JP7193405B2 - 身体洗浄剤組成物 - Google Patents
身体洗浄剤組成物 Download PDFInfo
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- JP7193405B2 JP7193405B2 JP2019070058A JP2019070058A JP7193405B2 JP 7193405 B2 JP7193405 B2 JP 7193405B2 JP 2019070058 A JP2019070058 A JP 2019070058A JP 2019070058 A JP2019070058 A JP 2019070058A JP 7193405 B2 JP7193405 B2 JP 7193405B2
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- oil
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- Cosmetics (AREA)
Description
一方で、低温安定性を向上させる方法として、トリエタノールアミンを対イオンとして使用した洗浄剤に関しても知られている(特許文献1~6)。しかしながら、トリエタノールアミン塩では起泡力が劣り、色相安定性も悪いといった欠点がある。また、トリエタノールアミンを対イオンとすることでナトリウム塩、カリウム塩よりも低温安定性は良くなるが、十分ではない。
脂肪酸トリエタノールアミン塩を使用したパーソナルクレンジング組成物の泡立ち性を改善するために、ベタイン型界面活性剤(特許文献1)、脂肪酸N-メチルタウリン塩(特許文献5)等を併用する方法が提案されている。しかしながら、これらの方法では、起泡力の向上効果又は泡保持性が不十分であったり、ヌメリ感が生じたりするという問題がある。
成分(a):炭素数14~18の高級脂肪酸と下記一般式(1)のアルカノールアミンとの中和塩5~25重量%を含むことを特徴とする身体洗浄剤組成物に関する。
本発明の身体洗浄剤組成物のa成分は、高級脂肪酸のアルカノールアミン塩である。起泡力、色相安定性、低温安定性、泡弾力の要となる、本発明の身体洗浄剤組成物の主剤である。高級脂肪酸として、炭素数14~18の飽和、不飽和、直鎖、分岐の高級脂肪酸、これらの高級脂肪酸の混合物を使用することができ、炭素数14~18の直鎖高級脂肪酸が好ましく、炭素数14のミリスチン酸と、炭素数16パルミチン酸が特に好ましい。炭素数が13以下では皮膚への刺激性の点で問題があり、炭素数が19以上では起泡力の点で問題がある。
スクワラン、流動パラフィン、ワセリン、セレシン、マイクロクリスタリンワックス、イソパラフィン等の炭化水素類、カルナバウロウ、パラフィンワックス、鯨ロウ、ミツロウ、キャンデリラワックス、ラノリン等のワックス類、
l-メントール、ハッカ油等の冷感剤、レチノール、レチノール誘導体等の創傷治癒剤、
香料等を配合することができる。
N-メチルエタノールアミンのプロピレンオキサイド1モル付加物の製造
1リットルのオートクレーブにN-メチルエタノールアミン(1.0モル、東京化成工業製)を仕込み、窒素置換、昇温後に95~105℃でプロピレンオキサイド付加(1.0モル、東京化成工業製)を実施した。プロピレンオキサイド導入後1時間の熟成を行い、目的物を取り上げた。
1H-NMRより構造を決定した。δ=1.1ppm(3H,d),2.3ppm(5H,m),2.5ppm(1H,m),2.6ppm(1H,m),3.6ppm(2H,m),3.8ppm(1H,m).
ミリスチン酸 花王製 ルナック(登録商標)MY-98
パルミチン酸 花王製 ルナックP-95
トリエタノールアミン 東京化成工業製
ミリスチン酸ナトリウム塩 東京化成工業製
ミリスチン酸カリウム塩 富士フィルムワコーケミカル製
ロス・マイルス試験法JIS K 3362に基づき、試料濃度0.25重量%の水溶液を、40℃にて起泡力を測定した。
4段階判定基準
◎:非常に良好(200mm以上)
○:良好(150mm以上200mm未満)
△:やや劣る(100mm以上150mm未満)
×:不良(100mm未満)
洗浄剤組成物を80℃の恒温槽に1週間保存して、色相の変化を目視により観察して評価した。
◎:非常に良好(色相の変化がほとんどない)
○:良好(色相の変化がわずかにある)
△:やや劣る(色相の変化がある)
×:不良(色相の変化がかなりある)
洗浄剤組成物を-10℃で凍結させたものを徐々に温度を上げ、その外観を目視により観察して透明となる温度を測定した。評価基準は下記の通りである。
◎:非常に良好(20℃未満)
〇:良好(20℃以上40℃未満)
△:やや劣る(40℃以上50℃未満)
×:不良(50℃以上)
各洗浄剤組成物につき、男女5名、計10名の専門パネラーを用いて、手洗い試験で泡の弾力を評価した。手洗い試験は、洗浄剤組成物0.5mLを手に取り、水道水で行った。なお、評価基準は下記の通りである。
◎:非常に良好(泡の弾力がかなりあり、クリーミーな泡質で、10人中8~10名が良いと答えた)
○:良好(泡の弾力がややあり、10人中6~7名が良いと答えた)
△:やや劣る(泡の弾力がわずかにあり、10人中3~5名が良いと答えた)
×:不良(泡の弾力がなく、泡質が水っぽく、10人中0~2名が良いと答えた
本発明の範囲外となる比較例4の身体洗浄剤組成物は、起泡力が低く、実使用には耐えないものであった。また、比較例5の身体洗浄剤組成物は、低温安定性が悪く、実使用には耐えないものであった。
ボディソープ
ミリスチン酸と製造例1のアルカノールアミンの中和塩 8重量%
パルミチン酸と製造例1のアルカノールアミンの中和塩 1重量%
ココイルグルタミン酸(*1)とN-メチルジエタノールアミンの中和塩 4重量%
ラウロアンホ酢酸Na(*2) 4重量%
ヒドロキシプロピルメチルセルロース(*3) 0.5重量%
水 バランス
性能評価結果は、起泡力試験◎、色相安定性◎、低温安定性◎、泡弾力評価◎であった。
ボディソープ
ミリスチン酸と製造例1のアルカノールアミンの中和塩 19重量%
パルミチン酸と製造例1のアルカノールアミンの中和塩 3重量%
オレイン酸と製造例1のアルカノールアミンの中和塩 1重量%
ラウロイルグルタミン酸(*4)と製造例1のアルカノールアミンの中和塩 1重量%
ラウラミドプロピルヒドロキシスルタイン(*5) 5重量%
ヒドロキシプロピルメチルセルロース 0.3重量%
水 バランス
性能評価結果は、起泡力試験〇、色相安定性◎、低温安定性〇、泡弾力評価◎であった。
ボディソープ
ミリスチン酸と製造例1のアルカノールアミンの中和塩 23重量%
パルミチン酸と製造例1のアルカノールアミンの中和塩 2重量%
ラウロイルグルタミン酸と製造例1のアルカノールアミンの中和塩 1重量%
ラウラミドプロピルアミンオキシド(*6) 1重量%
PEG-2コカミン(*7) 2重量%
グリセリン(*8) 5重量%
ヒドロキシプロピルメチルセルロース 0.2重量%
EDTA・4ナトリウム(*9) 0.2重量%
メチルパラベン(*10) 0.2重量%
水 バランス
性能評価結果は、起泡力試験◎、色相安定性◎、低温安定性〇、泡弾力評価◎であった。
ハンドソープ
ミリスチン酸と製造例1のアルカノールアミンの中和塩 5重量%
ココイルグルタミン酸と製造例1のアルカノールアミンの中和塩 1重量%
ラウラミドプロピルアミンオキシド 3重量%
ココアンホ酢酸Na(*11) 12重量%
PEG-2カプリリルアミン(*12) 2重量%
グリセリン 3重量%
水 バランス
性能評価結果は、起泡力試験◎、色相安定性◎、低温安定性◎、泡弾力評価◎であった。
ボディシャンプー
ミリスチン酸と製造例1のアルカノールアミンの中和塩 18重量%
パルミチン酸と製造例1のアルカノールアミンの中和塩 2重量%
ラウレス-6カルボン酸(*13)と製造例1のアルカノールアミンの中和塩 9重量%
ラウロイルグルタミン酸と製造例1のアルカノールアミンの中和塩 1重量%
ヒドロキシアルキル(C12-14)ヒドロキシエチルサルコシン(*14) 1重量%
PPG-2コカミド(*15) 1重量%
ミリスチルアルコール(*16) 1重量%
ソルビトール(*17) 3重量%
ヒドロキシプロピルメチルセルロース 0.2重量%
水 バランス
性能評価結果は、起泡力試験◎、色相安定性◎、低温安定性◎、泡弾力評価◎であった。
(*2):ソフタゾリンLHL(川研ファインケミカル社製)
(*3):メトローズ(登録商標)60SH10000(信越化学工業社製)
(*4):アミソフトLA-D(味の素ヘルシーサプライ社製)
(*5):ソフタゾリンLSB(川研ファインケミカル社製)
(*6):ソフタゾリンLAO-C(川研ファインケミカル社製)
(*7):ビスコファインE2C(川研ファインケミカル社製)
(*8):グリセリン(東京化成工業社製)
(*9):キレスト(登録商標)2D-SD(丸善薬品産業社製)
(*10):メチルパラベン(東京化成工業社製)
(*11):ソフタゾリンCH(川研ファインケミカル社製)
(*12):フォーマイト2E8(川研ファインケミカル社製)
(*13):カオーアキポ(登録商標)RLM-45(花王社製)
(*14):ソフタゾリンLMEB(川研ファインケミカル社製)
(*15):アミゼット1PC(川研ファインケミカル社製)
(*16):カルコール(登録商標)4098(花王社製)
(*17):ソルビトール(東京化成工業社製)
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Citations (3)
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US20030013627A1 (en) | 2001-06-07 | 2003-01-16 | Kao Corporation | Esters derived from alkanolamines, dicarboxylic acids and fatty alvohols and the cationic surfactants obtainable therefrom |
US6653275B1 (en) | 1999-01-07 | 2003-11-25 | Goldschmidt Rewo Gmbh & Co. Kg | Clear softening agent formulations |
JP2004522866A (ja) | 2000-12-22 | 2004-07-29 | カオー コルポラティオン ソシエダッド アノニマ | ノニオン界面活性剤を含有する繊維柔軟剤組成物 |
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Publication number | Priority date | Publication date | Assignee | Title |
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US6653275B1 (en) | 1999-01-07 | 2003-11-25 | Goldschmidt Rewo Gmbh & Co. Kg | Clear softening agent formulations |
JP2004522866A (ja) | 2000-12-22 | 2004-07-29 | カオー コルポラティオン ソシエダッド アノニマ | ノニオン界面活性剤を含有する繊維柔軟剤組成物 |
US20030013627A1 (en) | 2001-06-07 | 2003-01-16 | Kao Corporation | Esters derived from alkanolamines, dicarboxylic acids and fatty alvohols and the cationic surfactants obtainable therefrom |
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