JP7324010B2 - 積層体 - Google Patents
積層体 Download PDFInfo
- Publication number
- JP7324010B2 JP7324010B2 JP2019012990A JP2019012990A JP7324010B2 JP 7324010 B2 JP7324010 B2 JP 7324010B2 JP 2019012990 A JP2019012990 A JP 2019012990A JP 2019012990 A JP2019012990 A JP 2019012990A JP 7324010 B2 JP7324010 B2 JP 7324010B2
- Authority
- JP
- Japan
- Prior art keywords
- acid
- meth
- resin film
- adhesive layer
- acrylate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 229920005989 resin Polymers 0.000 claims description 194
- 239000011347 resin Substances 0.000 claims description 186
- 239000010410 layer Substances 0.000 claims description 162
- 239000004820 Pressure-sensitive adhesive Substances 0.000 claims description 114
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 104
- 239000003431 cross linking reagent Substances 0.000 claims description 97
- 239000012790 adhesive layer Substances 0.000 claims description 77
- 239000000203 mixture Substances 0.000 claims description 72
- 239000000178 monomer Substances 0.000 claims description 53
- 229920000058 polyacrylate Polymers 0.000 claims description 49
- 239000000853 adhesive Substances 0.000 claims description 46
- 230000001070 adhesive effect Effects 0.000 claims description 46
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 37
- 229920001225 polyester resin Polymers 0.000 claims description 32
- 239000004645 polyester resin Substances 0.000 claims description 32
- 239000002985 plastic film Substances 0.000 claims description 28
- 229920006255 plastic film Polymers 0.000 claims description 28
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims description 26
- 239000012298 atmosphere Substances 0.000 claims description 24
- 125000000217 alkyl group Chemical group 0.000 claims description 16
- 125000004432 carbon atom Chemical group C* 0.000 claims description 16
- 238000006116 polymerization reaction Methods 0.000 claims description 16
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 14
- 125000005907 alkyl ester group Chemical group 0.000 claims description 13
- 239000003522 acrylic cement Substances 0.000 claims description 7
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 6
- -1 polyethylene terephthalate Polymers 0.000 description 201
- 239000010408 film Substances 0.000 description 193
- 230000000694 effects Effects 0.000 description 90
- 239000000758 substrate Substances 0.000 description 66
- 238000004519 manufacturing process Methods 0.000 description 57
- 238000000034 method Methods 0.000 description 54
- 239000002253 acid Substances 0.000 description 53
- 229920001940 conductive polymer Polymers 0.000 description 49
- 239000003999 initiator Substances 0.000 description 48
- 238000000576 coating method Methods 0.000 description 40
- 230000001771 impaired effect Effects 0.000 description 38
- 229920001296 polysiloxane Polymers 0.000 description 32
- 239000011248 coating agent Substances 0.000 description 31
- 150000001768 cations Chemical class 0.000 description 27
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 24
- 239000003505 polymerization initiator Substances 0.000 description 24
- 238000011282 treatment Methods 0.000 description 24
- 239000003795 chemical substances by application Substances 0.000 description 23
- 239000007788 liquid Substances 0.000 description 22
- 239000000463 material Substances 0.000 description 22
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 21
- 238000006243 chemical reaction Methods 0.000 description 21
- 238000001035 drying Methods 0.000 description 21
- 239000002608 ionic liquid Substances 0.000 description 21
- 150000002148 esters Chemical class 0.000 description 19
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 18
- 239000011230 binding agent Substances 0.000 description 18
- 239000007787 solid Substances 0.000 description 18
- 229910052751 metal Inorganic materials 0.000 description 16
- 239000002184 metal Substances 0.000 description 16
- 238000005259 measurement Methods 0.000 description 15
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 14
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 14
- 239000002904 solvent Substances 0.000 description 14
- 230000003014 reinforcing effect Effects 0.000 description 13
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 description 12
- 239000004593 Epoxy Substances 0.000 description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 12
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 12
- 239000004698 Polyethylene Substances 0.000 description 12
- 239000004743 Polypropylene Substances 0.000 description 12
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 12
- ISAOCJYIOMOJEB-UHFFFAOYSA-N benzoin Chemical compound C=1C=CC=CC=1C(O)C(=O)C1=CC=CC=C1 ISAOCJYIOMOJEB-UHFFFAOYSA-N 0.000 description 12
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 12
- 229920000573 polyethylene Polymers 0.000 description 12
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 12
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 11
- 229920001971 elastomer Polymers 0.000 description 11
- 239000011521 glass Substances 0.000 description 11
- 230000001681 protective effect Effects 0.000 description 11
- 239000005060 rubber Substances 0.000 description 11
- OZAIFHULBGXAKX-UHFFFAOYSA-N 2-(2-cyanopropan-2-yldiazenyl)-2-methylpropanenitrile Chemical compound N#CC(C)(C)N=NC(C)(C)C#N OZAIFHULBGXAKX-UHFFFAOYSA-N 0.000 description 10
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 description 10
- 239000003054 catalyst Substances 0.000 description 10
- 238000004132 cross linking Methods 0.000 description 10
- 150000004820 halides Chemical class 0.000 description 10
- 239000012948 isocyanate Substances 0.000 description 10
- 150000002513 isocyanates Chemical class 0.000 description 10
- 229920000728 polyester Polymers 0.000 description 10
- 150000003839 salts Chemical class 0.000 description 10
- 239000000243 solution Substances 0.000 description 10
- 150000005846 sugar alcohols Polymers 0.000 description 10
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 9
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 9
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 9
- 229920001577 copolymer Polymers 0.000 description 9
- 150000002430 hydrocarbons Chemical group 0.000 description 9
- 239000003112 inhibitor Substances 0.000 description 9
- 239000000126 substance Substances 0.000 description 9
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 9
- KWOLFJPFCHCOCG-UHFFFAOYSA-N Acetophenone Chemical compound CC(=O)C1=CC=CC=C1 KWOLFJPFCHCOCG-UHFFFAOYSA-N 0.000 description 8
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 8
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 8
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 8
- 150000008065 acid anhydrides Chemical class 0.000 description 8
- 239000004840 adhesive resin Substances 0.000 description 8
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 8
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 description 8
- 238000011156 evaluation Methods 0.000 description 8
- 239000007789 gas Substances 0.000 description 8
- 125000005842 heteroatom Chemical group 0.000 description 8
- QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 description 8
- 239000000314 lubricant Substances 0.000 description 8
- BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 description 8
- 229940059574 pentaerithrityl Drugs 0.000 description 8
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 8
- CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 description 8
- 238000012719 thermal polymerization Methods 0.000 description 8
- 229920002554 vinyl polymer Polymers 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 150000001450 anions Chemical class 0.000 description 7
- 150000001875 compounds Chemical class 0.000 description 7
- 239000002322 conducting polymer Substances 0.000 description 7
- 238000005227 gel permeation chromatography Methods 0.000 description 7
- 238000010438 heat treatment Methods 0.000 description 7
- 239000004814 polyurethane Substances 0.000 description 7
- 229920002635 polyurethane Polymers 0.000 description 7
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 7
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 6
- 239000004925 Acrylic resin Substances 0.000 description 6
- 229920000178 Acrylic resin Polymers 0.000 description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- 229920000877 Melamine resin Polymers 0.000 description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 6
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 6
- 239000004696 Poly ether ether ketone Substances 0.000 description 6
- 239000004734 Polyphenylene sulfide Substances 0.000 description 6
- 244000028419 Styrax benzoin Species 0.000 description 6
- 235000000126 Styrax benzoin Nutrition 0.000 description 6
- 235000008411 Sumatra benzointree Nutrition 0.000 description 6
- 150000007513 acids Chemical class 0.000 description 6
- 239000004760 aramid Substances 0.000 description 6
- 229920003235 aromatic polyamide Polymers 0.000 description 6
- 125000003118 aryl group Chemical group 0.000 description 6
- 239000007869 azo polymerization initiator Substances 0.000 description 6
- 229960002130 benzoin Drugs 0.000 description 6
- RWCCWEUUXYIKHB-UHFFFAOYSA-N benzophenone Chemical compound C=1C=CC=CC=1C(=O)C1=CC=CC=C1 RWCCWEUUXYIKHB-UHFFFAOYSA-N 0.000 description 6
- 239000012965 benzophenone Substances 0.000 description 6
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical class C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 6
- QHIWVLPBUQWDMQ-UHFFFAOYSA-N butyl prop-2-enoate;methyl 2-methylprop-2-enoate;prop-2-enoic acid Chemical compound OC(=O)C=C.COC(=O)C(C)=C.CCCCOC(=O)C=C QHIWVLPBUQWDMQ-UHFFFAOYSA-N 0.000 description 6
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 6
- 239000005038 ethylene vinyl acetate Substances 0.000 description 6
- 239000001530 fumaric acid Substances 0.000 description 6
- 235000019382 gum benzoic Nutrition 0.000 description 6
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 6
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 6
- 239000011976 maleic acid Substances 0.000 description 6
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 description 6
- 239000012046 mixed solvent Substances 0.000 description 6
- KYTZHLUVELPASH-UHFFFAOYSA-N naphthalene-1,2-dicarboxylic acid Chemical compound C1=CC=CC2=C(C(O)=O)C(C(=O)O)=CC=C21 KYTZHLUVELPASH-UHFFFAOYSA-N 0.000 description 6
- 150000002978 peroxides Chemical class 0.000 description 6
- 229920001200 poly(ethylene-vinyl acetate) Polymers 0.000 description 6
- 229920000447 polyanionic polymer Polymers 0.000 description 6
- 229920001707 polybutylene terephthalate Polymers 0.000 description 6
- 229920002530 polyetherether ketone Polymers 0.000 description 6
- 229920000139 polyethylene terephthalate Polymers 0.000 description 6
- 239000005020 polyethylene terephthalate Substances 0.000 description 6
- 239000005056 polyisocyanate Substances 0.000 description 6
- 229920001228 polyisocyanate Polymers 0.000 description 6
- 229920000642 polymer Polymers 0.000 description 6
- 229920000069 polyphenylene sulfide Polymers 0.000 description 6
- 229920001155 polypropylene Polymers 0.000 description 6
- 239000004800 polyvinyl chloride Substances 0.000 description 6
- 229920000915 polyvinyl chloride Polymers 0.000 description 6
- 235000013772 propylene glycol Nutrition 0.000 description 6
- 229920002050 silicone resin Polymers 0.000 description 6
- 239000003381 stabilizer Substances 0.000 description 6
- YRHRIQCWCFGUEQ-UHFFFAOYSA-N thioxanthen-9-one Chemical compound C1=CC=C2C(=O)C3=CC=CC=C3SC2=C1 YRHRIQCWCFGUEQ-UHFFFAOYSA-N 0.000 description 6
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical class CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 description 6
- 238000012546 transfer Methods 0.000 description 6
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 5
- 150000001336 alkenes Chemical class 0.000 description 5
- 125000003700 epoxy group Chemical group 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 5
- KTQDYGVEEFGIIL-UHFFFAOYSA-N n-fluorosulfonylsulfamoyl fluoride Chemical compound FS(=O)(=O)NS(F)(=O)=O KTQDYGVEEFGIIL-UHFFFAOYSA-N 0.000 description 5
- 238000009832 plasma treatment Methods 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 5
- 229910001887 tin oxide Inorganic materials 0.000 description 5
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 4
- NIDNOXCRFUCAKQ-RNGGSSJXSA-N (1r,2r,3s,4s)-bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1[C@@H]2C=C[C@H]1[C@H](C(=O)O)[C@@H]2C(O)=O NIDNOXCRFUCAKQ-RNGGSSJXSA-N 0.000 description 4
- MYRTYDVEIRVNKP-UHFFFAOYSA-N 1,2-Divinylbenzene Chemical compound C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 description 4
- FKTHNVSLHLHISI-UHFFFAOYSA-N 1,2-bis(isocyanatomethyl)benzene Chemical compound O=C=NCC1=CC=CC=C1CN=C=O FKTHNVSLHLHISI-UHFFFAOYSA-N 0.000 description 4
- PXGZQGDTEZPERC-UHFFFAOYSA-N 1,4-cyclohexanedicarboxylic acid Chemical compound OC(=O)C1CCC(C(O)=O)CC1 PXGZQGDTEZPERC-UHFFFAOYSA-N 0.000 description 4
- KWVGIHKZDCUPEU-UHFFFAOYSA-N 2,2-dimethoxy-2-phenylacetophenone Chemical compound C=1C=CC=CC=1C(OC)(OC)C(=O)C1=CC=CC=C1 KWVGIHKZDCUPEU-UHFFFAOYSA-N 0.000 description 4
- JAHNSTQSQJOJLO-UHFFFAOYSA-N 2-(3-fluorophenyl)-1h-imidazole Chemical compound FC1=CC=CC(C=2NC=CN=2)=C1 JAHNSTQSQJOJLO-UHFFFAOYSA-N 0.000 description 4
- IMSODMZESSGVBE-UHFFFAOYSA-N 2-Oxazoline Chemical compound C1CN=CO1 IMSODMZESSGVBE-UHFFFAOYSA-N 0.000 description 4
- AOBIOSPNXBMOAT-UHFFFAOYSA-N 2-[2-(oxiran-2-ylmethoxy)ethoxymethyl]oxirane Chemical compound C1OC1COCCOCC1CO1 AOBIOSPNXBMOAT-UHFFFAOYSA-N 0.000 description 4
- 125000000022 2-aminoethyl group Chemical group [H]C([*])([H])C([H])([H])N([H])[H] 0.000 description 4
- NLGDWWCZQDIASO-UHFFFAOYSA-N 2-hydroxy-1-(7-oxabicyclo[4.1.0]hepta-1,3,5-trien-2-yl)-2-phenylethanone Chemical compound OC(C(=O)c1cccc2Oc12)c1ccccc1 NLGDWWCZQDIASO-UHFFFAOYSA-N 0.000 description 4
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 4
- XJMMNTGIMDZPMU-UHFFFAOYSA-N 3-methylglutaric acid Chemical compound OC(=O)CC(C)CC(O)=O XJMMNTGIMDZPMU-UHFFFAOYSA-N 0.000 description 4
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 4
- HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 description 4
- NOWKCMXCCJGMRR-UHFFFAOYSA-N Aziridine Chemical compound C1CN1 NOWKCMXCCJGMRR-UHFFFAOYSA-N 0.000 description 4
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 4
- GAWIXWVDTYZWAW-UHFFFAOYSA-N C[CH]O Chemical group C[CH]O GAWIXWVDTYZWAW-UHFFFAOYSA-N 0.000 description 4
- RRHGJUQNOFWUDK-UHFFFAOYSA-N Isoprene Chemical compound CC(=C)C=C RRHGJUQNOFWUDK-UHFFFAOYSA-N 0.000 description 4
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 4
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 4
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 description 4
- 239000006087 Silane Coupling Agent Substances 0.000 description 4
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 4
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical class C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 description 4
- 239000006096 absorbing agent Substances 0.000 description 4
- 239000000654 additive Substances 0.000 description 4
- 230000000996 additive effect Effects 0.000 description 4
- 239000001361 adipic acid Substances 0.000 description 4
- 235000011037 adipic acid Nutrition 0.000 description 4
- 125000002723 alicyclic group Chemical group 0.000 description 4
- 125000001931 aliphatic group Chemical group 0.000 description 4
- 150000004703 alkoxides Chemical class 0.000 description 4
- 150000001412 amines Chemical class 0.000 description 4
- RDOXTESZEPMUJZ-UHFFFAOYSA-N anisole Chemical compound COC1=CC=CC=C1 RDOXTESZEPMUJZ-UHFFFAOYSA-N 0.000 description 4
- 230000003712 anti-aging effect Effects 0.000 description 4
- 239000003963 antioxidant agent Substances 0.000 description 4
- 239000002216 antistatic agent Substances 0.000 description 4
- 229920005601 base polymer Polymers 0.000 description 4
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 4
- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 description 4
- 239000004202 carbamide Substances 0.000 description 4
- 150000001718 carbodiimides Chemical class 0.000 description 4
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 4
- 150000001735 carboxylic acids Chemical class 0.000 description 4
- 239000013522 chelant Substances 0.000 description 4
- 239000003086 colorant Substances 0.000 description 4
- 239000006258 conductive agent Substances 0.000 description 4
- 239000000470 constituent Substances 0.000 description 4
- 230000007797 corrosion Effects 0.000 description 4
- 238000005260 corrosion Methods 0.000 description 4
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 4
- 229910001873 dinitrogen Inorganic materials 0.000 description 4
- 150000002009 diols Chemical class 0.000 description 4
- 239000000975 dye Substances 0.000 description 4
- 239000000945 filler Substances 0.000 description 4
- 239000011888 foil Substances 0.000 description 4
- 238000007756 gravure coating Methods 0.000 description 4
- RRAMGCGOFNQTLD-UHFFFAOYSA-N hexamethylene diisocyanate Chemical compound O=C=NCCCCCCN=C=O RRAMGCGOFNQTLD-UHFFFAOYSA-N 0.000 description 4
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Images
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- B32B3/26—Layered products comprising a layer with external or internal discontinuities or unevennesses, or a layer of non-planar shape; Layered products comprising a layer having particular features of form characterised by a particular shape of the outline of the cross-section of a continuous layer; characterised by a layer with cavities or internal voids ; characterised by an apertured layer
- B32B3/266—Layered products comprising a layer with external or internal discontinuities or unevennesses, or a layer of non-planar shape; Layered products comprising a layer having particular features of form characterised by a particular shape of the outline of the cross-section of a continuous layer; characterised by a layer with cavities or internal voids ; characterised by an apertured layer characterised by an apertured layer, the apertures going through the whole thickness of the layer, e.g. expanded metal, perforated layer, slit layer regular cells B32B3/12
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- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B7/00—Layered products characterised by the relation between layers; Layered products characterised by the relative orientation of features between layers, or by the relative values of a measurable parameter between layers, i.e. products comprising layers having different physical, chemical or physicochemical properties; Layered products characterised by the interconnection of layers
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Description
樹脂フィルム(1)、粘着剤層(1)、樹脂フィルム(2)、粘着剤層(2)、樹脂フィルム(3)をこの順に有する、5層以上の積層体であって、
該樹脂フィルム(2)と該粘着剤層(2)が直接に積層されてなり、
温度23℃、湿度50%RHの雰囲気下における、剥離角度180度、剥離速度30mm/分で該粘着剤層(2)を該樹脂フィルム(2)から剥離するときの粘着力が1gf/25mm以上である。
本発明の積層体は、樹脂フィルム(1)、粘着剤層(1)、樹脂フィルム(2)、粘着剤層(2)、樹脂フィルム(3)をこの順に有する、5層以上の積層体であって、該樹脂フィルム(2)と該粘着剤層(2)が直接に積層されてなる。
樹脂フィルム(1)の厚みとしては、本発明の効果をより発現させ得る点で、好ましくは1μm~300μmであり、より好ましくは10μm~200μmであり、さらに好ましくは30μm~150μmであり、特に好ましくは40μm~100μmであり、最も好ましくは50μm~80μmである。
粘着剤層(1)は、本発明の効果を損なわない範囲で、任意の適切な粘着剤層を採用し得る。粘着剤層(1)は、1層のみであってもよいし、2層以上であってもよい。
アクリル系粘着剤は、アクリル系粘着剤組成物から形成される。
ウレタン系粘着剤としては、本発明の効果を損なわない範囲で、例えば、特開2017-039859号公報などに記載の公知のウレタン系粘着剤など、任意の適切なウレタン系粘着剤を採用し得る。このようなウレタン系粘着剤としては、例えば、ウレタン系粘着剤組成物から形成されるウレタン系粘着剤であって、該ウレタン系粘着剤組成物が、ウレタンプレポリマーおよびポリオールからなる群から選ばれる少なくとも1種と架橋剤とを含むものである。ウレタン系粘着剤は、1種のみであってもよいし、2種以上であってもよい。ウレタン系粘着剤は、本発明の効果を損なわない範囲で、任意の適切な成分を含有し得る。
ゴム系粘着剤としては、本発明の効果を損なわない範囲で、例えば、特開2015-074771号公報などに記載の公知のゴム系粘着剤など、任意の適切なゴム系粘着剤を採用し得る。これらは、1種のみであってもよいし、2種以上であってもよい。ゴム系粘着剤は、本発明の効果を損なわない範囲で、任意の適切な成分を含有し得る。
シリコーン系粘着剤としては、本発明の効果を損なわない範囲で、例えば、特開2014-047280号公報などに記載の公知のシリコーン系粘着剤など、任意の適切なシリコーン系粘着剤を採用し得る。これらは、1種のみであってもよいし、2種以上であってもよい。シリコーン系粘着剤は、本発明の効果を損なわない範囲で、任意の適切な成分を含有し得る。
粘着剤層(1)は導電成分を含んでいてもよい。代表的には、粘着剤層(1)の材料となる粘着剤組成物(アクリル系粘着剤組成物、ウレタン系粘着剤組成物、ゴム系粘着剤組成物、シリコーン系粘着剤組成物からなる群から選ばれる少なくとも1種)は、導電成分を含んでいてもよい。
粘着剤層(1)の材料となる粘着剤組成物(アクリル系粘着剤組成物、ウレタン系粘着剤組成物、ゴム系粘着剤組成物、シリコーン系粘着剤組成物からなる群から選ばれる少なくとも1種)は、本発明の効果を損なわない範囲で、任意の適切な他の成分を含有し得る。このような他の成分としては、例えば、他のポリマー成分、架橋促進剤、架橋触媒、シランカップリング剤、粘着付与樹脂(ロジン誘導体、ポリテルペン樹脂、石油樹脂、油溶性フェノールなど)、老化防止剤、無機充填剤、有機充填剤、金属粉、着色剤(顔料や染料など)、箔状物、紫外線吸収剤、酸化防止剤、光安定剤、連鎖移動剤、可塑剤、軟化剤、界面活性剤、帯電防止剤、導電剤、安定剤、表面潤滑剤、レベリング剤、腐食防止剤、耐熱安定剤、重合禁止剤、滑剤、溶剤、触媒などが挙げられる。
樹脂フィルム(2)の厚みとしては、本発明の効果を損なわない範囲で、目的に応じて、任意の適切な厚みを採用し得る。このような厚みとしては、本発明の効果をより発現させ得る点で、好ましくは25μm~500μmであり、より好ましくは25μm~400μmであり、さらに好ましくは25μm~300μmであり、特に好ましくは25μm~200μmであり、最も好ましくは25μm~150μmである。
粘着剤層(2)は、本発明の効果を損なわない範囲で、任意の適切な粘着剤層を採用し得る。粘着剤層(2)は、1層のみであってもよいし、2層以上であってもよい。
粘着剤層(2)は、好ましくは、アクリル系粘着剤から構成される。
粘着剤層(2)は導電成分を含んでいてもよい。導電成分については、<1-2-5.導電成分>の項における説明をそのまま援用し得る。
粘着剤層(2)の材料となる粘着剤組成物(好ましくは、アクリル系粘着剤組成物)は、本発明の効果を損なわない範囲で、任意の適切な他の成分を含有し得る。このような他の成分としては、例えば、他のポリマー成分、架橋促進剤、架橋触媒、シランカップリング剤、粘着付与樹脂(ロジン誘導体、ポリテルペン樹脂、石油樹脂、油溶性フェノールなど)、老化防止剤、無機充填剤、有機充填剤、金属粉、着色剤(顔料や染料など)、箔状物、紫外線吸収剤、酸化防止剤、光安定剤、連鎖移動剤、可塑剤、軟化剤、界面活性剤、帯電防止剤、導電剤、安定剤、表面潤滑剤、レベリング剤、腐食防止剤、耐熱安定剤、重合禁止剤、滑剤、溶剤、触媒などが挙げられる。
樹脂フィルム(3)の厚みは、本発明の効果をより発現させ得る点で、好ましくは4μm~450μmであり、より好ましくは8μm~350μmであり、さらに好ましくは12μm~250μmであり、特に好ましくは16μm~150μmであり、最も好ましくは20μm~100μmである。
本発明の積層体は、本発明の効果を損なわない範囲で、任意の適切な方法によって製造し得る。
重量平均分子量は、ゲルパーミエーションクロマトグラフ(GPC)法により測定した。具体的には、GPC測定装置として、商品名「HLC-8120GPC」(東ソー株式会社製)を用いて、下記の条件にて測定し、標準ポリスチレン換算値により算出した。
(分子量測定条件)
・サンプル濃度:0.2重量%(テトラヒドロフラン溶液)
・サンプル注入量:10μL
・カラム:商品名「TSKguardcolumn SuperHZ-H(1本)+TSKgel SuperHZM-H(2本)」(東ソー株式会社製)
・リファレンスカラム:商品名「TSKgel SuperH-RC(1本)」(東ソー株式会社製)
・溶離液:テトラヒドロフラン(THF)
・流量:0.6mL/min
・検出器:示差屈折計(RI)
・カラム温度(測定温度):40℃
10cm×10cmの積層体(I)のセパレータを剥離し、温度23℃、湿度50%RHの雰囲気下で、評価用サンプルの粘着剤層表面を10cm×10cmガラス板(松浪硝子工業株式会社製、商品名:マイクロスライドガラスS)にハンドローラーにて貼り付け、その後、0.25MPaの圧力にて圧着した。予め除電しておいたセパレータ付表面保護フィルム(キャリアシートと称してもよい)を幅25mm、長さ150mmに切断し、温度23℃、湿度50%RHの雰囲気下で、ガラスに固定した積層体(I)の樹脂フィルム側に、2.0kgローラー1往復により貼り付け、その後、0.25MPaの圧力にて圧着した。温度23℃、湿度50%RHの雰囲気下で30分間養生した後、万能引張試験機(ミネベア株式会社製、製品名:TCM-1kNB)を用い、剥離角度180度、剥離速度30mm/分で、粘着剤層(2)を樹脂フィルム(2)から剥離し、粘着力を測定した。
10cm×10cmの積層体(I)のセパレータを剥離し、温度23℃、湿度50%RHの雰囲気下で、評価用サンプルの粘着剤層表面を10cm×10cmガラス板(松浪硝子工業株式会社製、商品名:マイクロスライドガラスS)にハンドローラーにて貼り付け、その後、0.25MPaの圧力にて圧着した。予め除電しておいたセパレータ付表面保護フィルム(キャリアシートと称してもよい)を幅25mm、長さ150mmに切断し、温度23℃、湿度50%RHの雰囲気下で、ガラスに固定した積層体(I)の樹脂フィルム側に、2.0kgローラー1往復により貼り付け、その後、0.25MPaの圧力にて圧着した。温度23℃、湿度50%RHの雰囲気下で30分間養生した後、万能引張試験機(ミネベア株式会社製、製品名:TCM-1kNB)を用い、剥離角度180度、剥離速度300mm/分で、粘着剤層(2)を樹脂フィルム(2)から剥離し、粘着力を測定した。
10cm×10cmの積層体(I)のセパレータを剥離し、温度23℃、湿度50%RHの雰囲気下で、評価用サンプルの粘着剤層表面を10cm×10cmガラス板(松浪硝子工業株式会社製、商品名:マイクロスライドガラスS)にハンドローラーにて貼り付け、その後、0.25MPaの圧力にて圧着した。予め除電しておいたセパレータ付表面保護フィルム(キャリアシートと称してもよい)を幅25mm、長さ150mmに切断し、温度23℃、湿度50%RHの雰囲気下で、ガラスに固定した積層体(I)の樹脂フィルム側に、2.0kgローラー1往復により貼り付け、その後、0.25MPaの圧力にて圧着した。温度23℃、湿度50%RHの雰囲気下で30分間養生した後、万能引張試験機(ミネベア株式会社製、製品名:TCM-1kNB)を用い、剥離角度180度、剥離速度2400mm/分で、粘着剤層(2)を樹脂フィルム(2)から剥離し、粘着力を測定した。
樹脂フィルム(1)/粘着剤層(1)/樹脂フィルム(2)からなる積層体(I)を幅25mm、長さ150mmに切断して評価用サンプルを作製した。温度23℃、湿度50%RHの雰囲気下において、作製した評価用サンプルから樹脂フィルム(1)を剥離し、ガラス板(松浪硝子工業株式会社製、商品名:マイクロスライドガラスS)に、2.0kgローラー1往復により貼り付けた。温度23℃、湿度50%RHの雰囲気下で30分間養生した後、万能引張試験機を用い、剥離角度180度、剥離速度300mm/分で剥離し、粘着力(1)を測定した。
セパレータ/粘着剤層(2)/樹脂フィルム(3)からなるセパレータ付きの積層体(II)を幅25mm、長さ150mmに切断して評価用サンプルを作製した。別途、<粘着力(1)の測定>の項目で説明した、積層体(I)から樹脂フィルム(1)を剥離した後にガラス板に張り付けた被着体を準備しておき、温度23℃、湿度50%RHの雰囲気下において、上記評価用サンプルからセパレータを剥離し、上記被着体に、2.0kgローラー1往復により貼り付けた。温度23℃、湿度50%RHの雰囲気下で30分間養生した後、万能引張試験機を用い、剥離角度180度、剥離速度300mm/分で剥離し、粘着力(2)を測定した。
村上色彩技術研究所のHM-150Nを使用し、JIS-K-7361の条件で全光線透過率を、JIS-K-7136の条件でヘイズを測定した。この際、5層積層品は光源側に樹脂フィルム(3)が向くように設置した。
積層体(I)を、幅50mm、長さ300mmに切断し、樹脂フィルム(2)側からCO2レーザーによって5mm幅で等間隔になるように5か所を、樹脂フィルム(1)の面までハーフカットし(つまり、樹脂フィルム(1)はカットされない)、5mm幅の部分を手で除去した。その後、幅60mm、長さ400mmに切断した積層体(II)の粘着剤層(2)の面を、積層体(I)の樹脂フィルム(2)の面に貼り付け、測定サンプルとした。
測定サンプルを、直径6インチのロールに対して樹脂フィルム(1)が外側になるように巻き付け、区分けされた複数の粘着剤層(1)と樹脂フィルム(2)の積層部分が粘着剤層(2)から浮いている最大量をルーペにて測定し、任意の5か所の測定の平均値を浮き量とした。
攪拌羽根、温度計、窒素ガス導入管、冷却器を備えた四つ口フラスコに、ブチルアクリレート(日本触媒社製)95部、アクリル酸(東亜合成社製)5部、重合開始剤として2,2’-アゾビスイソブチロニトリル(和光純薬工業社製)0.2部、酢酸エチル156重量部を仕込み、緩やかに攪拌しながら窒素ガスを導入し、フラスコ内の液温を63℃付近に保って10時間重合反応を行い、重量平均分子量70万の(メタ)アクリル系重合体(1)溶液(40重量%)を調製した。(メタ)アクリル系重合体(1)溶液に、(メタ)アクリル系重合体(1)溶液の固形分100重量部に対して、架橋剤としてTETRAD-C(三菱瓦斯化学社製)を固形分換算で6重量部を加えて、全体の固形分が20重量%となるように酢酸エチルで希釈し、ディスパーで攪拌し、アクリル系樹脂を含む粘着剤組成物(1)を得た。
攪拌羽根、温度計、窒素ガス導入管、冷却器を備えた四つ口フラスコに2-エチルヘキシルアクリレート(日本触媒社製)100重量部、2-ヒドロキシエチルアクリレート(東亜合成社製)4重量部、重合開始剤として2,2’-アゾビスイソブチロニトリル(和光純薬工業社製)0.2重量部、酢酸エチル156重量部を仕込み、緩やかに攪拌しながら窒素ガスを導入し、フラスコ内の液温を65℃付近に保って8時間重合反応を行い、重量平均分子量55万の(メタ)アクリル系重合体(2)溶液(40重量%)を調製した。(メタ)アクリル系重合体(2)溶液に、(メタ)アクリル系重合体(2)溶液の固形分100重量部に対して、架橋剤としてコロネートHX(東ソー社製)を固形分換算で4重量部、架橋触媒としてエンビライザーOL-1(東京ファインケミカル社製)を固形分換算で0.01重量部を加えて、全体の固形分が25重量%となるように酢酸エチルで希釈し、ディスパーで攪拌し、アクリル系樹脂を含む粘着剤組成物(2)を得た。
架橋触媒としてエンビライザーOL-1の使用量を固形分換算で0.05重量部とする以外は、製造例2と同じ手順によって、アクリル系樹脂を含む粘着剤組成物(3)を得た。
攪拌羽根、温度計、窒素ガス導入管、冷却器を備えた四つ口フラスコに2-エチルヘキシルアクリレート(日本触媒社製)100重量部、酢酸ビニルモノマー(昭和電工社製)80重量部、アクリル酸(東亞合成社製)5重量部、トルエン45重量部を仕込み、緩やかに攪拌しながら窒素ガスを導入し、重合開始剤としてナイパーBW(日油社製)0.2重量部、フラスコ内の液温を40℃付近に保って3時間重合反応を行い、重量平均分子量70万の(メタ)アクリル系重合体(4)溶液(35重量%)を調製した。(メタ)アクリル系重合体(4)溶液に、(メタ)アクリル系重合体(4)溶液の固形分100重量部に対して、架橋剤としてTETRAD-C(三菱瓦斯化学社製)を固形分換算で10重量部を加えて、全体の固形分が20重量%となるようにメチルエチルケトンで希釈し、ディスパーで攪拌し、アクリル系樹脂を含む粘着剤組成物(4)を得た。
多官能ポリオールとして、プレミノールS3011(旭硝子株式会社製、Mn=10000)を固形分換算で100重量部、架橋剤としてコロネートHX(日本ポリウレタン工業社製)を固形分換算で18重量部、架橋触媒としてナーセム第2鉄(日本化学産業社製)を固形分換算で0.04重量部、劣化防止剤としてIrganox1010(BASF社製)を固形分換算で0.5重量部を加えて、全体の固形分が35重量%となるように酢酸エチルで希釈し、ディスパーで攪拌し、ウレタン系樹脂を含む粘着剤組成物(5)を得た。
架橋剤としてTETRAD-C(三菱瓦斯化学社製)の使用量を固形分換算で0.07重量部とする以外は、製造例1と同じ手順によって、アクリル系樹脂を含む粘着剤組成物(6)を得た。
製造例6で得られた粘着剤組成物(6)を、ポリエステル樹脂からなる基材「ルミラーS10」(厚み75μm、東レ社製)にファウンテンロールで乾燥後の厚みが15μmとなるよう塗布し、乾燥温度130℃、乾燥時間2分の条件でキュアーして乾燥した。このようにして、基材上に粘着剤層を作製した。次いで、粘着剤層の表面に、一方の面にシリコーン処理を施した厚さ75μmのポリエステル樹脂「ルミラーS10」(厚み75μm、東レ社製)からなる基材のシリコーン処理面を貼合せて、樹脂フィルム(シリコーン処理面付)/粘着剤層/樹脂フィルムの構成の積層体(A)を得た。
製造例1で得られた粘着剤組成物(1)を、ポリエステル樹脂からなる基材「ルミラーS10」(厚み38μm、東レ社製)にファウンテンロールで乾燥後の厚みが5μmとなるよう塗布し、乾燥温度130℃、乾燥時間30秒の条件でキュアーして乾燥した。このようにして、基材上に粘着剤層を作製した。次いで、粘着剤層の表面に、一方の面にシリコーン処理を施した厚さ25μmのポリエステル樹脂からなる基材のシリコーン処理面を貼合せて、セパレータ/粘着剤層/樹脂フィルムの構成の積層体(B1)を得た。
ポリエステル樹脂からなる基材「ルミラーS10」(厚み38μm、東レ社製)を「ルミラーS10」(厚み50μm、東レ社製)に変更した以外は、製造例8と同様の手順により、セパレータ/粘着剤層/樹脂フィルムの構成の積層体(B2)を得た。
ポリエステル樹脂からなる基材「ルミラーS10」(厚み38μm、東レ社製)を基材「ルミラーS10」(厚み75μm、東レ社製)に変更し、粘着剤層の厚みを15μmに変更した以外は、製造例8と同じ手順により、セパレータ/粘着剤層/樹脂フィルムの構成の積層体(B3)を得た。
製造例2で得られた粘着剤組成物(2)を、ポリエステル樹脂からなる基材「ルミラーS10」(厚み38μm、東レ社製)にファウンテンロールで乾燥後の厚みが20μmとなるよう塗布し、乾燥温度130℃、乾燥時間30秒の条件でキュアーして乾燥した。このようにして、基材上に粘着剤層を作製した。次いで、粘着剤層の表面に、一方の面にシリコーン処理を施した厚さ25μmのポリエステル樹脂からなる基材のシリコーン処理面を貼合せて、セパレータ/粘着剤層/樹脂フィルムの構成の積層体(B4)を得た。
製造例3で得られた粘着剤組成物(3)を、ポリエステル樹脂からなる基材「ルミラーS10」(厚み38μm、東レ社製)にファウンテンロールで乾燥後の厚みが20μmとなるよう塗布し、乾燥温度130℃、乾燥時間30秒の条件でキュアーして乾燥した。このようにして、基材上に粘着剤層を作製した。次いで、粘着剤層の表面に、一方の面にシリコーン処理を施した厚さ25μmのポリエステル樹脂からなる基材のシリコーン処理面を貼合せて、セパレータ/粘着剤層/樹脂フィルムの構成の積層体(B5)を得た。
製造例4で得られた粘着剤組成物(4)を、ポリエステル樹脂からなる基材「ルミラーS10」(厚み38μm、東レ社製)にファウンテンロールで乾燥後の厚みが20μmとなるよう塗布し、乾燥温度130℃、乾燥時間30秒の条件でキュアーして乾燥した。このようにして、基材上に粘着剤層を作製した。次いで、粘着剤層の表面に、一方の面にシリコーン処理を施した厚さ25μmのポリエステル樹脂からなる基材のシリコーン処理面を貼合せて、セパレータ/粘着剤層/樹脂フィルムの構成の積層体(B6)を得た。
製造例5で得られた粘着剤組成物(5)を、ポリエステル樹脂からなる基材「ルミラーS10」(厚み38μm、東レ社製)にファウンテンロールで乾燥後の厚みが12μmとなるよう塗布し、乾燥温度130℃、乾燥時間30sの条件でキュアーして乾燥した。このようにして、基材上に粘着剤層を作製した。次いで、粘着剤層の表面に、一方の面にシリコーン処理を施した厚さ25μmのポリエステル樹脂からなる基材のシリコーン処理面を貼合せて、セパレータ/粘着剤層/樹脂フィルムの構成の積層体(B7)を得た。
製造例8で得られた積層体(B1)からセパレータを剥離し、露出した粘着剤層に、製造例7で得られた積層体(A)の樹脂フィルム(シリコーン処理がされていない樹脂フィルム)側を貼り付け、積層体(1)を得た。結果を表1に示した。
製造例9で得られた積層体(B2)からセパレータを剥離し、露出した粘着剤層に、製造例7で得られた積層体(A)の樹脂フィルム(シリコーン処理がされていない樹脂フィルム)側を貼り付け、積層体(2)を得た。結果を表1に示した。
製造例10で得られた積層体(B3)からセパレータを剥離し、露出した粘着剤層に、製造例7で得られた積層体(A)の樹脂フィルム(シリコーン処理がされていない樹脂フィルム)側を貼り付け、積層体(3)を得た。結果を表1に示した。
製造例11で得られた積層体(B4)からセパレータを剥離し、露出した粘着剤層に、製造例7で得られた積層体(A)の樹脂フィルム(シリコーン処理がされていない樹脂フィルム)側を貼り付け、積層体(4)を得た。結果を表1に示した。
製造例12で得られた積層体(B5)からセパレータを剥離し、露出した粘着剤層に、製造例7で得られた積層体(A)の樹脂フィルム(シリコーン処理がされていない樹脂フィルム)側を貼り付け、積層体(5)を得た。結果を表1に示した。
製造例13で得られた積層体(B6)からセパレータを剥離し、露出した粘着剤層に、製造例7で得られた積層体(A)の樹脂フィルム(シリコーン処理がされていない樹脂フィルム)側を貼り付け、積層体(6)を得た。結果を表1に示した。
製造例14で得られた積層体(B7)からセパレータを剥離し、露出した粘着剤層に、製造例7で得られた積層体(A)の樹脂フィルム(シリコーン処理がされていない樹脂フィルム)側を貼り付け、積層体(C1)を得た。結果を表1に示した。
粘着剤層(1) 20
樹脂フィルム(2) 30
粘着剤層(2) 40
樹脂フィルム(3) 50
積層体 100
Claims (3)
- 樹脂フィルム(1)、粘着剤層(1)、樹脂フィルム(2)、粘着剤層(2)、樹脂フィルム(3)をこの順に有する、5層以上の積層体であって、
該樹脂フィルム(2)と該粘着剤層(2)が直接に積層されてなり、
該樹脂フィルム(1)はセパレータであり、
該粘着剤層(2)と該樹脂フィルム(3)が直接に積層され、該粘着剤層(2)と該樹脂フィルム(3)の積層体部分がキャリアシートであり、
該粘着剤層(1)はアクリル系粘着剤から構成され、
該粘着剤層(2)はアクリル系粘着剤から構成され、該アクリル系粘着剤はアクリル系粘着剤組成物から形成され、該アクリル系粘着剤組成物は、アクリル系ポリマーと架橋剤を含み、該アクリル系ポリマーは、(a成分)アルキルエステル部分のアルキル基の炭素数が4~12である(メタ)アクリル酸アルキルエステル、(b成分)OH基を有する(メタ)アクリル酸エステルおよび(メタ)アクリル酸からなる群から選ばれる少なくとも1種、を含む組成物(B)から重合によって形成され、該アクリル系ポリマーを構成するモノマー成分全量に対する該a成分の含有量が50重量%~99重量%であり、該アクリル系ポリマーを構成するモノマー成分全量に対する該b成分の含有量が1重量%~30重量%であり、
該樹脂フィルム(2)は、ポリエステル系樹脂から構成されるプラスチックフィルムであり、
温度23℃、湿度50%RHの雰囲気下における、剥離角度180度、剥離速度30mm/分で該粘着剤層(2)を該樹脂フィルム(2)から剥離するときの粘着力が1gf/25mm~7gf/25mmである、
積層体。 - 温度23℃、湿度50%RHの雰囲気下における、剥離角度180度、剥離速度300mm/分で該粘着剤層(2)を該樹脂フィルム(2)から剥離するときの粘着力が2gf/25mm~10gf/25mmである、請求項1に記載の積層体。
- 温度23℃、湿度50%RHの雰囲気下における、剥離角度180度、剥離速度2400mm/分で該粘着剤層(2)を該樹脂フィルム(2)から剥離するときの粘着力が5gf/25mm~40gf/25mmである、請求項1または2に記載の積層体。
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