JP5992336B2 - 固液抽出 - Google Patents
固液抽出 Download PDFInfo
- Publication number
- JP5992336B2 JP5992336B2 JP2012550474A JP2012550474A JP5992336B2 JP 5992336 B2 JP5992336 B2 JP 5992336B2 JP 2012550474 A JP2012550474 A JP 2012550474A JP 2012550474 A JP2012550474 A JP 2012550474A JP 5992336 B2 JP5992336 B2 JP 5992336B2
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- JP
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- solvent
- oil
- saponifiable
- solvent system
- fraction
- Prior art date
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- 239000002904 solvent Substances 0.000 claims description 91
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- 238000000034 method Methods 0.000 claims description 53
- 239000003921 oil Substances 0.000 claims description 51
- JWUJQDFVADABEY-UHFFFAOYSA-N 2-methyltetrahydrofuran Chemical compound CC1CCCO1 JWUJQDFVADABEY-UHFFFAOYSA-N 0.000 claims description 39
- 238000000605 extraction Methods 0.000 claims description 35
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- 235000008673 Persea americana Nutrition 0.000 claims description 20
- UQEAIHBTYFGYIE-UHFFFAOYSA-N hexamethyldisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)C UQEAIHBTYFGYIE-UHFFFAOYSA-N 0.000 claims description 17
- GETTZEONDQJALK-UHFFFAOYSA-N (trifluoromethyl)benzene Chemical compound FC(F)(F)C1=CC=CC=C1 GETTZEONDQJALK-UHFFFAOYSA-N 0.000 claims description 15
- ZQBFAOFFOQMSGJ-UHFFFAOYSA-N hexafluorobenzene Chemical compound FC1=C(F)C(F)=C(F)C(F)=C1F ZQBFAOFFOQMSGJ-UHFFFAOYSA-N 0.000 claims description 15
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- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 9
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- MJYQFWSXKFLTAY-OVEQLNGDSA-N (2r,3r)-2,3-bis[(4-hydroxy-3-methoxyphenyl)methyl]butane-1,4-diol;(2r,3r,4s,5s,6r)-6-(hydroxymethyl)oxane-2,3,4,5-tetrol Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O.C1=C(O)C(OC)=CC(C[C@@H](CO)[C@H](CO)CC=2C=C(OC)C(O)=CC=2)=C1 MJYQFWSXKFLTAY-OVEQLNGDSA-N 0.000 claims description 2
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- 235000013311 vegetables Nutrition 0.000 claims description 2
- 235000020234 walnut Nutrition 0.000 claims description 2
- NUMQCACRALPSHD-VWNJCJTFSA-N 2-ethoxy-2-methylpropane Chemical group CCOC([13CH3])([13CH3])[13CH3] NUMQCACRALPSHD-VWNJCJTFSA-N 0.000 claims 1
- 235000011437 Amygdalus communis Nutrition 0.000 claims 1
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- 229940087559 grape seed Drugs 0.000 claims 1
- UIUXUFNYAYAMOE-UHFFFAOYSA-N methylsilane Chemical compound [SiH3]C UIUXUFNYAYAMOE-UHFFFAOYSA-N 0.000 claims 1
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 60
- 235000019198 oils Nutrition 0.000 description 41
- BZLVMXJERCGZMT-UHFFFAOYSA-N Methyl tert-butyl ether Chemical compound COC(C)(C)C BZLVMXJERCGZMT-UHFFFAOYSA-N 0.000 description 39
- 235000014121 butter Nutrition 0.000 description 30
- CZDYPVPMEAXLPK-UHFFFAOYSA-N tetramethylsilane Chemical compound C[Si](C)(C)C CZDYPVPMEAXLPK-UHFFFAOYSA-N 0.000 description 10
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 8
- 239000000126 substance Substances 0.000 description 8
- 235000015112 vegetable and seed oil Nutrition 0.000 description 8
- 239000008158 vegetable oil Substances 0.000 description 8
- 239000002537 cosmetic Substances 0.000 description 7
- AQEFLFZSWDEAIP-UHFFFAOYSA-N di-tert-butyl ether Chemical compound CC(C)(C)OC(C)(C)C AQEFLFZSWDEAIP-UHFFFAOYSA-N 0.000 description 6
- 239000003549 soybean oil Substances 0.000 description 6
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- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 4
- 125000001931 aliphatic group Chemical group 0.000 description 4
- 235000015872 dietary supplement Nutrition 0.000 description 4
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- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 4
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- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
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Classifications
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- A23L13/40—Meat products; Meat meal; Preparation or treatment thereof containing additives
- A23L13/45—Addition of, or treatment with, microorganisms
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- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
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- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
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- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
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- A23L33/115—Fatty acids or derivatives thereof; Fats or oils
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- A—HUMAN NECESSITIES
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- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
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- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/20—Reducing nutritive value; Dietetic products with reduced nutritive value
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- A61K36/06—Fungi, e.g. yeasts
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- A61K36/185—Magnoliopsida (dicotyledons)
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/286—Carthamus (distaff thistle)
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Description
− 第一の溶媒系であって、フッ素化芳香族溶媒、特にトリフルオロトルエン(BTF)およびヘキサフルオロベンゼン(BHF)、tert‐ブチルエーテル、特にエチル‐tert‐ブチル‐エーテル(ETBE)とも称される2‐エトキシ‐2‐メチルプロパンおよび2‐メトキシ‐2‐メチルプロパンもしくはメチル‐tert‐ブチルエーテル(MTBE)、少なくとも1つのケイ素原子を含有する溶媒、特にヘキサメチルジシロキサン(HMDS)およびテトラメチルシラン(TMS)、メチル‐テトラヒドロフラン(MeTHF)、ならびにこれらの混合物、の中から選択される溶媒を、溶媒系の全体積の少なくとも50体積%の濃度で含む第一の溶媒系、を用いた少なくとも1つの固体植物質または微生物の固液抽出工程、
− 所望により、特に非けん化性成分に富む、油またはバターを含む画分の回収工程、
を含む。
− 第一の溶媒系であって、フッ素化芳香族溶媒、特にトリフルオロトルエン(BTF)およびヘキサフルオロベンゼン(BHF)、tert‐ブチルエーテル、特にエチル‐tert‐ブチル‐エーテル(ETBE)とも称される2‐エトキシ‐2‐メチルプロパンおよび2‐メトキシ‐2‐メチルプロパンもしくはメチル‐tert‐ブチルエーテル(MTBE)、少なくとも1つのケイ素原子を含有する溶媒、特にヘキサメチルジシロキサン(HMDS)およびテトラメチルシラン(TMS)、メチル‐テトラヒドロフラン(MeTHF)、ならびにこれらの混合物、の中から選択される溶媒を、溶媒系の全体積の少なくとも50体積%の濃度で含む第一の溶媒系、を用いた少なくとも1つの固体植物質または微生物の固液抽出工程、
− 所望により、油もしくはバターに富む有機溶液の回収、または、油もしくはバターの回収、特に非けん化性成分に富む前記油もしくはバターの回収工程、
− 特にけん化およびエステル化の中から選択される工程による、前記油もしくはバターの水性アルコール溶液への変換工程、
− この水性アルコール溶液の抽出であって、脂肪画分は、液液抽出または蒸留により非けん化性画分から分離される、抽出工程、ならびに、
− 特に部分または全非けん化性画分の回収工程、
を含む。
乾燥アボカドからの抽出を、ヘキサン(参照)、および以下の溶媒:HMDS、MeTHF、BTF、BHF、MTBE、ETBE、により行った。
凍結乾燥アボカドパルプ粉末を、ヘキサン(参照)、および以下の溶媒:HMDS、MeTHF、BTF、MTBE、ETBE、により、実施例1に記載の方法に従って抽出した。結果を表2に示す。
乾燥アボカドからの抽出を、ヘキサン(参照)、および以下の溶媒:BTFおよびETBE、により行う。
乾燥コレラからの抽出を、ヘキサン(参照)、および以下の溶媒:BTFおよびMTBE、により、実施例1に記載の方法に従って行った。結果を表4に示す。
Claims (14)
- 全または部分非けん化性画分を得るための方法であって、以下の工程:
− 第一の溶媒系であって、フッ素化芳香族溶媒、エチル‐tert‐ブチル‐エーテル(ETBE)、少なくとも1つのケイ素原子を含有する溶媒、メチル‐テトラヒドロフラン(MeTHF)、およびこれらの混合物の中から選択される溶媒を、前記溶媒系の全体積の少なくとも50体積%の濃度で含む第一の溶媒系、を用いた少なくとも1つの固体植物質または微生物の固液抽出工程、
− 油もしくは脂に富む有機溶液の回収工程、または、前記油もしくは脂の回収工程、
− けん化またはエステル化による、前記油もしくは脂の水性アルコール溶液への変換工程、
− 前記水性アルコール溶液の抽出であって、脂肪画分は、液液抽出により前記非けん化性画分から分離される、抽出工程、ならびに、
− 前記非けん化性画分の回収工程、
を含む、方法。 - 前記油または脂は、非けん化性成分含有量が高い、請求項1に記載の方法。
- 前記第一の溶媒系が、フッ素化芳香族溶媒、エチル‐tert‐ブチル‐エーテル(ETBE)、少なくとも1つのケイ素原子を含有する溶媒、メチル‐テトラヒドロフラン(MeTHF)、およびこれらの混合物の中から選択される溶媒を、前記第一の溶媒系の全体積に対して少なくとも75体積%の濃度で含むことを特徴とする、請求項1または2に記載の方法。
- 前記第一の溶媒系が、2‐エトキシ‐2‐メチルプロパン(ETBE)、メチル‐テトラヒドロフラン(MeTHF)、トリフルオロトルエン(BTF)、ヘキサフルオロベンゼン(BHF)、ヘキサメチルジシロキサン(HMDS)、テトラメチルシラン(TMS)、またはこれらの混合物から成ることを特徴とする、請求項1〜3のいずれか一項に記載の方法。
- 前記第一の溶媒系が、フッ素化芳香族溶媒、エチル‐tert‐ブチル‐エーテル(ETBE)、少なくとも1つのケイ素原子を含有する溶媒、メチル‐テトラヒドロフラン(MeTHF)、およびこれらの混合物の中から選択される溶媒を、前記第一の溶媒系の全体積に対して少なくとも90体積%の濃度で含むことを特徴とする、請求項1〜4のいずれか一項に記載の方法。
- 前記油が、前記第一の溶媒系からの少なくとも1つの溶媒を含むかまたはそれから成る第二の溶媒系中にて、水性アルコール溶液へ変換されることを特徴とする、請求項1〜5のいずれか一項に記載の方法。
- 前記第二の溶媒系が、メチル‐テトラヒドロフラン(MeTHF)である、請求項6に記載の方法。
- 前記変換が、油または脂に富む有機溶液ベース上、油または脂に富む前記有機溶液の全質量に対して少なくとも2質量%の油を含む前記有機溶液ベース上で直接行われることを特徴とする、請求項1〜7のいずれか一項に記載の方法。
- 前記変換が、少なくとも50質量%の他の溶媒が添加された、または他の溶媒は添加されない、部分的に蒸発させた画分に対して行われることを特徴とする、請求項8に記載の方法。
- C2〜C4のアルコール、メチルテトラヒドロフラン(MeTHF)、およびこれらの混合物などの少なくとも1つの他の溶媒の少なくとも10%を、油に富む前記蒸発させた画分へ添加してよいことを特徴とする、請求項8に記載の方法。
- 前記第一および第二の溶媒系が、メチルテトラヒドロフラン(MeTHF)を含むことを特徴とする、請求項5〜10のいずれか一項に記載の方法。
- 前記水性アルコール溶液の前記抽出が、前記第一および/もしくは第二の溶媒系で用いられたものと同じ溶媒のすべてまたは一部を含む第三の溶媒系によって実施される液液抽出を用いて行われることを特徴とする、請求項1〜11のいずれか一項に記載の方法。
- 前記固体植物質または前記微生物が、ダイズ、アブラナ、トウモロコシ、ヒマワリ、ゴマ、ルピナス、ワタ、ココナツ、オリーブ、アボカド、カカオ、イリッペ、シアバターノキ、パーム核、ピーナッツ、コプラ、アマニ、ヒマ、ブドウ種子、ヒョウタン(gourd)種子、クロフサスグリ種子、メロン種子、トマト種子、カボチャ種子、アーモンド、へーゼルナッツ、クルミ、マツヨイグサ、ルリヂシャ、ベニバナ、カメリナ、ケシ種子、大型藻類、微細藻類、ヘマトココカス、ドゥナリエラ、スピルリナ、コレラなど、ならびに/または微生物、酵母、カビ、および細菌およびこれらの混合物から得られるものであることを特徴とする、請求項1〜12のいずれか一項に記載の方法。
- 得られる前記非けん化性成分が、ダイズ非けん化性成分、アボカド非けん化性成分、フラン画分に富むアボカド非けん化性成分および/またはステロール画分に富むアボカド非けん化性成分、ならびに、アボカドおよびダイズ非けん化性成分の混合物(ASU)の中から選択されることを特徴とする、請求項1〜13のいずれか一項に記載の方法。
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FR2955783B1 (fr) | 2014-02-07 |
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FR2955783A1 (fr) | 2011-08-05 |
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EP2528458A2 (fr) | 2012-12-05 |
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PL2528458T3 (pl) | 2020-05-18 |
LT2528458T (lt) | 2020-02-25 |
RS59903B1 (sr) | 2020-03-31 |
EP3613412A1 (fr) | 2020-02-26 |
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