JP7090071B2 - 中気門亜目ダニ類の防除剤 - Google Patents
中気門亜目ダニ類の防除剤 Download PDFInfo
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- JP7090071B2 JP7090071B2 JP2019506293A JP2019506293A JP7090071B2 JP 7090071 B2 JP7090071 B2 JP 7090071B2 JP 2019506293 A JP2019506293 A JP 2019506293A JP 2019506293 A JP2019506293 A JP 2019506293A JP 7090071 B2 JP7090071 B2 JP 7090071B2
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
- A01N43/42—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings condensed with carbocyclic rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
- A01N37/22—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof the nitrogen atom being directly attached to an aromatic ring system, e.g. anilides
- A01N37/24—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof the nitrogen atom being directly attached to an aromatic ring system, e.g. anilides containing at least one oxygen or sulfur atom being directly attached to the same aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
- A01N37/50—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids the nitrogen atom being doubly bound to the carbon skeleton
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/24—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms
- A01N43/32—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms six-membered rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
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Description
で示される2,3-ジメチル-4-キノリノール誘導体は国際公開第01/92231号や特開2012-087090号公報にイネいもち病やチャ輪斑病に対する有用性が開示されているが、中気門亜目ダニ類に対する防除については何ら記載されていない。
本発明は、
[1]上記の一般式(1)で表される化合物、アゾキシストロビン、ピコキシストロビン、ピラクロストロビン、クレソキシムメチル、トリフロキシストロビン、メトミノストロビン、オリサストロビン、ファモキサスドン、フルオキサストロビン、ピリベンカルブ、シアゾファミド、アミスルブロム、フラトラニル、メプロニル、イソファタミド、フルオピラム、カルボキシン、チフルザミド、フルキサピロキサド、フラメトピル、ペンフルフェン、ペンチオピラド、ボスカリド、ジフルメトリム、フルアジナム、フェムリゾン、フェンピロキシメート、及びこれら化合物の酸付加塩からなる群から選択される少なくとも1種を有効成分として含有し、中気門亜目ダニ類(Mesostigmata)に対して防除効果を示す中気門亜目ダニ類防除剤。
[2]中気門亜目ダニ類がワクモ科のダニ類又はオオサシダニ科のダニ類である、[1]に記載の中気門亜目ダニ類防除剤。
[3]R1がアセチル基又はメトキシカルボニル基である一般式(1)で表される化合物、ピコキシストロビン、ピラクロストロビン、オリサストロビン、ファモキサスドン、アミスルブロム、ジフルメトリム、フルアジナム、フェンピロキシメート、及びこれら化合物の酸付加塩からなる群から選択される少なくとも1種を有効成分として含有する、[1]に記載の中気門亜目ダニ類防除剤。
[4][1]に記載の中気門亜目ダニ類防除剤を用いる、中気門亜目ダニ類を防除する方法。
[5]中気門亜目ダニ類防除剤の製造のための、上記一般式(1)で表される化合物、アゾキシストロビン、ピコキシストロビン、ピラクロストロビン、クレソキシムメチル、トリフロキシストロビン、メトミノストロビン、オリサストロビン、ファモキサスドン、フルオキサストロビン、ピリベンカルブ、シアゾファミド、アミスルブロム、フラトラニル、メプロニル、イソファタミド、フルオピラム、カルボキシン、チフルザミド、フルキサピロキサド、フラメトピル、ペンフルフェン、ペンチオピラド、ボスカリド、ジフルメトリム、フルアジナム、フェムリゾン、フェンピロキシメート、又はこれら化合物の酸付加塩の使用。
[6]上記一般式(1)で表される化合物、アゾキシストロビン、ピコキシストロビン、ピラクロストロビン、クレソキシムメチル、トリフロキシストロビン、メトミノストロビン、オリサストロビン、ファモキサスドン、フルオキサストロビン、ピリベンカルブ、シアゾファミド、アミスルブロム、フラトラニル、メプロニル、イソファタミド、フルオピラム、カルボキシン、チフルザミド、フルキサピロキサド、フラメトピル、ペンフルフェン、ペンチオピラド、ボスカリド、ジフルメトリム、フルアジナム、フェムリゾン、フェンピロキシメート、及びこれら化合物の酸付加塩からなる群から選択される少なくとも1種の有効量を、中気門亜目ダニ類、定温動物、昆虫、並びに、中気門亜目ダニ類、定温動物、又は昆虫の生息場所からなる群から選択される少なくとも1種に施用する中気門亜目ダニ類の防除方法。
[7]前記有効成分の有効量を中気門亜目ダニ類に直接噴霧する、[6]に記載の中気門亜目ダニ類の防除方法。
[8]前記有効成分の有効量を中気門亜目ダニ類が寄生する定温動物又は昆虫に噴霧する、[6]に記載の中気門亜目ダニ類の防除方法。
[9]前記有効成分の有効量を中気門亜目ダニ類の生息場所に噴霧する、[6]に記載の中気門亜目ダニ類の防除方法。
[10]前記有効成分の有効量を中気門亜目ダニ類が寄生する定温動物又は昆虫の生息場所に噴霧する、[6]に記載の中気門亜目ダニ類の防除方法。
modepside)、モネパンテル(monepantel)、フェンベンダゾール(fenbendazol)、フェバンテル(febantel)のようなベンズイミダゾール化合物;パモ酸ピランテル(pyrantel pamoate)、メタジアミド(meta-diamid)、ピリフルキナゾン(pyrifluquinazon)、クロラントラニリプロール(chlorantraniliprole)、シアントラニリプロール(cyantraniliprole)、スピロテトラマト(spirotetramat)、レピメクチン(lepimectin)、メタフルミゾン(metaflumizone)、ピラフルプロール(pyrafluprole)、ピリプロール(pyriprole)、ヒドラメチルノン(hydramethylnon)、トリアザメート(triazamate)、フロメトキン(flometoquin)、アフィドピロペン(afidopyropen)、フルララネル(fluralaner)、アフォキソラネル(afoxolaner)のようなイソキサゾリン化合物;トルトラズリル(toltrazuril)、スルファジメトキシン(sulfadimethoxine)のようなサルファ薬;クマテトラリル(coumatetralyl)のようなクマリン系化合物;N,N-ジエチル-m-トルアミド(DEET)、有機金属系化合物、ジニトロ系化合物、有機硫黄化合物、尿素系化合物、トリアジン系化合物、ヒドラジン系化合物、及び国際公開第12/029672号に記載の下記一般式(2)で表される化合物、及びこれらの動物薬上許容可能な酸付加塩が挙げられる。
本発明の化合物A20%、クレー40%、珪藻土32%、ホワイトカーボン2%、ラウリル硫酸ナトリウム1%、リグニンスルホン酸カルシウム5%を均一に混合粉砕して、水和剤とした。
本発明の化合物A20%、ナフタレンスルホン酸ホルマリン縮合物4%、プロピレングリコール5%、キサンタンガム0.05%、シリコーン消泡剤0.05%、水70.9%を加え均一に混合粉砕して、フロアブル剤とした。
本発明の化合物A20%、ポリオキシエチレントリスチリルフェニルエーテルサルフェート塩2%、プロピレングリコール5%、キサンタンガム0.2%、シリコーン消泡剤0.5%、リン酸3カルシウム0.5%、水71.8%を加え均一に混合粉砕して、フロアブル剤とした。
本発明の化合物A2%、クレー60%、タルク37%、ステアリン酸カルシウム1%を均一に混合して、粉剤を得た。
本発明の化合物A20%、N,N-ジメチルホルムアミド20%、キシレン50%、ポリオキシエテレンアルキルアリールエーテル10%を均一に混合して、溶解させ、乳剤を得た。
本発明の化合物A5%、ヘキシレングリコール50%、イソプロパノール45%を均一に混合して、経皮投与用液剤を得た。
本発明の化合物A2%、ジメチルスルホキシド10%、2-プロパノール35%、アセトン53%を均一に混合して、噴霧用液剤を得た。
本発明の化合物A2%、流動パラフィン98%を均一に混合して、(滴下)経皮投与用液剤を得た。
本発明の化合物A0.1gをネオチオゾールF(中央化成(株);ケロシン(ノルマルパラフィン)120ml、エタンガス180mlに混合して、エアゾール製剤を得た。
パスツールピペットの先端をパラフィルムで封印し、ピペット上部から所定濃度に希釈した下記表2に示す各サンプルのアセトン溶液(薬液)を流し込んだ。1分後に先端のパラフィルムを外して薬液を排出し、ピペットを風乾後、ピペット上端に脱脂綿を挿入し、ピペット内にワクモ(Dermanyssus gallinae)未吸血成ダニ20頭を放飼した。先端をヘマトシールで封印後、ピペットを暗黒下、温度27~28℃・湿度50~60%のインキュベーターで保存した。処理24、48、72時間後に実体顕微鏡下でダニを観察し、生死及び苦悶を判定し、次式に従って死苦悶虫率(%)を算出した。対照薬として、スピノサド、トリクロルホン、ペルメトリンを用いた。
死苦悶虫率(%)={(死亡虫数+苦悶虫数)/(生存虫数+苦悶虫数+死亡虫数)}×100
その結果を以下に示す。
ワクモ(Dermanyssus gallinae)未吸血成ダニ約50匹をトールビーカー(直径8cm×高さ15cm)に入れ、18メッシュナイロンネットで蓋をした。本発明の製剤例3のフロアブル剤を所定濃度に蒸留水で希釈した薬液2.5mLを15cmの高さからスプレーガンで噴霧した。噴霧後のビーカーは、温度27~28℃・湿度50~60%でインキュベートした。処理24時間後に実体顕微鏡下でダニを観察し、生死を判定し、次式に従って死虫率(%)を算出した。また、対照剤としてプロポクスル50%製剤を、陰性対照として蒸留水を、それぞれ用いた。
死虫率(%)={死亡虫数/(生存虫数+死亡虫数)}×100
その結果を以下に示す。
パスツールピペットの先端をパラフィルムで封印し、ピペット上部から所定濃度に希釈した下記表4に示す各サンプルのアセトン溶液(薬液)を流し込んだ。1分後に先端のパラフィルムを外して薬液を排出し、ピペットを風乾後、ピペット上端に脱脂綿を挿入し、ピペット内にトリサシダニ(Ornithonyssus sylviarum)吸血成ダニ10頭を放飼した。先端をヘマトシールで封印後、暗黒下、25℃・湿度80%のインキュベーターで保存した。処理2、24時間後に実体顕微鏡下でダニを観察し、生死及び苦悶を判定し、死苦悶虫率(%)を算出した。
死苦悶虫率(%)={(死亡虫数+苦悶虫数)/(生存虫数+苦悶虫数+死亡虫数)}×100
その結果を以下に示す。
パスツールピペットの先端をパラフィルムで封印し、ピペット上部から所定濃度に希釈した下記表5に示す各サンプルのアセトン溶液(薬液)を流し込んだ。1分後に先端のパラフィルムを外して薬液を排出し、ピペットを風乾後、ピペット上端に脱脂綿を挿入し、ピペット内にワクモ(Dermanyssus gallinae)未吸血成ダニ20頭を放飼した。先端をヘマトシールで封印後、ピペットを暗黒下、温度25~28℃・湿度40~60%のインキュベーターで保存した。処理24時間後にダニを観察し、生死及び苦悶を判定し、次式に従って死苦悶虫率(%)を算出した。対照薬として、アセキノシル、フルアクリピリムを用いた。
死苦悶虫率(%)={(死亡虫数+苦悶虫数)/(生存虫数+苦悶虫数+死亡虫数)}×100
その結果を以下に示す。
Claims (10)
- 中気門亜目ダニ類がワクモ科のダニ類又はオオサシダニ科のダニ類である、請求項1に記載の中気門亜目ダニ類防除剤。
- R1がアセチル基又はメトキシカルボニル基である一般式(1)で表される化合物及びその酸付加塩からなる群から選択される少なくとも1種を有効成分として含有する、請求項1に記載の中気門亜目ダニ類防除剤。
- 請求項1に記載の中気門亜目ダニ類防除剤を用いる、中気門亜目ダニ類を防除する方法(ただし人間を適用対象とするものを除く)。
- 前記有効成分の有効量を中気門亜目ダニ類に直接噴霧する、請求項6に記載の中気門亜目ダニ類の防除方法。
- 前記有効成分の有効量を中気門亜目ダニ類が寄生する定温動物(ただし人間を除く)又は昆虫に噴霧する、請求項6に記載の中気門亜目ダニ類の防除方法。
- 前記有効成分の有効量を中気門亜目ダニ類の生息場所に噴霧する、請求項6に記載の中気門亜目ダニ類の防除方法。
- 前記有効成分の有効量を中気門亜目ダニ類が寄生する定温動物又は昆虫の生息場所に噴霧する、請求項6に記載の中気門亜目ダニ類の防除方法。
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PCT/JP2018/010445 WO2018169045A1 (ja) | 2017-03-17 | 2018-03-16 | 中気門亜目ダニ類の防除剤 |
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JPWO2020054835A1 (ja) * | 2018-09-14 | 2021-08-30 | Meiji Seikaファルマ株式会社 | 中気門亜目ダニ類の防除用組成物 |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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JPWO2020054835A1 (ja) * | 2018-09-14 | 2021-08-30 | Meiji Seikaファルマ株式会社 | 中気門亜目ダニ類の防除用組成物 |
JP7389750B2 (ja) | 2018-09-14 | 2023-11-30 | Meiji Seikaファルマ株式会社 | 中気門亜目ダニ類の防除用組成物 |
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EP3597041A4 (en) | 2021-03-24 |
MX2019010886A (es) | 2019-10-15 |
EP3597041A1 (en) | 2020-01-22 |
KR20190137782A (ko) | 2019-12-11 |
JPWO2018169045A1 (ja) | 2020-01-16 |
AU2018234204A1 (en) | 2019-09-19 |
AU2018234204B2 (en) | 2023-07-27 |
KR102490180B1 (ko) | 2023-01-18 |
CA3054540A1 (en) | 2018-09-20 |
WO2018169045A1 (ja) | 2018-09-20 |
BR112019018020A2 (pt) | 2020-04-28 |
US20220312766A1 (en) | 2022-10-06 |
US20200037611A1 (en) | 2020-02-06 |
CN110418575A (zh) | 2019-11-05 |
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