JP6236465B2 - 温度安定性クロキントセット−メキシル水性組成物 - Google Patents
温度安定性クロキントセット−メキシル水性組成物 Download PDFInfo
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- JP6236465B2 JP6236465B2 JP2015549730A JP2015549730A JP6236465B2 JP 6236465 B2 JP6236465 B2 JP 6236465B2 JP 2015549730 A JP2015549730 A JP 2015549730A JP 2015549730 A JP2015549730 A JP 2015549730A JP 6236465 B2 JP6236465 B2 JP 6236465B2
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- 239000003813 safflower oil Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 239000003352 sequestering agent Substances 0.000 description 1
- 239000008159 sesame oil Substances 0.000 description 1
- 235000011803 sesame oil Nutrition 0.000 description 1
- 238000005029 sieve analysis Methods 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- ODCWYMIRDDJXKW-UHFFFAOYSA-N simazine Chemical compound CCNC1=NC(Cl)=NC(NCC)=N1 ODCWYMIRDDJXKW-UHFFFAOYSA-N 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 235000012424 soybean oil Nutrition 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- FRGKKTITADJNOE-UHFFFAOYSA-N sulfanyloxyethane Chemical compound CCOS FRGKKTITADJNOE-UHFFFAOYSA-N 0.000 description 1
- OORLZFUTLGXMEF-UHFFFAOYSA-N sulfentrazone Chemical compound O=C1N(C(F)F)C(C)=NN1C1=CC(NS(C)(=O)=O)=C(Cl)C=C1Cl OORLZFUTLGXMEF-UHFFFAOYSA-N 0.000 description 1
- FZMKKCQHDROFNI-UHFFFAOYSA-N sulfometuron Chemical compound CC1=CC(C)=NC(NC(=O)NS(=O)(=O)C=2C(=CC=CC=2)C(O)=O)=N1 FZMKKCQHDROFNI-UHFFFAOYSA-N 0.000 description 1
- 239000002600 sunflower oil Substances 0.000 description 1
- 235000020238 sunflower seed Nutrition 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- 235000012222 talc Nutrition 0.000 description 1
- UJMBCXLDXJUMFB-GLCFPVLVSA-K tartrazine Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)C1=NN(C=2C=CC(=CC=2)S([O-])(=O)=O)C(=O)C1\N=N\C1=CC=C(S([O-])(=O)=O)C=C1 UJMBCXLDXJUMFB-GLCFPVLVSA-K 0.000 description 1
- 235000012756 tartrazine Nutrition 0.000 description 1
- 239000004149 tartrazine Substances 0.000 description 1
- IROINLKCQGIITA-UHFFFAOYSA-N terbutryn Chemical compound CCNC1=NC(NC(C)(C)C)=NC(SC)=N1 IROINLKCQGIITA-UHFFFAOYSA-N 0.000 description 1
- XSKZXGDFSCCXQX-UHFFFAOYSA-N thiencarbazone-methyl Chemical compound COC(=O)C1=CSC(C)=C1S(=O)(=O)NC(=O)N1C(=O)N(C)C(OC)=N1 XSKZXGDFSCCXQX-UHFFFAOYSA-N 0.000 description 1
- LOQQVLXUKHKNIA-UHFFFAOYSA-N thifensulfuron Chemical compound COC1=NC(C)=NC(NC(=O)NS(=O)(=O)C2=C(SC=C2)C(O)=O)=N1 LOQQVLXUKHKNIA-UHFFFAOYSA-N 0.000 description 1
- 235000010215 titanium dioxide Nutrition 0.000 description 1
- IYMLUHWAJFXAQP-UHFFFAOYSA-N topramezone Chemical compound CC1=C(C(=O)C2=C(N(C)N=C2)O)C=CC(S(C)(=O)=O)=C1C1=NOCC1 IYMLUHWAJFXAQP-UHFFFAOYSA-N 0.000 description 1
- DQFPEYARZIQXRM-LTGZKZEYSA-N tralkoxydim Chemical compound C1C(=O)C(C(/CC)=N/OCC)=C(O)CC1C1=C(C)C=C(C)C=C1C DQFPEYARZIQXRM-LTGZKZEYSA-N 0.000 description 1
- XOPFESVZMSQIKC-UHFFFAOYSA-N triasulfuron Chemical compound COC1=NC(C)=NC(NC(=O)NS(=O)(=O)C=2C(=CC=CC=2)OCCCl)=N1 XOPFESVZMSQIKC-UHFFFAOYSA-N 0.000 description 1
- BQZXUHDXIARLEO-UHFFFAOYSA-N tribenuron Chemical compound COC1=NC(C)=NC(N(C)C(=O)NS(=O)(=O)C=2C(=CC=CC=2)C(O)=O)=N1 BQZXUHDXIARLEO-UHFFFAOYSA-N 0.000 description 1
- YMXOXAPKZDWXLY-QWRGUYRKSA-N tribenuron methyl Chemical group COC(=O)[C@H]1CCCC[C@@H]1S(=O)(=O)NC(=O)N(C)C1=NC(C)=NC(OC)=N1 YMXOXAPKZDWXLY-QWRGUYRKSA-N 0.000 description 1
- ZSDSQXJSNMTJDA-UHFFFAOYSA-N trifluralin Chemical compound CCCN(CCC)C1=C([N+]([O-])=O)C=C(C(F)(F)F)C=C1[N+]([O-])=O ZSDSQXJSNMTJDA-UHFFFAOYSA-N 0.000 description 1
- 239000002383 tung oil Substances 0.000 description 1
- 230000017260 vegetative to reproductive phase transition of meristem Effects 0.000 description 1
- 235000020234 walnut Nutrition 0.000 description 1
- 239000004562 water dispersible granule Substances 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
- 239000000230 xanthan gum Substances 0.000 description 1
- 229920001285 xanthan gum Polymers 0.000 description 1
- 235000010493 xanthan gum Nutrition 0.000 description 1
- 229940082509 xanthan gum Drugs 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/22—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing ingredients stabilising the active ingredients
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
- A01N43/42—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings condensed with carbocyclic rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/32—Ingredients for reducing the noxious effect of the active substances to organisms other than pests, e.g. toxicity reducing compositions, self-destructing compositions
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Environmental Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Zoology (AREA)
- Plant Pathology (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Medicinal Preparation (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
Description
本出願は、参照によりその開示が本明細書に明確に組み込まれている、2012年12月21日に出願された米国仮特許出願第61/745,110号の利益を主張する。
結晶成長を防ぐことおよび水和CQCM(クロキントセット−メキシル)水性懸濁組成物に対して粒径安定性をもたらすことについての評価
例示的な水和CQCM懸濁状濃縮組成物を表1に示す。
ピロキシスラムを含有する水和CQCM懸濁状濃縮組成物
実施例1において、ETHOMEEN T/25は、結晶成長を抑制することが示された。MORWET D−425は、ある程度の結晶成長抑制を与え、さらには組成物に対して良好な分散特性を与えることが示された。引き続き、(結晶成長を抑制する)ETHOMEEN C/25と(良好な分散特性を与える)MORWET D−425とを含有する水和CQCM懸濁状濃縮組成物を評価した。
Claims (34)
- 水和クロキントセット−メキシルの水性懸濁液の結晶成長を抑制する方法であって、
水和クロキントセット−メキシルの水性懸濁液を、牛脂アミンアルコキシレート、ココアミンアルコキシレート、およびこれらの混合物からなる群から選択される界面活性剤に接触させて、安定化された組成物を生成することを含む方法。 - 水和クロキントセット−メキシルの水性懸濁液を安定化させる方法であって、
水和クロキントセット−メキシルの水性懸濁液を、牛脂アミンアルコキシレート、ココアミンアルコキシレート、およびこれらの混合物からなる群から選択される界面活性剤に接触させて、安定化された組成物を形成することを含み、
前記安定化された組成物が30℃以上の温度で安定している、方法。 - 前記安定化された組成物が、30℃〜45℃の温度で安定している、請求項1または2に記載の方法。
- 前記安定化された組成物が、少なくとも1年間、30℃から45℃の温度で安定している、請求項1〜3のいずれか一項に記載の方法。
- 前記界面活性剤がエトキシ化されている、請求項1〜4のいずれか一項に記載の方法。
- 前記界面活性剤が、平均で10〜20モルのエチレンオキシドを含む、請求項5に記載の方法。
- 前記界面活性剤が、平均で12〜15モルのエチレンオキシドを含む、請求項6に記載の方法。
- 前記安定化された組成物が、農薬をさらに含む、請求項1〜7のいずれか一項に記載の方法。
- 前記農薬が、クロジナホップ−プロパギル、フルピルスルフロン、ピロキシスラム、および4−アミノピコリン酸系除草剤からなる群から選択される、請求項8に記載の方法。
- 前記農薬がピロキシスラムを含む、請求項8に記載の方法。
- 水和クロキントセット−メキシルと前記農薬との重量比が、1:1〜9:1である、請求項8〜10のいずれか一項に記載の方法。
- 前記安定化された組成物が、150g/L〜225g/Lの水和クロキントセット−メキシルを含む、請求項1〜11のいずれかに記載の方法。
- 前記安定化された組成物が、前記安定化された組成物の物理的安定性および分散を促進するために有効な量の追加的な界面活性剤をさらに含む、請求項1〜12のいずれかに記載の方法。
- 水和クロキントセット−メキシルの安定化された水性組成物を作製する方法であって、
無水クロキントセット−メキシルを、水および湿潤界面活性剤を含む水性組成物と混合して、水性クロキントセット−メキシル組成物を形成することと;
無水クロキントセット−メキシルの少なくとも95%を水和クロキントセット−メキシルに変換することと;
牛脂アミンアルコキシレート、ココアミンアルコキシレート、またはこれらの組み合わせを含む安定化界面活性剤を、水性の水和クロキントセット−メキシル組成物と混合することと;
得られる生成物を粉砕することと
を含む方法。 - 前記安定化界面活性剤がエトキシ化されている、請求項14に記載の方法。
- 前記安定化界面活性剤が、平均で10〜20モルのエチレンオキシドを含む、請求項15に記載の方法。
- 前記安定化界面活性剤が、平均で12〜15モルのエチレンオキシドを含む、請求項16に記載の方法。
- 農薬を、得られた生成物と合わせる、請求項14〜17のいずれか一項に記載の方法。
- 前記農薬が、クロジナホップ−プロパギル、フルピルスルフロン、ピロキシスラム、および4−アミノピコリン酸系除草剤からなる群から選択される、請求項18に記載の方法。
- 前記農薬がピロキシスラムを含む、請求項18に記載の方法。
- 水和クロキントセット−メキシルと前記農薬との重量比が、1:1〜9:1である、請求項18〜20のいずれか一項に記載の方法。
- 前記安定化された組成物が、150g/L〜225g/Lの水和クロキントセット−メキシルを含む、請求項18〜21のいずれかに記載の方法。
- 前記組成物の物理的安定性および分散を促進するために有効な量の追加的な界面活性剤を添加することをさらに含む、請求項14〜22のいずれかに記載の方法。
- 水和クロキントセット−メキシルと;
牛脂アミンアルコキシレート、ココアミンアルコキシレート、またはこれらの組み合わせを含む界面活性剤と;
水と
を含む温度安定性水性組成物。 - 懸濁状濃縮物である、請求項24に記載の組成物。
- 前記界面活性剤がエトキシ化されている、請求項24〜25のいずれか一項に記載の組成物。
- 前記界面活性剤が、平均で10〜20モルのエチレンオキシドを含む、請求項26に記載の組成物。
- 前記界面活性剤が、平均で12〜15モルのエチレンオキシドを含む、請求項26に記載の組成物。
- 農薬をさらに含む、請求項24〜28のいずれか一項に記載の組成物。
- 前記農薬が、クロジナホップ−プロパギル、フルピルスルフロン、ピロキシスラム、および4−アミノピコリン酸系除草剤からなる群から選択される、請求項29に記載の組成物。
- 前記農薬がピロキシスラムを含む、請求項29に記載の組成物。
- 水和クロキントセット−メキシルと前記農薬との重量比が、1:1〜9:1である、請求項29〜31のいずれか一項に記載の組成物。
- 150g/L〜225g/Lの水和クロキントセット−メキシルを含む、請求項29〜32のいずれかに記載の組成物。
- 前記組成物の物理的安定性および分散を促進するために有効な量の追加的な界面活性剤をさらに含む、請求項24〜33のいずれかに記載の組成物。
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PCT/US2013/076668 WO2014100465A2 (en) | 2012-12-21 | 2013-12-19 | Temperature stable cloquintocet-mexyl aqueous compositions |
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