JP6831410B2 - ポリマーを含んでなる粒子を含有する分散物および組成物 - Google Patents
ポリマーを含んでなる粒子を含有する分散物および組成物 Download PDFInfo
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- JP6831410B2 JP6831410B2 JP2019039952A JP2019039952A JP6831410B2 JP 6831410 B2 JP6831410 B2 JP 6831410B2 JP 2019039952 A JP2019039952 A JP 2019039952A JP 2019039952 A JP2019039952 A JP 2019039952A JP 6831410 B2 JP6831410 B2 JP 6831410B2
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- Prior art keywords
- styrene
- aqueous dispersion
- wax
- hair
- oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 229920001281 polyalkylene Polymers 0.000 description 1
- 150000004291 polyenes Chemical class 0.000 description 1
- 229940100518 polyglyceryl-4 isostearate Drugs 0.000 description 1
- 229920002959 polymer blend Polymers 0.000 description 1
- 229940068965 polysorbates Drugs 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 239000011164 primary particle Substances 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- AAYRWMCIKCRHIN-UHFFFAOYSA-N propane-1-sulfonic acid;prop-2-enamide Chemical compound NC(=O)C=C.CCCS(O)(=O)=O AAYRWMCIKCRHIN-UHFFFAOYSA-N 0.000 description 1
- 229920001384 propylene homopolymer Polymers 0.000 description 1
- 239000011253 protective coating Substances 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- JEXVQSWXXUJEMA-UHFFFAOYSA-N pyrazol-3-one Chemical compound O=C1C=CN=N1 JEXVQSWXXUJEMA-UHFFFAOYSA-N 0.000 description 1
- YRJYANBGTAMXRQ-UHFFFAOYSA-N pyrazolo[3,4-h]quinazolin-2-one Chemical compound C1=C2N=NC=C2C2=NC(=O)N=CC2=C1 YRJYANBGTAMXRQ-UHFFFAOYSA-N 0.000 description 1
- INCIMLINXXICKS-UHFFFAOYSA-M pyronin Y Chemical compound [Cl-].C1=CC(=[N+](C)C)C=C2OC3=CC(N(C)C)=CC=C3C=C21 INCIMLINXXICKS-UHFFFAOYSA-M 0.000 description 1
- 239000001020 pyronin dye Substances 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 150000003856 quaternary ammonium compounds Chemical class 0.000 description 1
- 125000001453 quaternary ammonium group Chemical group 0.000 description 1
- 229940079053 quaternium-27 Drugs 0.000 description 1
- 239000004172 quinoline yellow Substances 0.000 description 1
- 229940051201 quinoline yellow Drugs 0.000 description 1
- 235000012752 quinoline yellow Nutrition 0.000 description 1
- 238000010526 radical polymerization reaction Methods 0.000 description 1
- 230000008707 rearrangement Effects 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 238000003303 reheating Methods 0.000 description 1
- 230000002040 relaxant effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- PYWVYCXTNDRMGF-UHFFFAOYSA-N rhodamine B Chemical compound [Cl-].C=12C=CC(=[N+](CC)CC)C=C2OC2=CC(N(CC)CC)=CC=C2C=1C1=CC=CC=C1C(O)=O PYWVYCXTNDRMGF-UHFFFAOYSA-N 0.000 description 1
- 239000004170 rice bran wax Substances 0.000 description 1
- 235000019384 rice bran wax Nutrition 0.000 description 1
- 235000002020 sage Nutrition 0.000 description 1
- JZWFDVDETGFGFC-UHFFFAOYSA-N salacetamide Chemical group CC(=O)NC(=O)C1=CC=CC=C1O JZWFDVDETGFGFC-UHFFFAOYSA-N 0.000 description 1
- 229930195734 saturated hydrocarbon Natural products 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229910052624 sepiolite Inorganic materials 0.000 description 1
- 235000019355 sepiolite Nutrition 0.000 description 1
- 239000003352 sequestering agent Substances 0.000 description 1
- 230000021148 sequestering of metal ion Effects 0.000 description 1
- 210000002966 serum Anatomy 0.000 description 1
- 229940057910 shea butter Drugs 0.000 description 1
- 150000004756 silanes Chemical class 0.000 description 1
- 150000003377 silicon compounds Chemical class 0.000 description 1
- 229910052814 silicon oxide Inorganic materials 0.000 description 1
- 229920002050 silicone resin Polymers 0.000 description 1
- 229910021647 smectite Inorganic materials 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 235000019982 sodium hexametaphosphate Nutrition 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 229940045898 sodium stearoyl glutamate Drugs 0.000 description 1
- KDHFCTLPQJQDQI-BDQAORGHSA-M sodium;(4s)-4-amino-5-octadecanoyloxy-5-oxopentanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC(=O)OC(=O)[C@@H](N)CCC([O-])=O KDHFCTLPQJQDQI-BDQAORGHSA-M 0.000 description 1
- 229940057429 sorbitan isostearate Drugs 0.000 description 1
- 239000001593 sorbitan monooleate Substances 0.000 description 1
- 235000011069 sorbitan monooleate Nutrition 0.000 description 1
- 229940035049 sorbitan monooleate Drugs 0.000 description 1
- 229950011392 sorbitan stearate Drugs 0.000 description 1
- 235000019337 sorbitan trioleate Nutrition 0.000 description 1
- 229960000391 sorbitan trioleate Drugs 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 235000010356 sorbitol Nutrition 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
- 235000012424 soybean oil Nutrition 0.000 description 1
- 125000006850 spacer group Chemical group 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 229940032094 squalane Drugs 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 229940071136 stearoyl glutamate Drugs 0.000 description 1
- 150000003432 sterols Chemical class 0.000 description 1
- 235000003702 sterols Nutrition 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 159000000008 strontium salts Chemical class 0.000 description 1
- 229920003048 styrene butadiene rubber Polymers 0.000 description 1
- 229920000468 styrene butadiene styrene block copolymer Polymers 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- SEEPANYCNGTZFQ-UHFFFAOYSA-N sulfadiazine Chemical compound C1=CC(N)=CC=C1S(=O)(=O)NC1=NC=CC=N1 SEEPANYCNGTZFQ-UHFFFAOYSA-N 0.000 description 1
- 229940117986 sulfobetaine Drugs 0.000 description 1
- 125000000542 sulfonic acid group Chemical group 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- 235000020238 sunflower seed Nutrition 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
- 230000002459 sustained effect Effects 0.000 description 1
- 238000013268 sustained release Methods 0.000 description 1
- 239000012730 sustained-release form Substances 0.000 description 1
- 239000012209 synthetic fiber Substances 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 229940095064 tartrate Drugs 0.000 description 1
- UJMBCXLDXJUMFB-GLCFPVLVSA-K tartrazine Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)C1=NN(C=2C=CC(=CC=2)S([O-])(=O)=O)C(=O)C1\N=N\C1=CC=C(S([O-])(=O)=O)C=C1 UJMBCXLDXJUMFB-GLCFPVLVSA-K 0.000 description 1
- 235000012756 tartrazine Nutrition 0.000 description 1
- 239000004149 tartrazine Substances 0.000 description 1
- 229960000943 tartrazine Drugs 0.000 description 1
- 150000003512 tertiary amines Chemical class 0.000 description 1
- 150000003866 tertiary ammonium salts Chemical class 0.000 description 1
- OULAJFUGPPVRBK-UHFFFAOYSA-N tetratriacontan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCO OULAJFUGPPVRBK-UHFFFAOYSA-N 0.000 description 1
- 125000003831 tetrazolyl group Chemical group 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 238000007725 thermal activation Methods 0.000 description 1
- 238000001757 thermogravimetry curve Methods 0.000 description 1
- 239000001016 thiazine dye Substances 0.000 description 1
- 125000003396 thiol group Chemical group [H]S* 0.000 description 1
- DHCDFWKWKRSZHF-UHFFFAOYSA-L thiosulfate(2-) Chemical group [O-]S([S-])(=O)=O DHCDFWKWKRSZHF-UHFFFAOYSA-L 0.000 description 1
- 150000003585 thioureas Chemical class 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 description 1
- 235000010487 tragacanth Nutrition 0.000 description 1
- 239000000196 tragacanth Substances 0.000 description 1
- 229940116362 tragacanth Drugs 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 150000003918 triazines Chemical class 0.000 description 1
- 125000002889 tridecyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 150000005691 triesters Chemical class 0.000 description 1
- 229940118576 triisostearyl citrate Drugs 0.000 description 1
- 229940117985 trimethyl pentaphenyl trisiloxane Drugs 0.000 description 1
- LINXHFKHZLOLEI-UHFFFAOYSA-N trimethyl-[phenyl-bis(trimethylsilyloxy)silyl]oxysilane Chemical compound C[Si](C)(C)O[Si](O[Si](C)(C)C)(O[Si](C)(C)C)C1=CC=CC=C1 LINXHFKHZLOLEI-UHFFFAOYSA-N 0.000 description 1
- 125000000026 trimethylsilyl group Chemical group [H]C([H])([H])[Si]([*])(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- 229940026256 trioctyldodecyl citrate Drugs 0.000 description 1
- ICWQKCGSIHTZNI-UHFFFAOYSA-N tris(16-methylheptadecyl) 2-hydroxypropane-1,2,3-tricarboxylate Chemical compound CC(C)CCCCCCCCCCCCCCCOC(=O)CC(O)(C(=O)OCCCCCCCCCCCCCCCC(C)C)CC(=O)OCCCCCCCCCCCCCCCC(C)C ICWQKCGSIHTZNI-UHFFFAOYSA-N 0.000 description 1
- BIEMOBPNIWQLMF-UHFFFAOYSA-N tris(2-octyldodecyl) 2-hydroxypropane-1,2,3-tricarboxylate Chemical compound CCCCCCCCCCC(CCCCCCCC)COC(=O)CC(O)(C(=O)OCC(CCCCCCCC)CCCCCCCCCC)CC(=O)OCC(CCCCCCCC)CCCCCCCCCC BIEMOBPNIWQLMF-UHFFFAOYSA-N 0.000 description 1
- NELZVYZKKXHHAB-IUPFWZBJSA-N tris[(z)-octadec-9-enyl] 2-hydroxypropane-1,2,3-tricarboxylate Chemical compound CCCCCCCC\C=C/CCCCCCCCOC(=O)CC(O)(C(=O)OCCCCCCCC\C=C/CCCCCCCC)CC(=O)OCCCCCCCC\C=C/CCCCCCCC NELZVYZKKXHHAB-IUPFWZBJSA-N 0.000 description 1
- HRXKRNGNAMMEHJ-UHFFFAOYSA-K trisodium citrate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O HRXKRNGNAMMEHJ-UHFFFAOYSA-K 0.000 description 1
- 235000013799 ultramarine blue Nutrition 0.000 description 1
- 125000004417 unsaturated alkyl group Chemical group 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 229930195735 unsaturated hydrocarbon Natural products 0.000 description 1
- 150000003672 ureas Chemical class 0.000 description 1
- 150000003673 urethanes Chemical class 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- 239000007762 w/o emulsion Substances 0.000 description 1
- 229920001285 xanthan gum Polymers 0.000 description 1
- 239000000230 xanthan gum Substances 0.000 description 1
- 235000010493 xanthan gum Nutrition 0.000 description 1
- 229940082509 xanthan gum Drugs 0.000 description 1
- 239000000811 xylitol Substances 0.000 description 1
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 1
- 235000010447 xylitol Nutrition 0.000 description 1
- 229960002675 xylitol Drugs 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
- PAPBSGBWRJIAAV-UHFFFAOYSA-N ε-Caprolactone Chemical compound O=C1CCCCCO1 PAPBSGBWRJIAAV-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8105—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- A61K8/8117—Homopolymers or copolymers of aromatic olefines, e.g. polystyrene; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A45—HAND OR TRAVELLING ARTICLES
- A45D—HAIRDRESSING OR SHAVING EQUIPMENT; EQUIPMENT FOR COSMETICS OR COSMETIC TREATMENTS, e.g. FOR MANICURING OR PEDICURING
- A45D7/00—Processes of waving, straightening or curling hair
- A45D7/06—Processes of waving, straightening or curling hair combined chemical and thermal
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0241—Containing particulates characterized by their shape and/or structure
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0241—Containing particulates characterized by their shape and/or structure
- A61K8/025—Explicitly spheroidal or spherical shape
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/044—Suspensions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/06—Preparations for styling the hair, e.g. by temporary shaping or colouring
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Insects & Arthropods (AREA)
- Zoology (AREA)
- Dispersion Chemistry (AREA)
- Thermal Sciences (AREA)
- Physics & Mathematics (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Description
(a)1μm以上から約100μmまでの範囲のピークを有する体積基準の粒径分布を有し、かつ
(i)少なくとも1種のスチレン系ブロックコポリマーを含んでなる油ゲル化剤と、
(ii)35℃より高い融点を有する少なくとも1種のワックス、少なくとも1種の油、およびそれらの混合物から選択される脂肪物質と
を含んでなる粒子、ならびに
(b)
(i)少なくとも1種の非イオン性界面活性剤と、
(ii)少なくとも1種のイオン性界面活性剤と、
(iii)水と
を含んでなる界面活性剤混合物
を含有する水性分散物に関する。
A.上記で開示され、かつ
(a)1μmから約100μmまでの範囲のピークを有する体積基準の粒径分布を有し、かつ
(i)少なくとも1種のスチレン系ブロックコポリマーを含んでなる油ゲル化剤と、
(ii)35℃より高い融点を有する少なくとも1種のワックス、少なくとも1種の油、およびそれらの混合物から選択される脂肪物質と、
(iii)任意選択的に、a)(i)以外の油ゲル化剤、着色剤、日焼け止め剤、35℃以下の融点を有するワックス、芳香油、乳化ポリマー、シリカ、タルク、粘土およびそれらの混合物から選択される少なくとも1種の追加成分と
を含んでなる粒子、
(b)
(i)少なくとも1種の非イオン性界面活性剤と、
(ii)少なくとも1種のイオン性界面活性剤と
を含んでなる界面活性剤混合物、ならびに
(c)水
を含んでなる水性分散物と、
B.水、揮発性有機溶媒、非揮発性有機溶媒、シリコーン、非シリコーン油およびそれらの混合物を含んでなる担体と
を含有する組成物に関する。
A.
(a)約20μm〜約70μmの範囲のピークを有する体積基準の粒径分布を有し、かつ水性分散物の全重量に基づく重量で、
(i)スチレン−エチレン/ブチレンジブロックコポリマー、スチレン−エチレン/ブチレン−スチレントリブロックコポリマー、およびそれらの混合物から選択される、少なくとも1種のスチレン系ブロックコポリマーを含んでなる、約0.1重量%〜約15重量%の油ゲル化剤と、
(ii)35℃より高い融点を有する少なくとも1種のワックスを含んでなる、約10重量%〜約60重量%の脂肪物質と、
(iii)任意選択的に、a)(i)以外の油ゲル化剤、着色剤、日焼け止め剤、35℃以下の融点を有するワックス、芳香油、乳化ポリマー、シリカ、タルク、粘土およびそれらの混合物から選択される少なくとも1種の追加成分と
を含んでなる粒子、
(b)
(i)少なくとも1種の非イオン性界面活性剤と、
(ii)少なくとも1種のイオン性界面活性剤と
を含んでなる界面活性剤混合物、ならびに
(c)水
を含んでなる水性分散物と、
B.水、揮発性有機溶媒、非揮発性有機溶媒、シリコーン、非シリコーン油およびそれらの混合物を含んでなる担体と、
C.任意選択的に、液体脂質/油、ワックス、フィルム形成ポリマー、レオロジー変性剤、湿潤剤および保湿剤、乳化剤、構成化剤、噴射剤、界面活性剤、光沢剤、コンディショニング剤、化粧品的、皮膚科学的および薬学的活性剤、ビタミン、植物抽出物およびそれらの混合物から選択される少なくとも1種の補助成分と
を含有する組成物に関する。
A.
(a)約20μm〜約70μmの範囲のピークを有する体積基準の粒径分布を有し、かつ水性分散物の全重量に基づく重量で、
(i)スチレン−エチレン/ブチレンジブロックコポリマー、スチレン−エチレン/ブチレン−スチレントリブロックコポリマー、およびそれらの混合物から選択される、少なくとも1種のスチレン系ブロックコポリマーを含んでなる、約0.1重量%〜約15重量%の油ゲル化剤と、
(ii)少なくとも1種の油を含んでなる脂肪物質と、
(iii)任意選択的に、a)(i)以外の油ゲル化剤、着色剤、日焼け止め剤、35℃以下の融点を有するワックス、芳香油、乳化ポリマー、シリカ、タルク、粘土およびそれらの混合物から選択される少なくとも1種の追加成分と
を含んでなる粒子、
(b)
(i)少なくとも1種の非イオン性界面活性剤と、
(ii)少なくとも1種のイオン性界面活性剤と
を含んでなる界面活性剤混合物、ならびに
(c)水
を含んでなる水性分散物と、
B.水、揮発性有機溶媒、非揮発性有機溶媒、シリコーン、非シリコーン油およびそれらの混合物を含んでなる担体と、
C.任意選択的に、液体脂質/油、ワックス、フィルム形成ポリマー、レオロジー変性剤、湿潤剤および保湿剤、乳化剤、構成化剤、噴射剤、界面活性剤、光沢剤、コンディショニング剤、化粧品的、皮膚科学的および薬学的活性剤、ビタミン、植物抽出物およびそれらの混合物から選択される少なくとも1種の補助成分と
を含有する組成物に関する。
A.
(a)約20μm〜約70μmの範囲のピークを有する体積基準の粒径分布を有し、かつ水性分散物の全重量に基づく重量で、
(i)スチレン−エチレン/ブチレンジブロックコポリマー、スチレン−エチレン/ブチレン−スチレントリブロックコポリマー、およびそれらの混合物から選択される、少なくとも1種のスチレン系ブロックコポリマーを含んでなる、約0.1重量%〜約15重量%の油ゲル化剤と、
(ii)35℃より高い融点を有するワックスおよび少なくとも1種の油を含んでなる脂肪物質と、
(iii)任意選択的に、a)(i)以外の油ゲル化剤、着色剤、日焼け止め剤、35℃以下の融点を有するワックス、芳香油、乳化ポリマー、シリカ、タルク、粘土およびそれらの混合物から選択される少なくとも1種の追加成分と
を含んでなる粒子、
(b)
(i)少なくとも1種の非イオン性界面活性剤と、
(ii)少なくとも1種のイオン性界面活性剤と
を含んでなる界面活性剤混合物、ならびに
(c)水
を含んでなる水性分散物と、
B.水、揮発性有機溶媒、非揮発性有機溶媒、シリコーン、非シリコーン油およびそれらの混合物を含んでなる担体と、
C.任意選択的に、液体脂質/油、ワックス、フィルム形成ポリマー、レオロジー変性剤、湿潤剤および保湿剤、乳化剤、構成化剤、噴射剤、界面活性剤、光沢剤、コンディショニング剤、化粧品的、皮膚科学的および薬学的活性剤、ビタミン、植物抽出物およびそれらの混合物から選択される少なくとも1種の補助成分と
を含有する組成物に関する。
(a)約20μm〜約70μmの範囲のピークを有する体積基準の粒径分布を有し、かつ水性分散物の全重量に基づく重量で、
(i)スチレン−エチレン/ブチレンジブロックコポリマー、スチレン−エチレン/ブチレン−スチレントリブロックコポリマー、およびそれらの混合物から選択される、少なくとも1種のスチレン系ブロックコポリマーを含んでなる、約0.1重量%〜約15重量%の油ゲル化剤と、
(ii)蜜蝋、水素化ミリスチルオリーブエステル、水素化ステアリルオリーブエステル、VP/エイコセンコポリマー、ジトリメチロイルプロパンテトラステアレートおよびC30〜45アルキルジメチルシリルプロピルシルセスキオキサンおよびその混合物から選択される、35℃より高い融点を有する少なくとも1種のワックスから選択される、約10重量%〜約60重量%の脂肪物質と、
(iii)任意選択的に、a)(i)以外の油ゲル化剤、着色剤、日焼け止め剤、35℃以下の融点を有するワックス、乳化ポリマー、芳香油、シリカ、タルク、粘土およびそれらの混合物から選択される少なくとも1種の追加成分と
を含んでなる粒子、
(b)
(i)PEG−30 グリセリルステアレート、ソルビタンパルミテート、セチルPEG/PPG−10/1ジメチコン、ビス−PEG/PPG−16/16 PEG/PPG−16/16ジメチコン、ビス−PEG/PPG−20/5 PEG/PPG−20/5ジメチコン、PEG/PPG−25/4ジメチコン、ビス−(グリセリル/ラウリル)グリセリルラウリルジメチコン、ビス−PEG/PPG−14/14ジメチコンおよびそれらの混合から選択される少なくとも1種の非イオン性界面活性剤と、
(ii)少なくとも1種のイオン性界面活性剤と
を含んでなる、約1重量%〜約5重量%の界面活性剤混合物、ならびに
(c)水
を含んでなる水性分散物に関する。
本開示の水性分散物は、少なくとも1種のスチレン系ブロックコポリマーを含んでなる油ゲル化剤と、35℃より高い融点を有する少なくとも1種のワックス、少なくとも1種の油、およびそれらの混合物から選択される脂肪物質とを含んでなる粒子を含有する。
本発明の少なくとも1種の油ゲル化剤は、少なくとも1種のスチレン系ブロックコポリマーを含んでなる。
本発明の目的に関して、「ポリマー」という用語は、少なくとも2個の繰り返し単位、好ましくは少なくとも3個の繰り返し単位、特に少なくとも10個の繰り返し単位を含んでなる化合物を意味するように意図される。
本発明の目的に関して、「半結晶質ポリマー」は、結晶化可能な部分および非晶質部分を含んでなり、かつ特に溶融(固体−液体転移)の相温度の一次可逆変化を有するポリマーを意味する。結晶化可能な部分は、主鎖中の側鎖(またはペンダント鎖)あるいはブロックのいずれかである。
ポリマーおよびコポリマーは、特に好ましくは、結晶化可能な側鎖を有する半結晶質ポリマーから選択される。特に、米国特許第A−5156911号明細書および国際公開第A−01/19333号パンフレットに定義されるものが参照されてよい。
−重合に対して反応性またはエチレン系二重結合を有する、すなわち、ビニル、(メタ)アクリルまたはアリル基を有する1種またはそれ以上のモノマーの重合、特にラジカル重合から、
−共反応性基(カルボン酸、スルホン酸、アルコール、アミンまたはイソシアネート)を有する1種またはそれ以上のモノマー、例えば、ポリエステル、ポリウレタン、ポリエーテルまたはポリウレタンの重縮合から
得ることができる。
−Mはポリマー主鎖の原子を表し、Cは結晶化可能な基を表し、かつSはスペーサーを表す。
−「−S−C」結晶化可能な鎖は、飽和または不飽和C12〜C40、好ましくはC12〜C28、好ましくはC14〜C24炭化水素ベースのアルキル鎖を含んでなる、任意選択的にフッ素化またはペルフッ素化された炭化水素ベースの脂肪族または芳香族鎖である。
−「C」は、直鎖または分枝鎖または環式である基(CH2)nを表し、nは12〜40の範囲の整数である。好ましくは、「C」は直鎖の基である。好ましくは、「S」および「C」は異なる。)によって表され得る結晶化可能な鎖を含有する少なくとも1種のモノマーの重合から得られるホモポリマーおよびコポリマーから特に選択される。
これらのポリマーは、特に、その1つが結晶化可能である、異なる化学的性質を有する少なくとも2つのブロックからなるブロックコポリマーである。
ポリエステル重縮合物は、脂肪族ポリエステルから選択され得る。それらの分子量は、好ましくは200g/モル以上で且つ10000g/モル以下、より好ましくは300g/モル以上で且つ5000g/モル以下、好ましくは500g/モル以上で且つ2000g/モル以下である。
本発明の組成物の半結晶質ポリマーは、米国特許出願公開第2007/0031361号明細書に記載のものなどのメタロセン触媒作用によって得られるポリマーであってもよい。
本発明のグルタミドをベースとする化合物は、一種の有機ゲル化剤を含んでなることが知られている。好ましくは、本発明のグルタミドをベースとする化合物は、ポリマーではない。
本発明のポリアミドは、炭化水素をベースとするポリアミド、シリコーンポリアミドおよびそれらの混合物から選択されてよい。
「炭化水素をベースとするポリアミド」という用語は、炭素および水素原子、ならびに任意選択的に酸素および窒素原子から本質的に形成されるか、またはそれらから構成され、かついずれかのケイ素またはフッ素原資を含有しないポリアミドを意味する。これは、アルコール、エステル、エーテル、カルボン酸、アミンおよび/またはアミド基を含有してもよい。
本発明のシリコーンポリアミドは、好ましくは、室温(25℃)および気圧(760mmHg)において固体である。
−R4、R5、R6およびR7は、同一であっても、または異なっていてもよく、
−それらの鎖中に1個またはそれ以上の酸素、硫黄および/または窒素原子を含有している可能性があり、かつフッ素原子によって部分的に、または完全に置換されている可能性のある、直鎖、分枝鎖または環式、飽和または不飽和のC1〜C40炭化水素ベースの基、
−任意選択的に1個またはそれ以上のC1〜C4アルキル基によって置換されたC6〜C10アリール基、
−1個またはそれ以上の酸素、硫黄および/または窒素原子を含有する可能性があるポリオルガノシロキサン鎖
から選択される基を表し、
−基Xは、同一であっても、または異なっていてもよく、その鎖中に1個またはそれ以上の酸素および/または窒素原子を含有している可能性のある直鎖または分枝鎖C1〜C30アルキレンジイル基を表し、
−Yは、1個またはそれ以上の酸素、硫黄および/または窒素原子を含んでなり得、かつ/または置換基として以下の原子または原子の群:フッ素、ヒドロキシル、C3〜C8シクロアルキル、C1〜C40アルキル、C5〜C10アリール、任意選択的に1〜3個のC1〜C3アルキルによって置換されたフェニル、C1〜C3ヒドロキシアルキルおよびC1〜C6アミノアルキル基の1つを有し得る、飽和または不飽和C1〜C50直鎖または分枝鎖アルキレン、アリーレン、シクロアルキレン、アルキルアリーレンまたはアリールアルキレン二価基であるか、あるいは
−Yは、次式
−Tは、任意選択的にポリオルガノシロキサン鎖によって置換され、かつO、NおよびSから選択される1個またはそれ以上の原子を含有する可能性がある、直鎖または分枝鎖、飽和または不飽和のC3〜C24三価または四価の炭化水素ベースの基を表すか、あるいはTは、N、PおよびAlから選択される三価原子を表し、かつ
−R8は、ポリマーの別の鎖と連結される可能性があり得る1つまたはそれ以上のエステル、アミド、ウレタン、チオカバーメート、尿素、チオ尿素および/またはスルホンアミド基を含んでなる可能性がある、直鎖または分枝鎖C1〜C50アルキル基またはポリオルガノシロキサン鎖を表す)に相当する基を表し、
−nは、2〜500、好ましくは2〜200の範囲の整数であり、かつmは、1〜1000、好ましくは1〜700、さらに良好には6〜200の範囲の整数である]の少なくとも1つの単位を含んでなるポリマーであってよい。
本開示の分散物粒子中に存在することができる少なくとも1種のワックスは、35℃より高い融点、例えば35℃より高く約250℃まで、または例えば40℃より高く約100℃までの融点を有する。35℃より高い融点を有する少なくとも1種のワックスは、固体/液体状態の可逆変化を有するものとして定義される。固体状態のワックスの融点は、その液体状態の氷点と同じであり、かつ物質の純度および周囲圧力などの要素に依存する。融点は、いずれかの一定圧力において固体およびその液体が平衡にある温度である。固体ワックスは、ワックスの融点付近の温度で軟化を開始する。温度を増加させると、特定の温度になるまで、ワックスは軟化/溶融し続けて、ワックスは標準気圧で完全に液体になる。実際の融点値が考慮中に材料のために与えられるのは、この段階である。熱が除去されると、液化したワックス材料は、材料が固体状態に戻るまで凝固を開始する。ワックス材料を液体状態(溶融)にすることによって、油などの他の材料と混和させて、顕微鏡的に均一な混合物を形成することが可能となる。しかしながら、混合物の温度が室温になると、混合物中の他の材料とのワックスの再結晶が得られ得る。
「非シリコーン油」という用語は、いずれかのケイ素原子(Si)を含有しない油を意味し、かつ「シリコーン油」という用語は、少なくとも1個のケイ素原子を含有する油を意味する。
−例えば、オイル70047V500000などのRhodiaから販売される47および70047シリーズのSilbione(登録商標)オイルまたはMirasil(登録商標)オイル、
−Rhodiaから販売されるMirasil(登録商標)シリーズのオイル、
−60000mm2/秒の粘度を有するDC200などのDow Corning社からの200シリーズのオイル、
−General ElectricからのViscasil(登録商標)オイルおよびGeneral ElectricからのSFシリーズ(SF96、SF18)の特定のオイル。
本発明の粒子は、少なくとも1種のスチレン系ブロックコポリマーを含んでなる油ゲル化剤と、35℃より高い融点を有する少なくとも1種のワックス、少なくとも1種の油およびそれらの混合物から選択される脂肪物質とを含んでなる。
水性分散物の粒子は、1μm以上から約100μmまでの範囲でピークを有する体積基準の粒径分布を有する。
粒子は、少なくとも1種のスチレン系ブロックコポリマーを含んでなる油ゲル化剤以外の上記油ゲル化剤、着色剤、日焼け止め剤、揮発性溶媒、35℃以下の融点を有するワックス、乳化ポリマー、シリカ、タルク、粘土、セラミドおよびそれらの混合物などの追加的な成分をさらに含んでなることができる。粒子の物理的特性を改善/変性するため、そして/または粒子が、ワックスから得られる利点に加えて他の利点を提供するように、水性分散物の製造時間の間に、これらの追加的な成分を添加することができる。
本発明の水性分散物の粒子は、サブミクロンサイズからミクロンサイズのシリカ、タルクおよび粘土の粒子をさらに含んでなってもよく、これには、限定されないが、モンモリロナイト、ベントナイト、ヘクトライト、アタパルジャイト、セピオライト、ラポナイト、スメクタイト、カオリンおよびそれらの混合物が含まれる。
−R18およびR19は、独立して、10〜22個の炭素原子を有するアルキル−またはアルケニル基から選択され、
−R20は、メチル、エチル、n−プロピルまたはイソプロピル基から選択され、かつ
−nは、例えば、2または3などの1〜6の範囲の数である)
の化合物が含まれる。
−R1は、飽和または不飽和、直鎖または分枝鎖C1〜C50、例えば、C5〜C50炭化水素基(この基に関して、酸R7COOHによって任意選択的にエステル化された1個またはそれ以上のヒドロキシル基によって置換されることが可能であり、R7は、任意選択的にモノ−またはポリヒドロキシル化された直鎖または分枝鎖、飽和または不飽和C1〜C35炭化水素基であり、基R7のヒドロキシルに関して、任意選択的にモノ−またはポリヒドロキシル化された直鎖または分枝鎖、飽和または不飽和C1〜C35脂肪酸によってエステル化されることが可能である)、あるいは基R’’−(NR−CO)−R’(Rは水素原子、またはモノ−もしくはポリヒドロキシル化された基から選択される)から選択され、
−R2は、水素原子、サッカライド型基から選択され、
−R3は、水素原子、または水酸化もしくは非水酸化、飽和または不飽和、C1〜C33炭化水素基から選択され、
−R4は、水素原子、メチルまたはエチル基、任意選択的に水酸化された直鎖または分枝鎖、飽和または不飽和C3〜C50炭化水素基、あるいは基−CH2−CHOH−CH2−O−R6(R6はC10〜C26炭化水素基を示す)、あるいは基から選択され
−R8−O−CO−(CH2)p(R8はC1〜C20炭化水素基から選択され、pは1〜12の範囲の整数である)から選択され、かつ
−R5は、水素原子、または任意選択的にモノ−もしくはポリヒドロキシル化された直鎖または分枝鎖、飽和または不飽和C1〜C35炭化水素基を表すが、
−ただし、R3およびR5が水素を示す場合、またはR3が水素を示し、かつR5がメチルを示す場合、R4は、水素原子またはメチルもしくはエチル基を示さない]
の化合物から選択されてもよい。
−R1は、C14〜C30脂肪酸から誘導される直鎖または分枝鎖、飽和または不飽和アルキル基から選択され、
−R2は、水素原子、または(グリコシル)n、(ガラクトシル)mもしくはスルホガラクトシル基から選択され、nは1〜4の範囲の整数であり、かつmは1〜8の範囲の整数であり、かつ
−R3は、アルファ位で飽和または不飽和のC5〜C26炭化水素をベースとする基から選択され、この基に関して、1個またはそれ以上のC1〜C14アルキル基によって置換されることが可能である)
の化合物から選択されてもよい。
−R11およびR12は、独立して、10〜22個の炭素原子を有するアルキルまたはアルケニル基から選択され、
−R13は、1〜4個の炭素原子を有するアルキルまたはヒドロキシルアルキル基であり、かつ
−nは、2または3などの1〜6の範囲の数である)
の化合物から選択されてもよい。
本開示の界面活性剤混合物は、少なくとも1種の非イオン性界面活性剤および少なくとも1種のイオン性界面活性剤を含んでなる。
i)アルキルピリジニウム塩、イミダゾリンのアンモニウム塩、ジ第4級アンモニウム塩、および少なくとも1つのエステル官能基を含有するアンモニウム塩。
ii)以下の一般式を有する第4級アンモニウム塩:
R5は、8〜30個の炭素原子を含有するアルケニルまたはアルキル基、例えば、タローまたはココナッツの脂肪酸誘導体を表し、
R6は、水素原子、C1〜C4アルキル基、あるいは8〜30個の炭素原子を含有するアルケニルまたはアルキル基を表し、
R7は、C1〜C4アルキル基を表し、
R8は、水素原子またはC1〜C4アルキル基を表し、
X’は、ハライド、ホスフェート、アセテート、ラクテート、C2〜C6アルキルスルフェート、アルキルスルホネートまたはアルキルアリールスルホネートの群から選択されるアニオンである)。
iv)次式のジ第4級アンモニウム塩:
R9は、約16〜30個の炭素原子を含有する脂肪族基を示し、
R10、R11、R12、R13およびR14は、同一であっても異なってもよく、水素および1〜4個の炭素原子を含有するアルキル基から選択され、かつ
X−は、ハライド、アセテート、ホスフェート、ニトレート、エチルスルフェートおよびメチルスルフェートの群から選択されるアニオンである)。
v)次式のものなどの少なくとも1つのエステル官能基を含有する第4級アンモニウム塩:
R15は、C1〜C6アルキル基およびC1〜C6ヒドロキシアルキルまたはジヒドロキシアルキル基から選択され;
R16は、基R19−CO−、直鎖または分枝鎖、飽和または不飽和C1〜C22炭化水素ベースの基R20、水素原子から選択され;
R18は、基R21−CO、直鎖または分枝鎖、飽和または不飽和C1〜C22炭化水素ベースの基R22、水素原子から選択され;
R17、R19およびR21は、同一であっても異なってもよく、直鎖または分枝鎖、飽和または不飽和C7〜C21炭化水素ベースの基から選択され;
r、nおよびpは、同一であっても異なってもよく、2〜6の範囲の整数であり;
yは、1〜10の範囲の整数であり;
xおよびzは、同一であっても異なってもよく、0〜10の範囲の整数であり;
X−は、単一または錯体の有機または鉱物アニオンであるが;
ただし、合計x+y+zが1〜15であり、xが0である場合、R16はR20を示し、かつzが0である場合、R18はR22を示すことを条件とする)。
本開示の水性分散物は、少なくとも以下の工程を含んでなるプロセスによって得られてもよい:
−少なくとも1種のスチレン系ブロックコポリマーを含んでなる油ゲル化剤と、35℃より高い融点を有する少なくとも1種のワックス、少なくとも1種の油およびそれらの混合物から選択される脂肪物質と、非イオン性界面活性剤およびイオン性界面活性剤を含んでなる界面活性剤混合物と、水と、任意選択的に、少なくとも1種のスチレン系ブロックコポリマーを含んでなる油ゲル化剤以外の油ゲル化剤、着色剤、日焼け止め剤、揮発性溶媒、35℃以下の融点を有するワックス、芳香油、乳化ポリマー、シリカ、タルク、粘土およびそれらの混合物から選択される少なくとも1種の追加成分とを含有する混合物を、少なくとも1種のワックスの融点より高い乳化温度で乳化するステップ(2種以上のワックスが使用される場合、乳化温度は、より高い、または最高融点を有するワックスの融点より高くなければならない)、
−混合物に、上記工程で使用される混合物の乳化温度より少なくとも5〜10℃高い温度で、粒子の製造を導くプロセスを受けさせるステップ、ならび
−そのようにして得られる分散物を冷却するステップ。
(1)35℃より高い融点を有する少なくとも1種のワックス、少なくとも1種の油およびそれらの混合物から選択された脂肪物質を加熱して、脂肪物質を溶融または軟化させるステップと、
(2)任意選択的に、(1)の脂肪物質と一緒に、少なくとも1種のスチレン系ブロックコポリマーを含んでなる油ゲル化剤以外の油ゲル化剤、着色剤、日焼け止め剤、35℃以下の融点を有するワックス、乳化ポリマー、(1)の少なくとも1種の油以外の芳香油、シリカ、タルク、粘土およびそれらの混合物から選択される少なくとも1種の追加成分を加熱するステップと、
(3)少なくとも1種のスチレン系ブロックコポリマーを含んでなる油ゲル化剤を加熱するステップと、
(4)(1)または(2)の脂肪物質と、(3)の油ゲル化剤を混合して、スチレン系ブロックコポリマー油ゲル化剤/脂肪物質ブレンドを形成するステップと、
(5)少なくとも1種の非イオン性界面活性剤および少なくとも1種のイオン性界面活性剤を含んでなる界面活性剤混合物ならびに水を加熱して、界面活性剤/水の組み合わせを形成するステップと、
(6)室温より高い温度で、スチレン系ブロックコポリマー油ゲル化剤/脂肪物質ブレンドと、界面活性剤/水の組み合わせを剪断作用によって混合して、水性分散物を形成するステップと、
(7)(6)の水性分散物を冷却するステップと
によるプロセスによって得られるが、
脂肪物質が、35℃より高い融点を有する少なくとも1種のワックスを含んでなる場合、脂肪物質は、少なくとも1種のワックスの融点より高い温度まで加熱される。
上記のプロセスによって、粒子は、好ましくは、水性および/または水溶性連続相中の分散物として得られる。そのような分散物は、水中油型エマルジョンまたは水中油型分散物として記載されてもよい。
本開示の水性分散物は、様々なガレヌス形態の組成物に調合されてもよい。
(a)1μm〜約70μmの範囲のピークを有する体積基準の粒径分布を有し、かつ
(i)少なくとも1種のスチレン系ブロックコポリマーを含んでなる油ゲル化剤と、
(ii)少なくとも1種の芳香油を含んでなる脂肪物質と
を含んでなる粒子、ならびに
(b)
(i)少なくとも1種の非イオン性界面活性剤と、
(ii)少なくとも1種のイオン性界面活性剤と、
を含んでなる界面活性剤混合物、ならびに
(c)水
を含んでなる水性分散物である。
本開示の水性分散物および水性分散物を含んでなる組成物は、液体脂質/油、ワックス、フィルム形成ポリマー、レオロジー変性剤、湿潤剤および保湿剤、乳化剤、構成化剤、噴射剤、界面活性剤、光沢剤、コンディショニング剤、化粧品的、皮膚科学的および薬学的活性剤、ビタミン、植物抽出物およびそれらの混合物から選択される補助剤を追加的に含有してもよい。
上記分散物プロトコルに基づき、以下の通り、本発明の水性分散物および水性分散物を含有する組成物を調製/製造した。
A.水性界面活性剤溶液:
1.容器中で非イオン性界面活性剤およびイオン性界面活性剤のグラム量を添加することによって、界面活性剤混合物を調製した。
2.水性分散物の最終的な重量(ワックスの重量を含む)が100グラムであるような量で、脱イオン水を添加した。
3.界面活性剤溶液を水浴中、約80℃〜約85℃の範囲内の温度まで加熱した。
1.水性界面活性剤溶液がなお高温(室温より高く、例えば、約65℃〜約70℃)にある時、溶液を約3000〜約9000rpmの範囲の速度でホモジナイザー/混合機(例えば、Silversonホモジナイザー)を使用して混合した。
2.混合しながら、加熱されたブレンド(なお室温より高い温度)を、ホモジナイザーの混合ヘッド付近で界面活性剤溶液に添加した。
3.全ての加熱されたブレンドを添加したら、混合を少なくとも5分間継続した。
4.ホモジナイザーブレードを取り外し、そしてエマルジョン(水性分散物)を混合し、そして室温へわずかに冷却し、ポリマー/ワックスおよび/または油の粒子を形成した。分散物を別の容器に移すか、または水性分散物を含有する組成物が製造される場合、組成物を構成する他の成分をこの段階で組み合わせて、そして水性分散物のアリコートを組成物に添加する。
5.分散物または組成物を室温で貯蔵した。
6.上記プロトコルに続いて、種々の濃度で種々のスチレン系ブロックコポリマーおよび/または脂肪物質(ワックスおよび油)および/または界面活性剤を使用して、本発明の他の水性分散物を調製する。
7.分散物を構成する粒子の粒径は、Shimadzu SALD−7001レーザー回折粒径分析器および1.2の屈折率を有する石英キュベットを用いて、レーザー回折法を使用して、体積基準の粒径分布(「PSD」)を測定することによって決定された。
以下の配合物は、例示された配合物の成分の残りに水性分散系Iのアリコートを添加することによって、実施例1の水性分散物から個々に調製された。
水性分散物を毛髪材料見本上に適用した。毛髪が他着性または粘着性のいずれでもないことが観察された。
Kraton G1657 Mなどのスチレン系ブロックコポリマーとワックスとの組み合わせから得られるブレンド材料の特性を、ワックス単独を使用して得られた特性と比較した。ブレンド材料中のスチレン系ブロックコポリマーの量が増加した時、毛髪の表面上のブレンド材料のフィルムのモジュラスおよびブレンド材料の粘着性を測定した。
測定器:Texture Technologies TA.XT Plus Texture Analyzer
試料は、厚さ約0.75mmのワックスブレンドの溶融形成ディスクであった。全ての試験に金属ボールプローブが使用された。以下を変更して標準的な粘着試験を使用した:試験後の速度:0.5mm/秒;適用された力:図1のデータに関しては250g、図2のデータに関しては100g。
測定器:TA Q800 DMA
試料は、薄い(厚さ約0.75mm)のワックスブレンドの溶融形成ディスクから切断された。ストリップは、15mm×5.5mm×0.75mmのおよその寸法(L×W×T)を有した。正確な寸法は、キャリパーを使用して測定された。
ワックスの粘着性およびワックスと8%スチレン系コポリマーとを含んでなるブレンド材料の粘着性は、添加された合成油皮脂の関数として測定された。試験は、サロンのボランティアの毛髪上で行なわれた。
Claims (15)
- 毛髪を成形する方法であって、
(i)組成物を毛髪上に適用するステップであって、前記組成物が、
A. 水性分散物であって、
a)1μm以上100μm以下の範囲のピークを有する体積基準の粒径分布を有する粒子であって、前記粒子が、
a1)少なくとも1種のスチレン系ブロックコポリマーを含む油ゲル化剤、ならびに
a2)脂肪物質であって、
− 蜜蝋、水素化ミリスチルオリーブエステル、水素化ステアリルオリーブエステル、VP/エイコセンコポリマー、ジトリメチロイルプロパンテトラステアレート、シルセスキオキサン樹脂ワックスおよびそれらの混合物から選択される、35℃より高い融点を有する少なくとも1種のワックス、
− C 6 〜C 16 アルカン、植物、鉱物または合成由来の非シリコーン油、液体脂肪アルコール、液体脂肪酸、脂肪酸の液体エステル、脂肪アルコールの液体エステル、シリコーン油、芳香油およびそれらの混合物から選択される、少なくとも1種の油、ならびに
− それらの混合物
から選択される、脂肪物質
を含む、粒子、
b)
b1)グリセリルエステルのポリエチレングリコールエーテル、ソルビタンエステル、アルコキシル化基および/または側鎖を有するシリコーンベースの乳化ポリマー、ならびにそれらの混合物から選択される、少なくとも1種の非イオン性界面活性剤、ならびに
b2)アシルグルタメート、アルキルスルフェートおよびそれらの塩、アルキルエーテルスルフェートおよびそれらの塩、アルキルエーテルカルボキシレート、ならびにそれらの混合物から選択される、少なくとも1種のアニオン性界面活性剤
を含む界面活性剤混合物、ならびに
c)水
を含有する、水性分散物、
B. 水、揮発性有機溶媒、非揮発性有機溶媒、シリコーン、非シリコーン油およびそれらの混合物から選択される少なくとも1種の成分を含む担体、ならびに
C. 任意選択的に、液体脂質/油、ワックス、フィルム形成ポリマー、レオロジー変性剤、湿潤剤および保湿剤、乳化剤、構成化剤、噴射剤、界面活性剤、光沢剤、コンディショニング剤、化粧品的、皮膚科学的および薬学的活性剤、ビタミン、植物抽出物、ならびにそれらの混合物から選択される少なくとも1種の補助成分
を含む、ステップ、ならびに
(ii)前記毛髪に熱を適用するステップ
を含み、
「体積基準の粒径分布」という用語は、個体群のパーセンテージが、示された直径において粒子の体積に基づき決定される、分散物の粒径分布を指す、方法。 - 前記水性分散物において、前記少なくとも1種のスチレン系ブロックコポリマーが、スチレン−エチレン/ブチレンジブロックコポリマー、スチレン−エチレン/プロピレンジブロックコポリマー、スチレン−エチレン/ブチレン−スチレントリブロックコポリマー、およびそれらの混合物から選択される、請求項1に記載の方法。
- 前記水性分散物において、前記少なくとも1種のスチレン系ブロックコポリマーが、スチレン−エチレン/ブチレンジブロックコポリマーおよびスチレン−エチレン/ブチレン−スチレントリブロックコポリマーを含む、請求項1または2に記載の方法。
- 前記水性分散物において、前記脂肪物質が、35℃より高い融点を有する少なくとも1種のワックスから選択される、請求項1〜3のいずれか一項に記載の方法。
- 前記水性分散物において、前記35℃より高い融点を有する少なくとも1種のワックスの量対前記少なくとも1種のスチレン系ブロックコポリマーの量の重量比が、100:1〜1:100の範囲である、請求項4に記載の方法。
- 前記水性分散物において、前記35℃より高い融点を有する少なくとも1種のワックスが、前記水性分散物の全重量に基づき、10重量%〜60重量%の量で存在し、かつ前記少なくとも1種のスチレン系ブロックコポリマーが、前記水性分散物の全重量に基づき、0.1重量%〜15重量%の量で存在する、請求項4または5に記載の方法。
- 前記水性分散物において、前記脂肪物質が、少なくとも1種の油から選択される、請求項1から3のいずれか一項に記載の方法。
- 前記水性分散物において、前記少なくとも1種の油の量対前記少なくとも1種のスチレン系ブロックコポリマーの量の重量比が、100:1〜1:100の範囲である、請求項7に記載の方法。
- 前記水性分散物において、前記少なくとも1種の油対前記少なくとも1種のスチレン系ブロックコポリマーの重量比が、5:1〜1000:1の範囲である、請求項7に記載の方法。
- 前記水性分散物において、前記粒子が、20μm〜70μmの範囲のピークを有する体積基準の粒径分布を有する、請求項1〜9のいずれか一項に記載の方法。
- 前記水性分散物において、前記脂肪物質が、35℃より高い融点を有する少なくとも1種のワックスおよび少なくとも1種の油を含む、請求項1〜10のいずれか一項に記載の方法。
- 前記水性分散物において、前記35℃より高い融点を有する少なくとも1種のワックスの重量による量が、前記少なくとも1種の油の重量による全量および前記少なくとも1種のスチレン系ブロックコポリマーの量以上である、請求項11に記載の方法。
- 前記水性分散物において、前記イオン性界面活性剤が、前記界面活性剤混合物の全重量に基づき、5重量%〜30重量%の量で存在する、請求項1〜12のいずれか一項に記載の方法。
- 前記水性分散物が、半結晶質ポリマー、グルタミドベースの化合物、ポリアミド、およびそれらの混合物から選択されるa1)以外の少なくとも1種の油ゲル化剤をさらに含む、請求項1〜13のいずれか一項に記載の方法。
- 前記水性分散物が、前記組成物の全重量に基づき、1重量%〜30重量%の量で前記組成物中に存在する、請求項1〜14のいずれか一項に記載の方法。
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BR112016021662B1 (pt) | 2021-01-05 |
EP3129106B2 (en) | 2021-10-27 |
KR102393235B1 (ko) | 2022-04-29 |
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US20150290109A1 (en) | 2015-10-15 |
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US10561596B2 (en) | 2020-02-18 |
BR112016021662A2 (pt) | 2017-08-15 |
KR20160147725A (ko) | 2016-12-23 |
WO2015154928A1 (en) | 2015-10-15 |
CN106170319B (zh) | 2019-12-24 |
EP3129106B1 (en) | 2018-05-23 |
JP2017510601A (ja) | 2017-04-13 |
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