JP5869137B2 - 補助電源ユニット用途における水素化脱硫ユニットおよび固体酸化物形燃料電池システムの組み合わせへの送達のための非触媒水素発生プロセス - Google Patents
補助電源ユニット用途における水素化脱硫ユニットおよび固体酸化物形燃料電池システムの組み合わせへの送達のための非触媒水素発生プロセス Download PDFInfo
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M8/00—Fuel cells; Manufacture thereof
- H01M8/06—Combination of fuel cells with means for production of reactants or for treatment of residues
- H01M8/0606—Combination of fuel cells with means for production of reactants or for treatment of residues with means for production of gaseous reactants
- H01M8/0612—Combination of fuel cells with means for production of reactants or for treatment of residues with means for production of gaseous reactants from carbon-containing material
- H01M8/0625—Combination of fuel cells with means for production of reactants or for treatment of residues with means for production of gaseous reactants from carbon-containing material in a modular combined reactor/fuel cell structure
- H01M8/0631—Reactor construction specially adapted for combination reactor/fuel cell
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
- B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G25/00—Refining of hydrocarbon oils in the absence of hydrogen, with solid sorbents
- C10G25/003—Specific sorbent material, not covered by C10G25/02 or C10G25/03
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G35/00—Reforming naphtha
- C10G35/02—Thermal reforming
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
- C10G45/02—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G63/00—Treatment of naphtha by at least one reforming process and at least one other conversion process
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M8/00—Fuel cells; Manufacture thereof
- H01M8/06—Combination of fuel cells with means for production of reactants or for treatment of residues
- H01M8/0606—Combination of fuel cells with means for production of reactants or for treatment of residues with means for production of gaseous reactants
- H01M8/0612—Combination of fuel cells with means for production of reactants or for treatment of residues with means for production of gaseous reactants from carbon-containing material
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M8/00—Fuel cells; Manufacture thereof
- H01M8/06—Combination of fuel cells with means for production of reactants or for treatment of residues
- H01M8/0662—Treatment of gaseous reactants or gaseous residues, e.g. cleaning
- H01M8/0675—Removal of sulfur
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M8/00—Fuel cells; Manufacture thereof
- H01M8/22—Fuel cells in which the fuel is based on materials comprising carbon or oxygen or hydrogen and other elements; Fuel cells in which the fuel is based on materials comprising only elements other than carbon, oxygen or hydrogen
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2257/00—Components to be removed
- B01D2257/30—Sulfur compounds
- B01D2257/304—Hydrogen sulfide
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
- C10G2300/40—Characteristics of the process deviating from typical ways of processing
- C10G2300/42—Hydrogen of special source or of special composition
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/50—Fuel cells
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P30/00—Technologies relating to oil refining and petrochemical industry
- Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Manufacturing & Machinery (AREA)
- Life Sciences & Earth Sciences (AREA)
- Sustainable Development (AREA)
- Sustainable Energy (AREA)
- Electrochemistry (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Analytical Chemistry (AREA)
- Hydrogen, Water And Hydrids (AREA)
- Fuel Cell (AREA)
- Catalysts (AREA)
Description
表1.ディーゼル燃料供給原料
Claims (15)
- 硫黄含有炭化水素燃料流から硫黄を除去するための装置であって、
前記硫黄含有炭化水素燃料流から水素含有生成物ガス流を生成するように構成されている統合された非触媒改質器と、
前記硫黄含有炭化水素燃料流を水素化脱硫ユニットに送達するように構成されている供給材料ラインであって、硫黄含有化合物を除去するための炭化水素燃料流の前処理をせずに、前記硫黄含有炭化水素燃料流の一部を前記統合された非触媒改質器に導くように動作可能な、供給材料ラインと、
前記水素含有生成物ガス流を前記統合された非触媒改質器から前記水素化脱硫ユニットに送達するように構成されている、改質器出口ラインであって、前記水素化脱硫ユニットが、水素化脱硫触媒を含み、前記水素化脱硫ユニットが、前記硫黄含有炭化水素燃料流中の硫黄化合物を硫化水素に変換して、硫化水素を含有する処理済炭化水素燃料流を生成するように構成されている、改質器出口ラインと、
硫化水素を含有する前記処理済炭化水素燃料流を前記水素化脱硫ユニットから吸着器に送達するように構成されている、水素化脱硫ユニット出口ラインであって、前記吸着器が、硫化水素を含有する前記処理済炭化水素燃料流から硫化水素を除去して、脱硫炭化水素燃料流を生成するように動作可能である吸着剤を含む吸着剤層を備える、水素化脱硫ユニット出口ラインと、
を備える、装置。 - 前記脱硫炭化水素燃料流を固体酸化物形燃料電池に送達するように構成されている吸着剤出口ラインを更に備え、前記固体酸化物形燃料電池が、前記脱硫炭化水素燃料流を電気に変換するように構成されている、請求項1に記載の装置。
- 前記水素化脱硫ユニットに必要な水素の量に応じて、前記統合された非触媒改質器に供給される前記硫黄含有炭化水素燃料流の量を制御するように動作可能な、請求項1または2のいずれかに記載の装置。
- 前記吸着剤が酸化亜鉛を含む、請求項1〜3のいずれかに記載の装置。
- 前記装置が、約1ppm未満の総硫黄を含有する脱硫炭化水素燃料流を生成するように
動作可能である、請求項1〜4のいずれかに記載の装置。 - 硫黄含有炭化水素燃料流から電気を生成する方法であって、
硫黄含有化合物を除去するための炭化水素燃料流の前処理をせずに、前記硫黄含有炭化水素燃料流の少なくとも一部を統合された非触媒改質器に供給して、水素含有生成物流を発生するステップと、
前記改質器からの前記水素含有生成物流および前記炭化水素燃料流の少なくとも一部を、水素化脱硫ユニットに供給するステップと、
前記水素化脱硫ユニット内で前記硫黄含有炭化水素燃料流を脱硫して、硫化水素含有炭化水素燃料流を生成するステップと、
前記水素化脱硫からの前記硫化水素含有炭化水素燃料流を、吸着器に供給するステップであって、前記吸着器が、前記炭化水素燃料流から硫化水素を除去して、脱硫炭化水素燃料流を生成するように動作可能である、ステップと、
前記脱硫炭化水素燃料流を固体酸化物形燃料電池に供給するステップであって、前記固体酸化物形燃料電池が、前記脱硫炭化水素燃料流から電気を生成するように構成されている、ステップと、
を含む、方法。 - 水および酸素を前記非触媒改質器に供給することを更に含み、前記硫黄含有炭化水素燃料流、水、および酸素の反応が、水素を含む生成物流を生成するように動作可能である、請求項6に記載の方法。
- 前記生成物流が約50〜53.6%の水素ガスを含む、請求項6または7のいずれかに記載の方法。
- 前記吸着器が、酸化亜鉛を含む吸着剤層を含む、請求項6〜8のいずれかに記載の方法。
- 前記脱硫炭化水素燃料流が約1ppm未満の硫黄を含む、請求項6〜9のいずれかに記載の方法。
- 前記脱硫炭化水素燃料流が約0.5ppm未満の硫黄を含む、請求項6〜10のいずれかに記載の方法。
- 連続動作の際に、前記硫黄含有炭化水素燃料流の約5〜22%が前記改質器に供給される、請求項6〜11のいずれかに記載の方法。
- 連続動作の際に、前記硫黄含有炭化水素燃料流の約10.4〜14.8%が前記改質器に供給される、請求項6〜12のいずれかに記載の方法。
- 前記水素化脱硫ユニットに供給された水素と硫黄含有炭化水素燃料の比が、約100:1〜500:1である、請求項6〜13のいずれかに記載の方法。
- 始動すると、前記炭化水素燃料の全てが、前記水素含有生成物流の生成のために前記改質器に供給される、請求項6〜14のいずれかに記載の方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
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US201161547562P | 2011-10-14 | 2011-10-14 | |
US61/547,562 | 2011-10-14 | ||
PCT/US2012/059935 WO2013101328A2 (en) | 2011-10-14 | 2012-10-12 | A non-catalytic hydrogen generation process for delivery to a hydrodesulfurization unit and solid oxide fuel cell system combination for auxiliary power unit application |
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JP2015501345A JP2015501345A (ja) | 2015-01-15 |
JP5869137B2 true JP5869137B2 (ja) | 2016-02-24 |
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Country Status (6)
Country | Link |
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US (2) | US10056631B2 (ja) |
EP (1) | EP2766457A2 (ja) |
JP (1) | JP5869137B2 (ja) |
KR (1) | KR101952986B1 (ja) |
CN (1) | CN104220558B (ja) |
WO (1) | WO2013101328A2 (ja) |
Families Citing this family (2)
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US11952275B1 (en) * | 2017-06-13 | 2024-04-09 | The Government Of The United States, As Represented By The Secretary Of The Army | Methods and systems for distributed reforming of hydrocarbon fuels for enhanced hydrogen production |
WO2022001985A1 (en) * | 2020-06-29 | 2022-01-06 | Ceres Intellectual Property Company Limited | Natural gas desulfurization apparatus |
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JP5057315B2 (ja) * | 1998-10-30 | 2012-10-24 | 日揮株式会社 | ガスタービン燃料油の製造方法 |
AUPR324201A0 (en) * | 2001-02-21 | 2001-03-15 | Ceramic Fuel Cells Limited | Fuel cell system |
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CA2628970C (en) * | 2004-11-08 | 2014-01-21 | Trustees Of Tufts College | Apparatus and methods for non-regenerative and regenerative hot gas desulfurization |
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-
2012
- 2012-10-12 JP JP2014535917A patent/JP5869137B2/ja not_active Expired - Fee Related
- 2012-10-12 US US13/650,674 patent/US10056631B2/en active Active
- 2012-10-12 CN CN201280050437.5A patent/CN104220558B/zh not_active Expired - Fee Related
- 2012-10-12 KR KR1020147012625A patent/KR101952986B1/ko active IP Right Grant
- 2012-10-12 EP EP12846794.1A patent/EP2766457A2/en not_active Ceased
- 2012-10-12 WO PCT/US2012/059935 patent/WO2013101328A2/en active Application Filing
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- 2018-07-18 US US16/039,040 patent/US10833341B2/en active Active
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EP2766457A2 (en) | 2014-08-20 |
US10833341B2 (en) | 2020-11-10 |
US10056631B2 (en) | 2018-08-21 |
JP2015501345A (ja) | 2015-01-15 |
CN104220558A (zh) | 2014-12-17 |
CN104220558B (zh) | 2016-06-01 |
KR20140116057A (ko) | 2014-10-01 |
KR101952986B1 (ko) | 2019-02-27 |
US20180323458A1 (en) | 2018-11-08 |
WO2013101328A3 (en) | 2013-10-17 |
US20140065501A1 (en) | 2014-03-06 |
WO2013101328A2 (en) | 2013-07-04 |
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