JP6284437B2 - 体臭抑制剤 - Google Patents
体臭抑制剤 Download PDFInfo
- Publication number
- JP6284437B2 JP6284437B2 JP2014120875A JP2014120875A JP6284437B2 JP 6284437 B2 JP6284437 B2 JP 6284437B2 JP 2014120875 A JP2014120875 A JP 2014120875A JP 2014120875 A JP2014120875 A JP 2014120875A JP 6284437 B2 JP6284437 B2 JP 6284437B2
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- Prior art keywords
- component
- body odor
- activated carbon
- titanium oxide
- mass
- Prior art date
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- Cosmetics (AREA)
Description
成分A:ノニオン性殺菌剤
成分B:炭素数1〜3の一価アルコール
成分C:セルロース系増粘剤、及びアクリル酸系増粘剤からなる群より選ばれた増粘剤
成分D:活性炭と、上記活性炭の表面に存在する酸化チタンとを含む酸化チタン被覆活性炭
成分E:水
上記成分Aとしては、特に限定されないが、例えば、イソプロピルメチルフェノール、トリクロサン、トリクロカルバン、ピロクトンオラミン、ジンクピリチオンなどが挙げられる。中でも、イソプロピルメチルフェノール、トリクロサンが好ましい。上記成分Aは、1種のみを用いてもよいし、2種以上を用いてもよい。ノニオン性殺菌剤は、低刺激性である点や、多種の容器で使用可能な点で好ましい。
上記成分Bは、炭素数1〜3の一価アルコールである。成分Bとしては、例えば、エタノール、プロピルアルコール、イソプロピルアルコールなどが挙げられる。上記の中でも、エタノールが好ましい。成分Bは、1種のみを用いてもよいし、2種以上を用いてもよい。成分A(ノニオン性殺菌剤)は、水への溶解性が低いため、成分Bは成分Aの溶解性を高める役割を有する。
上記成分Cは、セルロース系増粘剤及びアクリル酸系増粘剤のうちの、いずれか一方または両方である。成分Cは、1種のみを用いてもよいし、2種以上を用いてもよい。
上記成分Dである酸化チタン被覆活性炭は、活性炭の表面に酸化チタンが存在する構造を有する複合体である。成分Dは、1種のみを用いてもよいし、2種以上を用いてもよい。
上記成分Eは、特に限定されないが、精製水が好ましい。本発明の体臭抑制剤中の成分Eの含有量は、特に限定されないが、乾きのはやさの観点から、本発明の体臭抑制剤100質量%に対して、15.0〜69.0質量%が好ましく、より好ましくは20.0〜59.0質量%である。
本発明の体臭抑制剤は、成分A、成分B、成分C、成分D、成分E以外の成分(その他の成分)を含んでいてもよい。その他の成分としては、例えば、界面活性剤、油脂、炭化水素油、ロウ類、高級脂肪酸、エステル油、シリコーン油、高級アルコール、多価アルコール、ステロール類、保湿剤、pH調整剤、無機顔料、色素、酸化防止剤、紫外線吸収剤、ビタミン類、収斂剤、美白剤、動植物抽出物、金属イオン封鎖剤、防腐剤、制汗成分、消臭成分、清涼化剤、香料等が挙げられる。
また、成分Dは白色であるため、本発明の体臭抑制剤を塗布した場合に、塗布対象が黒く汚れることがない。このため、皮膚、衣類や履物に塗布して用いることができ、実用適性に優れる。成分Dのかわりに、黒色の活性炭を用いた場合には、皮膚や衣類などの塗布対象が黒く汚れてしまうため、実用上これらに直接塗布して用いることができない。
活性炭(商品名「GW−B32/60」、クラレケミカル株式会社製)を解砕機を用いて破砕し、さらに分級して、平均粒径:40.9μmの活性炭(粉末活性炭)を得た。
45%アクリル酸アルキル共重合体液(商品名「ヨドゾールGH800F」、アクゾノーベル(AkzoNobel)社製)0.1gに、精製水5.1gを加え、十分に撹拌し、混合液(1)を得た。
混合液(1)2.7gを撹拌しながら、混合液(1)を上記で得られた活性炭(平均粒径:40.9μm)1.8gに混合し、混合液(2)を得た。
得られた混合液(2)に酸化チタン(商品名「CR−50」、石原産業株式会社製、平均粒径:0.25μm)10.8gを混合し、混合液(3)を得た。
次いで、得られた混合液(3)を115℃で2時間乾燥し、さらに、乾燥物を解砕機にて粉状に解砕して酸化チタン被覆活性炭(D−1)を得た。
下記組成に従い、各成分を混合し、体臭抑制剤を調製した。より具体的には、以下の通りである。
イソプロピルメチルフェノールをエタノールに混合して溶解させた後、精製水を添加して均一化した。その後、ディスパーを用いて分散させながら、酸化チタン被覆活性炭(D−1)を添加した。さらに、(アクリロイルジメチルタウリンアンモニウム/VP)コポリマーを添加、均一化して、体臭抑制剤を得た。
<組成>
イソプロピルメチルフェノール : 0.3質量%
エタノール :70.0質量%
(アクリロイルジメチルタウリンアンモニウム/VP)コポリマー: 1.5質量%
酸化チタン被覆活性炭(D−1) : 1.0質量%
精製水 :22.2質量%
クロルヒドロキシアルミニウム : 5.0質量%
下記組成に従い、実施例1と同様にして、体臭抑制剤を調製した。
<組成>
イソプロピルメチルフェノール : 0.3質量%
エタノール :70.0質量%
(アクリロイルジメチルタウリンアンモニウム/VP)コポリマー: 1.5質量%
精製水 :23.2質量%
クロルヒドロキシアルミニウム : 5.0質量%
実施例及び比較例で得られた各体臭抑制剤について、下記評価を行った。
容量140mLのガラス瓶(マヨネーズ瓶)に、各体臭抑制剤約100mLを充填し、サンプルとした。サンプルを12時間静置後、約−20℃、24時間の条件にて凍結させた後、室温下で融解させた。さらに、サンプルを、約−20℃、24時間の条件にて凍結させた後、室温下で融解させる工程を2回繰り返した(即ち、凍結・融解の工程を計3回行った)。その後、サンプルの外観を目視にて観察した。
上記評価の結果、実施例1で得られた体臭抑制剤には離漿は見られず、優れた低温安定性を有していた。一方、比較例1で得られた体臭抑制剤には離漿が見られ、サンプルは、ゲル部と液部に明確に分離しており、低温安定性に劣っていた。
被験者の腋窩を無香料石鹸で洗浄後、一方の腋窩に実施例1で得られた体臭抑制剤(塗布量:約1.0g)を塗布した(塗布部)。比較のため、もう一方の腋窩には体臭抑制剤を塗布しなかった(未塗布部)。塗布6時間後に、両方の腋窩(塗布部、未塗布部)の臭気を下記評価基準に従い、被験者8名について専門パネル3名で評価した。
<におい強度の評価基準>
0点:におわない。
1点:かすかににおう。
2点:弱くにおう。
3点:はっきりにおう。
4点:やや強くにおう。
5点:かなり強くにおう。
上記評価の結果、実施例1の体臭抑制剤は、Wilcoxon検定において有意に臭気の抑制効果を発揮していた。即ち、未塗布部に比べて塗布部の方が、におい強度の点数が低く、におい強度が弱かった。
実施例1で得られた体臭抑制剤を、被験者の上腕内側部に塗布し、塗布部を目視にて評価した。その結果、塗布部に黒い汚れ及び白浮きは見られず、実施例で得られた体臭抑制剤は塗布汚れの抑止性に優れていることがわかった。
Claims (6)
- 下記成分Aと、下記成分Bと、下記成分Cと、下記成分Dと、下記成分Eとを含有し、
前記成分Aの含有量が0.05〜1.0質量%であり、
前記成分Bの含有量が30.0〜80.0質量%であり、
前記成分Cの含有量が0.10〜2.0質量%であり、
前記成分Dの含有量が0.10〜2.0質量%であることを特徴とする体臭抑制剤。
成分A:ノニオン性殺菌剤
成分B:炭素数1〜3の一価アルコール
成分C:セルロース系増粘剤、及びアクリル酸系増粘剤からなる群より選ばれた増粘剤
成分D:活性炭と、前記活性炭の表面に存在する酸化チタンとを含み、前記活性炭100質量部に対する、前記酸化チタンの質量割合が550〜1500質量部である酸化チタン被覆活性炭
成分E:水 - 前記活性炭の平均粒径が15.0〜50.0μmである請求項1に記載の体臭抑制剤。
- 前記酸化チタンの平均粒径が0.01〜0.5μmである請求項1または2に記載の体臭抑制剤。
- 前記活性炭100質量部に対する、前記酸化チタンの質量割合が600〜1500質量部である請求項1〜3のいずれか一項に記載の体臭抑制剤。
- ジェル状体臭抑制剤である請求項1〜4のいずれか一項に記載の体臭抑制剤。
- ロールオン容器と、前記ロールオン容器内に充填されている請求項1〜5のいずれか一項に記載の体臭抑制剤とを備えるロールオン製品。
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