JP6903123B2 - ガラス板用合紙及びその製造方法 - Google Patents
ガラス板用合紙及びその製造方法 Download PDFInfo
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- JP6903123B2 JP6903123B2 JP2019510107A JP2019510107A JP6903123B2 JP 6903123 B2 JP6903123 B2 JP 6903123B2 JP 2019510107 A JP2019510107 A JP 2019510107A JP 2019510107 A JP2019510107 A JP 2019510107A JP 6903123 B2 JP6903123 B2 JP 6903123B2
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- UQEAIHBTYFGYIE-UHFFFAOYSA-N hexamethyldisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)C UQEAIHBTYFGYIE-UHFFFAOYSA-N 0.000 description 1
- 125000004836 hexamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 description 1
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- VERNMKKMBJGSQB-UHFFFAOYSA-N octamethyltetrasiloxane-1,7-diol Chemical compound C[Si](C)(O)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O VERNMKKMBJGSQB-UHFFFAOYSA-N 0.000 description 1
- CXQXSVUQTKDNFP-UHFFFAOYSA-N octamethyltrisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)O[Si](C)(C)C CXQXSVUQTKDNFP-UHFFFAOYSA-N 0.000 description 1
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- 239000000312 peanut oil Substances 0.000 description 1
- 125000004817 pentamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 description 1
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- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
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- LINXHFKHZLOLEI-UHFFFAOYSA-N trimethyl-[phenyl-bis(trimethylsilyloxy)silyl]oxysilane Chemical compound C[Si](C)(C)O[Si](O[Si](C)(C)C)(O[Si](C)(C)C)C1=CC=CC=C1 LINXHFKHZLOLEI-UHFFFAOYSA-N 0.000 description 1
- SVTUWEUXLNHYPF-UHFFFAOYSA-N trimethyl-[propyl-bis(trimethylsilyloxy)silyl]oxysilane Chemical compound CCC[Si](O[Si](C)(C)C)(O[Si](C)(C)C)O[Si](C)(C)C SVTUWEUXLNHYPF-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D57/00—Internal frames or supports for flexible articles, e.g. stiffeners; Separators for articles packaged in stacks or groups, e.g. for preventing adhesion of sticky articles
- B65D57/002—Separators for articles packaged in stacks or groups, e.g. stacked or nested
- B65D57/003—Separators for articles packaged in stacks or groups, e.g. stacked or nested for horizontally placed articles, i.e. for stacked or nested articles
- B65D57/004—Separators for articles packaged in stacks or groups, e.g. stacked or nested for horizontally placed articles, i.e. for stacked or nested articles the articles being substantially flat panels, e.g. wooden planks
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B17/00—Layered products essentially comprising sheet glass, or glass, slag, or like fibres
- B32B17/06—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
- B32B17/065—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of paper or cardboard
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D85/00—Containers, packaging elements or packages, specially adapted for particular articles or materials
- B65D85/30—Containers, packaging elements or packages, specially adapted for particular articles or materials for articles particularly sensitive to damage by shock or pressure
- B65D85/48—Containers, packaging elements or packages, specially adapted for particular articles or materials for articles particularly sensitive to damage by shock or pressure for glass sheets
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B40/00—Preventing adhesion between glass and glass or between glass and the means used to shape it, hold it or support it
- C03B40/02—Preventing adhesion between glass and glass or between glass and the means used to shape it, hold it or support it by lubrication; Use of materials as release or lubricating compositions
- C03B40/033—Means for preventing adhesion between glass and glass
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21F—PAPER-MAKING MACHINES; METHODS OF PRODUCING PAPER THEREON
- D21F11/00—Processes for making continuous lengths of paper, or of cardboard, or of wet web for fibre board production, on paper-making machines
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/33—Synthetic macromolecular compounds
- D21H17/46—Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D21H17/59—Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
- D21H27/30—Multi-ply
-
- G—PHYSICS
- G02—OPTICS
- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
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Description
木材パルプのスラリーを調製するスラリー調製工程、
前記スラリーをシート状とするシート形成工程、
前記シートを脱水して湿紙を形成する湿紙調製工程、
前記湿紙を乾燥して前記合紙を得る乾燥工程
を少なくとも含み、
前記湿紙調製工程において脱水を前記シートの両面から行う、製造方法に関する。
R1 3SiO−(R1 2SiO)a−SiR1 3 (1)
R1 (4−c)Si(OSiR1 3)c (3)
(式中、
R1は、それぞれ独立して、水素原子、水酸基、或いは、置換若しくは非置換の一価炭化水素基、アルコキシ基で示される基から選択される基であり、
aは、0〜1000の整数であり、
bは3〜100の整数であり、
cは1〜4の整数、好ましくは2〜4の整数である)
で表されるオルガノポリシロキサンが挙げられる。
R2 3SiO−(R1 2SiO)d−(R1ASiO)e−SiR2 3 (4)
(式中、
R1は、それぞれ独立して、上記と同様であり、
R2は、それぞれ独立して、R1又はAであり、
Aは、それぞれ独立して、R3Gで表される基であり、R3は、置換若しくは非置換の二価炭化水素基であり、Gはエチレンオキサイド、プロピレンオキサイド等の炭素数2〜5のアルキレンオキサイドを少なくとも1種含有してなるポリオキシアルキレン基を表し、
dは1〜500の整数を表し、
eは1〜50の整数を表す)。
xは20〜160であり、yは1〜25であり、x/yの値は50〜2であり、
Aは、例えば−(CH2)3O−(CH2CH2O)m−(CH2CH2CH2O)n−R4であり、mは7〜40、nは0〜40、m+nの値は少なくとも1であり、グラフト重合されたものでもランダム重合されたものでもよく、R4は水素原子又は上記置換若しくは非置換の一価炭化水素基を表す。好適には、mは7〜30、nは0〜30である)
なお、ここでの「平均繊維径」とは、ガラス板用合紙の表面の複数箇所を電子顕微鏡によって拡大観察し、各電子顕微鏡画像中から所定数の繊維を無作為に選別し、選別された当該繊維の径を測定し平均して得られた平均繊維径を意味する。選別される繊維の数は100以上であり、150以上が好ましく、200以上がより好ましく、300以上が更により好ましい。
木材パルプのスラリーを調製するスラリー調製工程、
前記スラリーをシート状とするシート形成工程、
前記シートを脱水して湿紙を形成する湿紙調製工程、
前記湿紙を乾燥して前記合紙を得る乾燥工程
を少なくとも含み、
前記湿紙調製工程において脱水をシート状スラリーの両面から行う、製造方法である。
ガラス板用合紙を1m2にカットし、紙の一方の面を脱金属イオン水で充分に洗浄した。洗浄後の水溶液を回収し、ポリカーボネート製メンブランフィルター(MILLIPORE、ポアサイズ0.8μm)で濾過し、残渣を得た。この残渣を電子顕微鏡を用いて観察し、粒子径1μm以上の異物をEDS分析することで、ガラス合紙の表面のタルクの個数を測定した。
アルミ製で75度の角度がつけられたL 字架台上のガラス載置面に発泡ウレタンを敷き、ガラス板を垂直方向に載置するための載置面と、載置面の後端部から垂直方向に延びる背もたれ面に向けて、サイズ680mm×880mm×0.7mmのガラス板120枚と各ガラス板の間にガラス板用合紙を挿入して、背もたれ面に平行となるように立てかけ、架台に固定された帯状のベルトを後端部から背もたれ面へ全周にわたり掛け渡してガラス板を固定した。上記のようにセットされた架台は、外部からの埃や塵等の混入を防ぐため包装資材で全面を被覆した。その後、トラックでの輸送テストを実施した。輸送テスト条件は、輸送距離1000km(輸送途中に40℃×95%RHの環境下に5日間保管)でテストを実施した。
蒸解工程と、洗浄工程と、酸素脱リグニン反応工程と、二酸化塩素及び過酸化水素による多段晒漂白工程とからなる針葉樹晒クラフトパルプの製造装置において、洗浄工程中に使用されるピッチコントロール剤として非タルク系界面活性剤「ミラクルピチコン500」(片山ナルコ社製)を用いた。このようにして、製造工程中で非タルク系界面活性剤を使用した針葉樹晒クラフトパルプを得た。これを100質量部用意し、これを離解して叩解度を550mlc.s.f.に調製したスラリーに紙力増強剤としてポリアクリルアミド(商品名:ポリストロン1250、荒川化学工業社製)を全パルプ質量に対して0.2質量部添加し、0.4重量%濃度のパルプスラリーを調成した。これを、ワイヤーパートにオントップフォーマを備えた長網抄紙機を用いて抄紙し、オントップフォーマによって湿紙の両面から脱水して、坪量55g/m2のガラス板用合紙を得た。
オントップフォーマを使用しない以外は実施例1と同様の手法で坪量55g/m2のガラス板用合紙を得た。
また、界面活性剤としてタルク系ピッチコントロール剤「MISTRON VAPOR」(日本ミストロン社製)を使用した以外は実施例1と同様の手法で、坪量55g/m2のガラス板用合紙を得た。
Claims (15)
- 木材パルプを原料とするガラス板用合紙であって、
一方の表面におけるタルクの存在割合が10個/100m2以下であり、
一方の表面上のタルクの存在割合と他方の表面上のタルクの存在割合との差が5個/100m2以内である、ガラス板用合紙。 - 前記タルクの平均粒径が1〜10μmである、請求項1記載のガラス板用合紙。
- 前記タルクが疎水性物質と複合化している、請求項1又は2に記載のガラス板用合紙。
- 前記タルクと前記疎水性物質との複合化した形態の平均粒径が30μm以上である、請求項3記載のガラス板用合紙。
- 前記疎水性物質がシリコーンを含む、請求項4記載のガラス板用合紙。
- 厚みが20〜200μmである、請求項1〜5のいずれかに記載のガラス板用合紙。
- KES法による表面の摩擦係数の平均偏差(MMD)が0.022以下である、請求項1〜6のいずれかに記載のガラス板用合紙。
- 前記ガラス板がディスプレイ用である、請求項1〜7のいずれかに記載のガラス板用合紙。
- 前記ディスプレイがTFT液晶ディスプレイ又は有機ELディスプレイである、請求項8記載のガラス板用合紙。
- 請求項1〜9のいずれかに記載のガラス板用合紙及びガラス板からなる積層体。
- 請求項1〜9のいずれかに記載のガラス板用合紙をガラス板間に配置する工程を含む、ガラス板の保護方法。
- 請求項1〜9のいずれかに記載のガラス板用合紙の製造方法であって、
木材パルプのスラリーを調製するスラリー調製工程、
前記スラリーをシート状とするシート形成工程、
前記シートを脱水して湿紙を形成する湿紙調製工程、
前記湿紙を乾燥して前記合紙を得る乾燥工程
を少なくとも含み、
前記湿紙調製工程において脱水を前記シートの両面から行う、製造方法。 - 前記脱水を吸引により行う、請求項12記載の製造方法。
- 前記シートの一方の表面における前記吸引の脱水割合と他方の表面における前記吸引の脱水割合との差が該他方の表面における前記吸引の脱水割合の10%以下である、請求項13記載の製造方法。
- 前記乾燥工程後の合紙の両面を更に吸引する追加吸引工程を含む、請求項13又は14に記載の製造方法。
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