JP6251787B1 - 除菌用シート - Google Patents
除菌用シート Download PDFInfo
- Publication number
- JP6251787B1 JP6251787B1 JP2016160520A JP2016160520A JP6251787B1 JP 6251787 B1 JP6251787 B1 JP 6251787B1 JP 2016160520 A JP2016160520 A JP 2016160520A JP 2016160520 A JP2016160520 A JP 2016160520A JP 6251787 B1 JP6251787 B1 JP 6251787B1
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- JP
- Japan
- Prior art keywords
- sheet
- component
- impregnated
- aqueous
- sterilization
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 230000000249 desinfective effect Effects 0.000 title abstract description 25
- 238000004659 sterilization and disinfection Methods 0.000 claims abstract description 46
- 239000000645 desinfectant Substances 0.000 claims abstract description 44
- 230000001954 sterilising effect Effects 0.000 claims abstract description 42
- 239000000835 fiber Substances 0.000 claims abstract description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000007788 liquid Substances 0.000 claims abstract description 11
- 150000003242 quaternary ammonium salts Chemical class 0.000 claims abstract description 10
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 9
- 239000004094 surface-active agent Substances 0.000 claims abstract description 8
- 239000003792 electrolyte Substances 0.000 claims abstract description 7
- 239000000758 substrate Substances 0.000 claims abstract description 5
- 229920002994 synthetic fiber Polymers 0.000 claims abstract description 4
- 239000012209 synthetic fiber Substances 0.000 claims abstract description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical group [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 13
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 12
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 12
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 10
- 239000003206 sterilizing agent Substances 0.000 claims description 9
- 239000004115 Sodium Silicate Substances 0.000 claims description 8
- 229910052913 potassium silicate Inorganic materials 0.000 claims description 8
- 235000019353 potassium silicate Nutrition 0.000 claims description 8
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 8
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 8
- 239000004111 Potassium silicate Substances 0.000 claims description 7
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 7
- NNHHDJVEYQHLHG-UHFFFAOYSA-N potassium silicate Chemical compound [K+].[K+].[O-][Si]([O-])=O NNHHDJVEYQHLHG-UHFFFAOYSA-N 0.000 claims description 7
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 7
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 claims description 6
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 claims description 6
- 235000019796 monopotassium phosphate Nutrition 0.000 claims description 6
- 229910000402 monopotassium phosphate Inorganic materials 0.000 claims description 6
- 235000019799 monosodium phosphate Nutrition 0.000 claims description 6
- 229910000403 monosodium phosphate Inorganic materials 0.000 claims description 6
- PJNZPQUBCPKICU-UHFFFAOYSA-N phosphoric acid;potassium Chemical compound [K].OP(O)(O)=O PJNZPQUBCPKICU-UHFFFAOYSA-N 0.000 claims description 6
- 229910000027 potassium carbonate Inorganic materials 0.000 claims description 6
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims description 6
- UREZNYTWGJKWBI-UHFFFAOYSA-M benzethonium chloride Chemical compound [Cl-].C1=CC(C(C)(C)CC(C)(C)C)=CC=C1OCCOCC[N+](C)(C)CC1=CC=CC=C1 UREZNYTWGJKWBI-UHFFFAOYSA-M 0.000 claims description 5
- 229960001950 benzethonium chloride Drugs 0.000 claims description 5
- 239000002738 chelating agent Substances 0.000 claims description 5
- ZPWVASYFFYYZEW-UHFFFAOYSA-L dipotassium hydrogen phosphate Chemical compound [K+].[K+].OP([O-])([O-])=O ZPWVASYFFYYZEW-UHFFFAOYSA-L 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 4
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims description 4
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 4
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 4
- 229960000686 benzalkonium chloride Drugs 0.000 claims description 2
- RCTOVWPTGOZSPJ-UHFFFAOYSA-N benzyl(ethyl)azanium;chloride Chemical compound Cl.CCNCC1=CC=CC=C1 RCTOVWPTGOZSPJ-UHFFFAOYSA-N 0.000 claims description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims 1
- XIWFQDBQMCDYJT-UHFFFAOYSA-M benzyl-dimethyl-tridecylazanium;chloride Chemical compound [Cl-].CCCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 XIWFQDBQMCDYJT-UHFFFAOYSA-M 0.000 claims 1
- BDRTVPCFKSUHCJ-UHFFFAOYSA-N molecular hydrogen;potassium Chemical compound [K].[H][H] BDRTVPCFKSUHCJ-UHFFFAOYSA-N 0.000 claims 1
- 229960004418 trolamine Drugs 0.000 claims 1
- 241000700605 Viruses Species 0.000 abstract description 27
- 241000894006 Bacteria Species 0.000 abstract description 18
- 239000000463 material Substances 0.000 abstract description 15
- 230000000694 effects Effects 0.000 abstract description 14
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 abstract description 4
- 230000006866 deterioration Effects 0.000 abstract description 4
- 239000002585 base Substances 0.000 description 34
- 239000000243 solution Substances 0.000 description 25
- 238000012360 testing method Methods 0.000 description 17
- 238000011156 evaluation Methods 0.000 description 16
- 239000004745 nonwoven fabric Substances 0.000 description 16
- 239000003921 oil Substances 0.000 description 15
- 235000019198 oils Nutrition 0.000 description 15
- 239000003205 fragrance Substances 0.000 description 14
- -1 polyoxyethylene Polymers 0.000 description 14
- 238000005470 impregnation Methods 0.000 description 13
- 239000000975 dye Substances 0.000 description 12
- 238000004140 cleaning Methods 0.000 description 10
- 239000000049 pigment Substances 0.000 description 9
- 235000002639 sodium chloride Nutrition 0.000 description 9
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 8
- 125000000217 alkyl group Chemical group 0.000 description 8
- 239000000203 mixture Substances 0.000 description 8
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 7
- 239000004480 active ingredient Substances 0.000 description 7
- 230000007423 decrease Effects 0.000 description 7
- 239000012086 standard solution Substances 0.000 description 7
- 238000010998 test method Methods 0.000 description 7
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- JGFDZZLUDWMUQH-UHFFFAOYSA-N Didecyldimethylammonium Chemical compound CCCCCCCCCC[N+](C)(C)CCCCCCCCCC JGFDZZLUDWMUQH-UHFFFAOYSA-N 0.000 description 5
- 229920000297 Rayon Polymers 0.000 description 5
- 239000003513 alkali Substances 0.000 description 5
- 230000000844 anti-bacterial effect Effects 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 5
- 239000000284 extract Substances 0.000 description 5
- 238000001139 pH measurement Methods 0.000 description 5
- 235000015497 potassium bicarbonate Nutrition 0.000 description 5
- 229910000028 potassium bicarbonate Inorganic materials 0.000 description 5
- 239000011736 potassium bicarbonate Substances 0.000 description 5
- 235000011181 potassium carbonates Nutrition 0.000 description 5
- TYJJADVDDVDEDZ-UHFFFAOYSA-M potassium hydrogencarbonate Chemical compound [K+].OC([O-])=O TYJJADVDDVDEDZ-UHFFFAOYSA-M 0.000 description 5
- 239000002964 rayon Substances 0.000 description 5
- 235000017550 sodium carbonate Nutrition 0.000 description 5
- JMHWNJGXUIJPKG-UHFFFAOYSA-N CC(=O)O[SiH](CC=C)OC(C)=O Chemical compound CC(=O)O[SiH](CC=C)OC(C)=O JMHWNJGXUIJPKG-UHFFFAOYSA-N 0.000 description 4
- RUPBZQFQVRMKDG-UHFFFAOYSA-M Didecyldimethylammonium chloride Chemical compound [Cl-].CCCCCCCCCC[N+](C)(C)CCCCCCCCCC RUPBZQFQVRMKDG-UHFFFAOYSA-M 0.000 description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- 206010059866 Drug resistance Diseases 0.000 description 4
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 4
- 230000001580 bacterial effect Effects 0.000 description 4
- 229940078672 didecyldimethylammonium Drugs 0.000 description 4
- 229960004670 didecyldimethylammonium chloride Drugs 0.000 description 4
- 238000002845 discoloration Methods 0.000 description 4
- 229940079593 drug Drugs 0.000 description 4
- 239000003814 drug Substances 0.000 description 4
- 235000013305 food Nutrition 0.000 description 4
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 4
- 239000002953 phosphate buffered saline Substances 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 239000011780 sodium chloride Substances 0.000 description 4
- 238000001179 sorption measurement Methods 0.000 description 4
- 229910001220 stainless steel Inorganic materials 0.000 description 4
- 239000010935 stainless steel Substances 0.000 description 4
- LWIHDJKSTIGBAC-UHFFFAOYSA-K tripotassium phosphate Chemical compound [K+].[K+].[K+].[O-]P([O-])([O-])=O LWIHDJKSTIGBAC-UHFFFAOYSA-K 0.000 description 4
- 230000009385 viral infection Effects 0.000 description 4
- CIEZZGWIJBXOTE-UHFFFAOYSA-N 2-[bis(carboxymethyl)amino]propanoic acid Chemical compound OC(=O)C(C)N(CC(O)=O)CC(O)=O CIEZZGWIJBXOTE-UHFFFAOYSA-N 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 3
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- WEEGYLXZBRQIMU-UHFFFAOYSA-N Eucalyptol Chemical compound C1CC2CCC1(C)OC2(C)C WEEGYLXZBRQIMU-UHFFFAOYSA-N 0.000 description 3
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 3
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- WNLRTRBMVRJNCN-UHFFFAOYSA-L adipate(2-) Chemical compound [O-]C(=O)CCCCC([O-])=O WNLRTRBMVRJNCN-UHFFFAOYSA-L 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 238000009826 distribution Methods 0.000 description 3
- 230000007613 environmental effect Effects 0.000 description 3
- 238000005187 foaming Methods 0.000 description 3
- 208000015181 infectious disease Diseases 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- GYHFUZHODSMOHU-UHFFFAOYSA-N nonanal Chemical compound CCCCCCCCC=O GYHFUZHODSMOHU-UHFFFAOYSA-N 0.000 description 3
- 239000002736 nonionic surfactant Substances 0.000 description 3
- 239000003960 organic solvent Substances 0.000 description 3
- 239000001103 potassium chloride Substances 0.000 description 3
- 235000011164 potassium chloride Nutrition 0.000 description 3
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 3
- 239000001509 sodium citrate Substances 0.000 description 3
- 229910052938 sodium sulfate Inorganic materials 0.000 description 3
- 235000011152 sodium sulphate Nutrition 0.000 description 3
- 239000011550 stock solution Substances 0.000 description 3
- KYWIYKKSMDLRDC-UHFFFAOYSA-N undecan-2-one Chemical compound CCCCCCCCCC(C)=O KYWIYKKSMDLRDC-UHFFFAOYSA-N 0.000 description 3
- KMPQYAYAQWNLME-UHFFFAOYSA-N undecanal Chemical compound CCCCCCCCCCC=O KMPQYAYAQWNLME-UHFFFAOYSA-N 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- XHXUANMFYXWVNG-ADEWGFFLSA-N (-)-Menthyl acetate Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1OC(C)=O XHXUANMFYXWVNG-ADEWGFFLSA-N 0.000 description 2
- GRWFGVWFFZKLTI-IUCAKERBSA-N (-)-α-pinene Chemical compound CC1=CC[C@@H]2C(C)(C)[C@H]1C2 GRWFGVWFFZKLTI-IUCAKERBSA-N 0.000 description 2
- GXANMBISFKBPEX-ONEGZZNKSA-N (e)-hex-3-enal Chemical compound CC\C=C\CC=O GXANMBISFKBPEX-ONEGZZNKSA-N 0.000 description 2
- DHKHKXVYLBGOIT-UHFFFAOYSA-N 1,1-Diethoxyethane Chemical compound CCOC(C)OCC DHKHKXVYLBGOIT-UHFFFAOYSA-N 0.000 description 2
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 2
- YIWUKEYIRIRTPP-UHFFFAOYSA-N 2-ethylhexan-1-ol Chemical compound CCCCC(CC)CO YIWUKEYIRIRTPP-UHFFFAOYSA-N 0.000 description 2
- NGDNVOAEIVQRFH-UHFFFAOYSA-N 2-nonanol Chemical compound CCCCCCCC(C)O NGDNVOAEIVQRFH-UHFFFAOYSA-N 0.000 description 2
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 description 2
- HNVRRHSXBLFLIG-UHFFFAOYSA-N 3-hydroxy-3-methylbut-1-ene Chemical compound CC(C)(O)C=C HNVRRHSXBLFLIG-UHFFFAOYSA-N 0.000 description 2
- IWTBVKIGCDZRPL-UHFFFAOYSA-N 3-methylpentanol Chemical compound CCC(C)CCO IWTBVKIGCDZRPL-UHFFFAOYSA-N 0.000 description 2
- GNKZMNRKLCTJAY-UHFFFAOYSA-N 4'-Methylacetophenone Chemical compound CC(=O)C1=CC=C(C)C=C1 GNKZMNRKLCTJAY-UHFFFAOYSA-N 0.000 description 2
- DKKRDMLKVSKFMJ-UHFFFAOYSA-N 4-propan-2-ylcyclohexan-1-ol Chemical compound CC(C)C1CCC(O)CC1 DKKRDMLKVSKFMJ-UHFFFAOYSA-N 0.000 description 2
- KWOLFJPFCHCOCG-UHFFFAOYSA-N Acetophenone Chemical compound CC(=O)C1=CC=CC=C1 KWOLFJPFCHCOCG-UHFFFAOYSA-N 0.000 description 2
- 108091003079 Bovine Serum Albumin Proteins 0.000 description 2
- ZTQSAGDEMFDKMZ-UHFFFAOYSA-N Butyraldehyde Chemical compound CCCC=O ZTQSAGDEMFDKMZ-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- RGHNJXZEOKUKBD-SQOUGZDYSA-M D-gluconate Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O RGHNJXZEOKUKBD-SQOUGZDYSA-M 0.000 description 2
- RGHNJXZEOKUKBD-SQOUGZDYSA-N D-gluconic acid Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O RGHNJXZEOKUKBD-SQOUGZDYSA-N 0.000 description 2
- NUPSHWCALHZGOV-UHFFFAOYSA-N Decyl acetate Chemical compound CCCCCCCCCCOC(C)=O NUPSHWCALHZGOV-UHFFFAOYSA-N 0.000 description 2
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 2
- FHUODBDRWMIBQP-UHFFFAOYSA-N Ethyl p-anisate Chemical compound CCOC(=O)C1=CC=C(OC)C=C1 FHUODBDRWMIBQP-UHFFFAOYSA-N 0.000 description 2
- 241000233866 Fungi Species 0.000 description 2
- 240000001972 Gardenia jasminoides Species 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 2
- AEMRFAOFKBGASW-UHFFFAOYSA-N Glycolic acid Chemical compound OCC(O)=O AEMRFAOFKBGASW-UHFFFAOYSA-N 0.000 description 2
- RZKSECIXORKHQS-UHFFFAOYSA-N Heptan-3-ol Chemical compound CCCCC(O)CC RZKSECIXORKHQS-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- AMIMRNSIRUDHCM-UHFFFAOYSA-N Isopropylaldehyde Chemical compound CC(C)C=O AMIMRNSIRUDHCM-UHFFFAOYSA-N 0.000 description 2
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 description 2
- CRZQGDNQQAALAY-UHFFFAOYSA-N Methyl benzeneacetate Chemical compound COC(=O)CC1=CC=CC=C1 CRZQGDNQQAALAY-UHFFFAOYSA-N 0.000 description 2
- FSVCELGFZIQNCK-UHFFFAOYSA-N N,N-bis(2-hydroxyethyl)glycine Chemical compound OCCN(CCO)CC(O)=O FSVCELGFZIQNCK-UHFFFAOYSA-N 0.000 description 2
- JYXGIOKAKDAARW-UHFFFAOYSA-N N-(2-hydroxyethyl)iminodiacetic acid Chemical compound OCCN(CC(O)=O)CC(O)=O JYXGIOKAKDAARW-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 description 2
- 229940022663 acetate Drugs 0.000 description 2
- 229940024606 amino acid Drugs 0.000 description 2
- 235000001014 amino acid Nutrition 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- HUMNYLRZRPPJDN-UHFFFAOYSA-N benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 description 2
- QUKGYYKBILRGFE-UHFFFAOYSA-N benzyl acetate Chemical compound CC(=O)OCC1=CC=CC=C1 QUKGYYKBILRGFE-UHFFFAOYSA-N 0.000 description 2
- SESFRYSPDFLNCH-UHFFFAOYSA-N benzyl benzoate Chemical compound C=1C=CC=CC=1C(=O)OCC1=CC=CC=C1 SESFRYSPDFLNCH-UHFFFAOYSA-N 0.000 description 2
- CADWTSSKOVRVJC-UHFFFAOYSA-N benzyl(dimethyl)azanium;chloride Chemical compound [Cl-].C[NH+](C)CC1=CC=CC=C1 CADWTSSKOVRVJC-UHFFFAOYSA-N 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- CRPUJAZIXJMDBK-UHFFFAOYSA-N camphene Chemical compound C1CC2C(=C)C(C)(C)C1C2 CRPUJAZIXJMDBK-UHFFFAOYSA-N 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- ULDHMXUKGWMISQ-UHFFFAOYSA-N carvone Chemical compound CC(=C)C1CC=C(C)C(=O)C1 ULDHMXUKGWMISQ-UHFFFAOYSA-N 0.000 description 2
- 239000003093 cationic surfactant Substances 0.000 description 2
- ONTQJDKFANPPKK-UHFFFAOYSA-L chembl3185981 Chemical compound [Na+].[Na+].CC1=CC(C)=C(S([O-])(=O)=O)C=C1N=NC1=CC(S([O-])(=O)=O)=C(C=CC=C2)C2=C1O ONTQJDKFANPPKK-UHFFFAOYSA-L 0.000 description 2
- NEHNMFOYXAPHSD-UHFFFAOYSA-N citronellal Chemical compound O=CCC(C)CCC=C(C)C NEHNMFOYXAPHSD-UHFFFAOYSA-N 0.000 description 2
- QMVPMAAFGQKVCJ-UHFFFAOYSA-N citronellol Chemical compound OCCC(C)CCC=C(C)C QMVPMAAFGQKVCJ-UHFFFAOYSA-N 0.000 description 2
- 230000000120 cytopathologic effect Effects 0.000 description 2
- MMFCJPPRCYDLLZ-UHFFFAOYSA-N dec-2-enal Chemical compound CCCCCCCC=CC=O MMFCJPPRCYDLLZ-UHFFFAOYSA-N 0.000 description 2
- KSMVZQYAVGTKIV-UHFFFAOYSA-N decanal Chemical compound CCCCCCCCCC=O KSMVZQYAVGTKIV-UHFFFAOYSA-N 0.000 description 2
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- RLQWHDODQVOVKU-UHFFFAOYSA-N tetrapotassium;silicate Chemical compound [K+].[K+].[K+].[K+].[O-][Si]([O-])([O-])[O-] RLQWHDODQVOVKU-UHFFFAOYSA-N 0.000 description 1
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Landscapes
- Cleaning Implements For Floors, Carpets, Furniture, Walls, And The Like (AREA)
- Apparatus For Disinfection Or Sterilisation (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Description
(1)液体の保持が可能な基材シートに対して水性除菌剤が含浸された除菌用シートにおいて、前記水性除菌剤が(A)成分として第四級アンモニウム塩型界面活性剤、(B)成分として無機電解質、(C)成分として(B)成分を除くアルカリ剤、(D)成分として水を含有していて、前記(B)成分が、炭酸ナトリウム又は炭酸カリウムと、炭酸水素ナトリウム又は炭酸水素カリウムとの組み合わせ、もしくはリン酸二水素ナトリウム又はリン酸二水素カリウムと、リン酸水素二ナトリウム又はリン酸水素二カリウムとの組み合わせであり、基材シートに含浸されている水性除菌剤のpHが9.8以上、12.0以下であり、
前記基材シートが、再生繊維からなるか、又は再生繊維に、合成系繊維、天然繊維のうちの少なくとも1種を混合してなる混合繊維よりなることを特徴とする除菌用シート、
(2)基材シートに含浸されている水性除菌剤が、基材シート100質量部あたり、150質量部以上、350質量部以下である上記(1)の除菌用シート、
(3)基材シートに含浸されている水性除菌剤中の(A)成分が0.00045質量%以上、20質量%以下であることを特徴とする上記(1)又は(2)の除菌用シート、
(4)(A)成分が、塩化ベンザルコニウム、塩化ベンゼトニウム、ジアルキルジメチルアンモニウムクロライド、エチルベンジルアンモニウムクロライドより選ばれた少なくとも1種であることを特徴とする上記(1)から(3)のいずれかの除菌用シート、
(5)(C)成分が、水酸化ナトリウム、水酸化カリウム、珪酸ナトリウム、珪酸カリウム、モノエタノールアミン、ジエタノールアミン、トリエタノールアミンより選ばれた少なくとも1種であることを特徴とする上記(1)から(4)のいずれかの除菌用シート、
(6)前記水性除菌剤が、(E)成分としてキレート剤を含有する上記(1)から(5)のいずれかの除菌用シート、
を要旨とするものである。
(A)成分以外の界面活性剤は洗浄性向上の点で、水性除菌剤中に0.001質量%以上、5質量%以下配合することが好ましく、0.01質量%以上、3質量%以下配合することがより好ましい。
芳香成分としては、従来公知の各種の芳香剤や芳香を有する天然物等に含有されるものを特に制限なく用いることができ、例えば、天然香料としては、アニス油、バジル油、ベルガモット油、シダー油、クローブ油、コリアンダー油、ユーカリ油、フェンネル油、ガルバヌム油、ゼラニウム油、ジャスミンアブソリュート、ラバンジン油、ラベンダー油、レモングラス油、レモン油、ラベンダースパイク油、ネロリ油、オークモスアブソリュート、パチョリ油、ぺチグレン油、パイン油、ローズ油、ローズマリー油、クラリーセージ油、サンダルウッド油、タイム油、トンカアブソリュート、チュベローズアブソリュート、ベチバー油、イランイラン油、ペパーミント油、しょう脳油、芳油、ペリラ油、スペアミント油、スターアニス油、ライム油、オコチア油、テレピン油、ナツメグ油、シトロネラ油、ボアドローズ油、カナンガ油、カルダモン油、カシア油、オレンジ油、マンダリン油、タンジェリン油、ベイ油、エレミ油、ヒバ油、桧油、グレープフルーツ油、ゆず油等が挙げられる。
合成系色素としては、具体的には、例えば、赤色1号、赤色2号、赤色3号、赤色4号、赤色5号、赤色101号、赤色102号、赤色103号、赤色104号、赤色105号、赤色106号、橙色1号、橙色2号、黄色1号、黄色2号、黄色3号、黄色4号、黄色5号、緑色1号、緑色2号、緑色3号、青色1号、青色2号、紫色1号、食用混合色素等を挙げることができる。
(A)成分
A−1:オクチルデシルジメチルアンモニウムクロライド
A−2:ジオクチルジメチルアンモニウムクロライド
A−3:ジデシルジメチルアンモニウムクロライド
A−4:アルキル(C12〜16)ジメチルベンジルアンモニウムクロライド
(A´)成分〔(A)成分の比較成分〕
A´−1:N−アルキル(C14〜18)トリメチレンジアミンオレイン酸塩
A´−2:アルキル(C8〜18)アミン酢酸塩
B−1:炭酸ナトリウム
B−2:炭酸水素ナトリウム
B−3:セスキ炭酸ナトリウム
B−4:硫酸ナトリウム
B−5:塩化ナトリウム
B−6:クエン酸ナトリウム
B−7:リン酸水素二ナトリウム
B−8:リン酸二水素ナトリウム
B−9:炭酸カリウム
B−10:炭酸水素カリウム
(B´)成分〔(B)成分の比較成分〕
B´−1:ポリアクリル酸ナトリウム(重量平均分子量:4,500)
B´−2:グリセリン
C−1:モノエタノールアミン
C−2:メタケイ酸ナトリウム・5水塩
C−3:水酸化ナトリウム
C−4:水酸化カリウム
D−1:水
E−1:エチレンジアミン四酢酸・四ナトリウム塩(EDTA−4Na)
E−2:メチルグリシン二酢酸・三ナトリウム塩(MGDA−3Na)
(F)成分
F−1:非イオン界面活性剤1[ポリオキシエチレン(EO:6.5モル)アルキル(C9〜11)エーテル]
F−2:非イオン界面活性剤2[ポリオキシエチレン(EO:25モル)アルキル(獣脂脂肪)エーテル]
F−3:オクチルジメチルアミンオキシド
G−1:イソプロピルアルコール
表1から表10に示す配合に基づき水性除菌剤を調製した。表に示す再生繊維を含む不織布の基材シートに、基材シート100質量部当たり表に示す含浸量となるように各水性除菌剤を24時間含浸させて除菌用シートとした。万力を用いて除菌用シートを10N・cmの力で10分間締め込み、搾出された溶液(以下、搾出液という)のpH、有効(A)成分量、除菌用シートの洗浄性、除菌性、除ウイルス性、吸着防止性、また、水性除菌剤の不織布に対する薬剤耐性、除菌用シートの使用感、被清掃素材の磨耗、除菌用シート中の薬剤の偏在等の性状を評価した。結果を表1から10にあわせて示す。
<pHメーターの校正>
pHメーター(HORIBA製;pH/イオンメーター F−23)にpH測定用複合電極(HORIBA製;ガラス摺り合わせスリーブ型)を接続し、電源を入れる。pH電極内部液としては、飽和塩化カリウム水溶液(3.33mol/L)を使用した。次に、pH4.01標準液(フタル酸塩標準液)、pH6.86標準液(中性リン酸塩標準液)、pH9.18標準液(ホウ酸塩標準液)をそれぞれ100mLビーカーに充填し、25℃の恒温槽に30分間浸漬した。恒温に調整された標準液にpH測定用電極を3分間浸し、pH6.86、pH9.18、pH4.01の順に校正操作を行った。
<pH測定>
恒温槽内にて25℃の恒温に調整された搾出液100mLにpH測定用電極を3分間浸し、pHを測定した。
搾出液8mLをビーカーにとり、搾出液に0.25MのpH5.7の酢酸ナトリウム緩衝液1mL、6×10−4MのクロムアズロールS溶液1mLを順次加え、磁気攪拌機で攪拌しながら、2.0mol/Lラウリル硫酸ナトリウム水溶液で滴定して搾出液中の(A)成分量を求めた。滴定の終点は、溶液が紫からオレンジに色調変化することを目視によって判定した。
試験方法:
ステンレス板(15×50mm)に擬似血液(牛血精製物:アルブミン、ヘモグロビン、フィブリノーゲン、トロンビン)を付着させた洗浄度評価インジケーター〔Pereg社製、商品名:TOSI〕を試験片とし質量を測定した。この試験片を搾出液200mLに浸漬し、5分間放置した後、イオン交換水ですすぎ、自然乾燥させた後、質量を測定した。洗浄率を洗浄前後の試験片の質量変化により算出し、次の尺度で示した。
評価基準:
◎:洗浄率80%以上、100%以下
○:洗浄率60%以上、80%未満
△:洗浄率40%以上、60%未満
×:洗浄率40%未満
とし、△、○、◎を実用性のあるものとして判定した。
試験方法:
供試菌株をSCDブイヨン培地で培養して2.0×108CFU/mL以上、9.0×108CFU/mL以下になるように菌数を調製して菌液とした。搾出液10mLに、各供試菌液0.1mLを添加し、25℃にて15分間接触させた後、滅菌中和溶液(SCDLP培地)を加えよく攪拌した。一般細菌として、Pseudomonas aeruginosa NBRC13736(108CFU/mLレベル)、Staphylococcus aureus NBRC13276(108CFU/mLレベル)、Escherichia coli ATCC11229(108CFU/mLレベル)、Alcaligenes faecalis NBRC14479(108CFU/mLレベル)、Serratia marcescens NBRC12648(108CFU/mLレベル)を用いた。
この1mLをSCD寒天培地で混釈培養し生菌数を確認し、下記の基準で評価した。
評価基準:
1点:供試菌のLog reductionが5以上の菌数減少
2点:供試菌のLog reductionが4以上、5未満の菌数減少
3点:供試菌のLog reductionが3以上、4未満の菌数減少
4点:供試菌のLog reductionが3未満の菌数減少
として上記各菌種について菌数減少を点数で評価し、菌数減少の点数の平均値を求め、以下の基準で除菌性を評価した。
◎:平均値が1.0点以上、1.5点未満。
〇:平均値が1.5点以上、2.5点未満。
△:平均値が2.5点以上、3.5点未満。
×:平均値が3.5以上。
とし、△、○、◎を実用性のあるものとして判定した。
試験方法:
試験管に0.9mLの搾出液とそれぞれ108TCID50/mLとなるように調整したウイルス液0.1mLを加え、ミキサーで混合し、25℃で10分間作用させた。作用後0.1mLをサンプリングし、9.9mLの作用停止液(2%チオ硫酸ナトリウム、0.2%レシチン及び1.5%ポリソルベート80を含む細胞増殖液)に添加して100倍希釈後、ウイルスに対する水性除菌剤(搾出液)の作用を停止させた。これをウイルス感染価測定用資料原液として感染価の測定に用いた。同様に、搾出液の代わりに、リン酸緩衝生理食塩水(phosphate bufferred saline、以下、PBSと略すことがある)を用いた試験を実施し、コントロールとした。リン酸緩衝生理食塩水は、塩化ナトリウム8g、塩化カリウム0.2g、リン酸水素二ナトリウム1.44g、リン酸二水素カリウム0.24gの4種類の塩を混合し、超純水で900mLに溶解後、塩酸でpHを7.4に調整する。1Lにメスアップ後、オートクレーブにより滅菌する。ウイルスとして、ネコカリシウイルス、マウスノロウイルス、B型肝炎ウイルス、C型肝炎ウイルス、アデノウイルス、AIDSウイルス、インフルエンザウイルスを用いた。
ウイルス感染価測定用試料原液をPBSで10倍段階希釈した後、感染価測定用試料原液及び希釈ウイルス液50μLとウシ胎仔血清(FBS)を5%添加したDulbecco‘s modified Eagle’s Medium(DMEM)に懸濁した細胞を96ウェルプレートに植え込んだ。その後、炭酸ガスふ卵器において37℃、5%CO2の条件で4日間培養した。培養後、倒立顕微鏡下でウイルスの増殖によるCPE(細胞変性効果)の有無を観察し、Reed−Muench法を用いてウイルス感染価(TCID50/mL)を求め、下記の基準で評価した。
評価基準:
1点:ウイルス感染価のLog reductionが5以上の減少
2点:ウイルス感染価のLog reductionが4以上、5未満の減少
3点:ウイルス感染価のLog reductionが3以上、4未満の減少
4点:ウイルス感染価のLog reductionが3未満の減少
として上記各ウイルスについてウイルス感染価の減少を点数で評価し平均値を求め、以下の基準で除ウイルス性を評価した。
◎:平均値が1.0点以上、1.5点未満。
〇:平均値が1.5点以上、2.5点未満。
△:平均値が2.5点以上、3.5点未満。
×:平均値が3.5以上。
とし、△、○、◎を実用性のあるものとして判定した。
搾出液について有効成分量を測定し、含浸前の溶液の測定値と比較し、溶液中の成分の不織布への吸着度合を評価した。有効成分量(陽イオン界面活性剤量)測定方法は、含浸前後の有効成分を測定し、下記の基準で評価した。
評価基準:
◎:有効成分量が含浸前の80%以上、100%以下
〇:有効成分量が含浸前の60%以上、80%未満
△:有効成分量が含浸前の40%以上、60%未満
×:有効成分量が含浸前の40%未満
とし、△、○、◎を実用性のあるものとして判定した。
試験方法:
表1から表10に示す各種素材からなる不織布(200mm×250mm)を10枚用い、各供試水性除菌剤200mLに含浸させ、40℃で1週間保存した後、不織布の外観変化を目視によって観察した。
評価基準:
◎:変色や劣化が発生していない。
○:薄い変色や軽微な劣化が発生している。
△:部分的に濃い変色や強い劣化が発生している。
×:全体的に濃い変色や強い劣化が発生している。
とし、△、○、◎を実用性のあるものとして判定した。
試験方法:
表1から表10に示す各種素材からなる不織布(200mm×250mm)を10枚用い、各供試水性除菌剤200mLに含浸させ、十分に薬液が行き渡ったことを確認した後、薬液が染み込んだ不織布を1枚取り出し、清浄なステンレス表面を約30センチメートル四方に渡って、上下5回左右5回ふき取りを行い、泡立ちやべたつき水っぽさやごわごわ感・湿り気などの観点から官能試験によって使用感を確認した。また、パネラーは無作為に選定し、それぞれのサンプルにつきn=10とした。評価結果の解析には統計処理を行い、最も評価が多い項目を評価結果として採用した。
評価基準:
○:泡立ち・べたつき・水っぽさ・ごわごわ感がなく、適度な湿り気があり使用感が良い。
△:やや泡立ち・べたつき・水っぽさ・ごわごわ感がある、もしくは適度な湿り気がない。
×:泡立ち・べたつき・水っぽさ・ごわごわ感が非常に強い、もしくはほとんど湿り気がなく使用感が悪い。
とし、△、○を実用性のあるものとして判定した。
試験方法:
表1から表10に示す各種素材からなる不織布(200mm×250mm)を10枚用い、各供試水性除菌剤200mLに含浸させ、十分に薬液が行き渡ったことを確認した後、薬液が染み込んだ不織布を1枚取り出し、清浄なステンレス表面を約30センチメートル四方に渡って、上下5回左右5回ふき取りを行った。その後、ステンレス表面に発生した傷について目視によって観察した。
評価基準:
◎:傷が見られない。
○:部分的にやや浅い傷が見られる。
△:部分的に深い傷が見られる。
×:全体的に深い傷が見られる。
とし、△、○、◎を実用性のあるものとして判定した。
試験方法:
表8から表10に示す各種素材からなる不織布(200mm×250mm×300枚)を容量3Lのポリプロピレン製の袋に入れて、各供試水性除菌剤2Lを含浸させ、25℃にて24時間保存した後、縦半分に裁断し、中心部分まで薬液が染み込んでいるかを目視によって観察した。
評価基準:
◎:全体にまんべんなく薬液が染み込んでいる。
○:ほとんど全体的に薬液が染み込んでいる。
△:一部染み込んでいない部分がある。
×:いたるところに染み込んでいない部分がある。
とし、△、○、◎を実用性のあるものとして判定した。
Claims (6)
- 液体の保持が可能な基材シートに対して水性除菌剤が含浸された除菌用シートにおいて、前記水性除菌剤が(A)成分として第四級アンモニウム塩型界面活性剤、(B)成分として無機電解質、(C)成分として(B)成分を除くアルカリ剤、(D)成分として水を含有していて、前記(B)成分が、炭酸ナトリウム又は炭酸カリウムと、炭酸水素ナトリウム又は炭酸水素カリウムとの組み合わせ、もしくはリン酸二水素ナトリウム又はリン酸二水素カリウムと、リン酸水素二ナトリウム又はリン酸水素二カリウムとの組み合わせであり、基材シートに含浸されている水性除菌剤のpHが9.8以上、12.0以下であり、
前記基材シートが、再生繊維からなるか、又は再生繊維に、合成系繊維、天然繊維のうちの少なくとも1種を混合してなる混合繊維よりなることを特徴とする除菌用シート。 - 基材シートに含浸されている水性除菌剤が、基材シート100質量部あたり、150質量部以上、350質量部以下である請求項1記載の除菌用シート。
- 基材シートに含浸されている水性除菌剤中の(A)成分が0.00045質量%以上、20質量%以下であることを特徴とする請求項1又は2に記載の除菌用シート。
- (A)成分が、塩化ベンザルコニウム、塩化ベンゼトニウム、ジアルキルジメチルアンモニウムクロライド、エチルベンジルアンモニウムクロライドより選ばれた少なくとも1種であることを特徴とする請求項1から3のいずれかに記載の除菌用シート。
- (C)成分が、水酸化ナトリウム、水酸化カリウム、珪酸ナトリウム、珪酸カリウム、モノエタノールアミン、ジエタノールアミン、トリエタノールアミンより選ばれた少なくとも1種であることを特徴とする請求項1から4のいずれかに記載の除菌用シート。
- 前記水性除菌剤が、(E)成分としてキレート剤を含有する請求項1から5のいずれかに記載の除菌用シート。
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