAOYSA-N 0.000 description 1
- 239000003989 dielectric material Substances 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 238000010894 electron beam technology Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000005297 material degradation process Methods 0.000 description 1
- 150000001247 metal acetylides Chemical class 0.000 description 1
- 229910052754 neon Inorganic materials 0.000 description 1
- GKAOGPIIYCISHV-UHFFFAOYSA-N neon atom Chemical compound [Ne] GKAOGPIIYCISHV-UHFFFAOYSA-N 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 229910000069 nitrogen hydride Inorganic materials 0.000 description 1
- GVGCUCJTUSOZKP-UHFFFAOYSA-N nitrogen trifluoride Chemical compound FN(F)F GVGCUCJTUSOZKP-UHFFFAOYSA-N 0.000 description 1
- 229910052755 nonmetal Inorganic materials 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 238000002161 passivation Methods 0.000 description 1
- 238000000059 patterning Methods 0.000 description 1
- 229920002120 photoresistant polymer Polymers 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- HQVNEWCFYHHQES-UHFFFAOYSA-N silicon nitride Chemical compound N12[Si]34N5[Si]62N3[Si]51N64 HQVNEWCFYHHQES-UHFFFAOYSA-N 0.000 description 1
- 229910052814 silicon oxide Inorganic materials 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
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- 238000012360 testing method Methods 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 238000004627 transmission electron microscopy Methods 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
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- H01L21/18—Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer the devices having semiconductor bodies comprising elements of Group IV of the Periodic Table or AIIIBV compounds with or without impurities, e.g. doping materials
- H01L21/30—Treatment of semiconductor bodies using processes or apparatus not provided for in groups H01L21/20 - H01L21/26
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Description
NH4F(g)+SiGeOx(s)→(NH4)2SiF6(s)+(NH4)2GeF6(s)+H2O(g)
酸化物変換工程の結果として、酸化物を、基材上で固体のアンモニウム-ヘキサフルオロシリケート化合物および固体のアンモニウム-ヘキサフルオロゲルマネート化合物に変換することができる。
(NH4)2SiF6(s)→NH3(g)+HF(g)+SiF4(g)
その後、ガス状生成物を反応チャンバーから除去することができる。
(NH4)2GeF6(s)→NH3(g)+HF(g)+GeF4(g)
その後、ガス状生成物を反応チャンバーから除去することができる。
C(s)+H*(g)→CxHy(g)
その後、ガス状生成物を反応チャンバーから除去することができる。
Claims (15)
- 反応器システムであって、
反応チャンバー空間および内表面を備える反応チャンバーと、
前記反応チャンバーに連結する遠隔プラズマ源と、
前記反応チャンバーと前記遠隔プラズマ源との間の搬送経路と、
それらの間にチャンバーを画定する頂部および底部を有するガス分配装置であって、前記底部は、それ自体を貫通して形成され、前記チャンバーと前記反応チャンバー空間との間を流体連通する複数の穴を有し、前記頂部は、前記ガス分配装置に入る全てのガスを受け入れるように構成された入口を有し、前記底部は、中央領域と外側領域とを有し、前記中央領域は、前記複数の穴のうち、第1の直径を有する穴を有し、前記外側領域は、前記複数の穴のうち、第2の直径を有する穴を有し、前記中央領域は、前記底部の75パーセント~99パーセントである、ガス分配装置と、
前記ガス分配装置の前記チャンバー内に全体が配置されたマニホールドプレートであって、前記マニホールドプレートが、
前記頂部の前記入口と前記反応チャンバーとの間を流体連通する複数のガスチャネルであって、全てのガスが前記入口から前記マニホールドプレートの前記複数のガスチャネルを通って前記チャンバー内に移動し、前記底部の前記複数の穴を通って前記反応チャンバー空間内に移動するように構成され、前記複数のガスチャネルの各々は、前記チャンバーの前記中央領域から前記チャンバーの端部までの距離の20パーセント~80パーセントの間で延在し、前記複数のガスチャネルは、前記底部の前記中央領域から全てのガスを分配するように構成されている、複数のガスチャネル、
を有するマニホールドプレートと、
前記遠隔プラズマ源に連結する水素源と、を備え、
前記搬送経路と前記内表面の一部とは、コーティングを備え、前記コーティングは、非多孔質ALD酸化アルミニウムコーティングおよび非多孔質陽極酸化アルミニウムコーティングの少なくとも一方を含む、反応器システム。 - 前記コーティングは、原子層堆積を用いて形成される、請求項1に記載の反応器システム。
- 前記コーティングは、前記非多孔質ALD酸化アルミニウムコーティングを含み、前記コーティングの厚さは、約100nm~約750nmの範囲である、請求項1に記載の反応器システム。
- 前記コーティングは陽極酸化処理を用いて形成され、前記コーティングは非多孔質である、請求項1に記載の反応器システム。
- 前記コーティングの平均表面粗さは、約0.1μm~約0.8μmの範囲である、請求項4に記載の反応器システム。
- 前記コーティングは、前記非多孔質陽極酸化アルミニウムコーティングを含み、前記コーティングの厚さは、約450nmである、請求項4に記載の反応器システム。
- 第二の遠隔プラズマユニットと、前記第二の遠隔プラズマユニットと前記反応チャンバーとの間の第二の搬送経路と、をさらに備え、前記第二の搬送経路は、前記コーティングを備える、請求項1に記載の反応器システム。
- 前記ガス分配装置は、前記コーティングを備える、請求項1に記載の反応器システム。
- 前記マニホールドプレートは、約2~約50のガスチャネルを備える、請求項1に記載の反応器システム。
- 前記穴の各々の直径は、約0.5mm~約3mmの範囲である、請求項1に記載の反応器システム。
- 前記ガスチャネルの各々の直径は、約5mm~約15mmの範囲である、請求項1に記載の反応器システム。
- 前記中央領域内の前記穴の直径は、約0.5mm~約1.5mmである、請求項1に記載の反応器システム。
- 前記外側領域内の前記穴の直径は、約1mm~約3mmである、請求項1に記載の反応器システム。
- 前記外側領域における前記複数の穴の密度は、前記中央領域における前記複数の穴の密度よりも大きい、請求項1に記載の反応器システム。
- 前記外側領域の周囲は、前記反応チャンバー内で処理される基材の周囲よりも大きい、請求項1に記載の反応器システム。
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US20190348261A1 (en) | 2019-11-14 |
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