JP5597456B2 - 誘電体の厚さ設定方法、及び電極に設けられた誘電体を備える基板処理装置 - Google Patents
誘電体の厚さ設定方法、及び電極に設けられた誘電体を備える基板処理装置 Download PDFInfo
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- 239000000758 substrate Substances 0.000 title claims description 68
- 238000000034 method Methods 0.000 title claims description 33
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 49
- 239000003990 capacitor Substances 0.000 claims description 27
- 235000012239 silicon dioxide Nutrition 0.000 claims description 26
- 239000000377 silicon dioxide Substances 0.000 claims description 23
- 230000009467 reduction Effects 0.000 claims description 13
- 238000005530 etching Methods 0.000 claims description 10
- 230000007423 decrease Effects 0.000 claims description 6
- 230000008569 process Effects 0.000 description 10
- 238000001312 dry etching Methods 0.000 description 9
- 230000008859 change Effects 0.000 description 5
- 239000004065 semiconductor Substances 0.000 description 4
- 238000001816 cooling Methods 0.000 description 3
- 239000010453 quartz Substances 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000004020 conductor Substances 0.000 description 2
- 230000005684 electric field Effects 0.000 description 2
- 230000007246 mechanism Effects 0.000 description 2
- 230000000149 penetrating effect Effects 0.000 description 2
- 238000009832 plasma treatment Methods 0.000 description 2
- 229910004298 SiO 2 Inorganic materials 0.000 description 1
- 238000004380 ashing Methods 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000011038 discontinuous diafiltration by volume reduction Methods 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 239000012212 insulator Substances 0.000 description 1
- 239000011229 interlayer Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000004973 liquid crystal related substance Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910021421 monocrystalline silicon Inorganic materials 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 238000011282 treatment Methods 0.000 description 1
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/32—Gas-filled discharge tubes
- H01J37/32009—Arrangements for generation of plasma specially adapted for examination or treatment of objects, e.g. plasma sources
- H01J37/32082—Radio frequency generated discharge
- H01J37/32091—Radio frequency generated discharge the radio frequency energy being capacitively coupled to the plasma
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/32—Gas-filled discharge tubes
- H01J37/32009—Arrangements for generation of plasma specially adapted for examination or treatment of objects, e.g. plasma sources
- H01J37/32082—Radio frequency generated discharge
- H01J37/32137—Radio frequency generated discharge controlling of the discharge by modulation of energy
- H01J37/32155—Frequency modulation
- H01J37/32165—Plural frequencies
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/32—Gas-filled discharge tubes
- H01J37/32431—Constructional details of the reactor
- H01J37/32532—Electrodes
- H01J37/3255—Material
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- Analytical Chemistry (AREA)
- Drying Of Semiconductors (AREA)
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Description
K = 1/(d1+d2) … (1)
ここで、容量低下率Kは、キャパシタC1及びキャパシタC2を直列接続したときの各キャパシタC1,C2に蓄えられる電荷の低下率とも考えられるため、例えば、キャパシタC2をキャパシタC1に直列接続することによってキャパシタC1の電位差も容量低下率Kにしたがって低下する。例えば、直列接続する前のキャパシタC1の電位差をVpreとし、直列接続した後のキャパシタC1の電位差をVaftとすると、電位差Vaftは下記式(2)で表される。
Vaft = K×Vpre … (2)
また、バイアス電力の周波数及びバイアス電力の電力値に対するプラズマの電位(正確には、チャンバ11の壁面に対するプラズマの電位)の変化形態は基板処理装置の種類毎に異なり、基板処理装置10において上部電極24に誘電体26が設けられない仕様では、チャンバ11内の圧力が30mTorr(4.00Pa)、プラズマ生成用電力の電力値が1500W、混合ガスの流量比がC4F6:C4F8:Ar:O2=30:15:450:50sccmである場合(以下、「処理条件A」という。)のプラズマの電位の変化形態は、図2のグラフに示す通りである。また、プラズマの電位の変化形態は、チャンバ11内におけるアノード電極のカソード電極に対する面積比(いわゆる、アノード/カソード比(以下、「A/C比」という。))によっても異なる。図2のグラフでは、バイアス電力の周波数が2MHzであってA/C比が6の場合のデータを「◆」で示し、バイアス電力の周波数が13MHzであってA/C比が4の場合のデータを「■」で示し、バイアス電力の周波数が13MHzであってA/C比が6の場合のデータを「▲」で示す。
λD = 7.43×103×(Te/Ne/106)0.5×103 mm … (3)
d = 0.606×λD×(2×V0/Te)0.75 mm … (4)
λDはデバイ長であり、V0はプラズマポテンシャルであり、dはシース長である。
0.50 > 1/(0.97+ddi) … (5)
上記式(5)より、誘電体26の厚さddiは下記式(6)を満たす必要があり、
0.97+ddi > 2 … (6)
その結果、誘電体26の厚さddiを1.03mmより大きくする必要がある。
第1の処理条件:チャンバ11内の圧力が60mTorr(8.00Pa)、プラズマ生成用電力の電力値が500W、バイアス電力の電力値が500W、CF4の流量が140sccm、処理継続時間が20秒間
第2の処理条件:チャンバ11内の圧力が30mTorr、プラズマ生成用電力の電力値が2700W、バイアス電力の電力値が2000W、混合ガスの流量比がCHF3:Ar:O2=100:1000:30sccm、処理継続時間が50秒間
第3の処理条件:チャンバ11内の圧力が40mTorr(5.33Pa)、プラズマ生成用電力の電力値が2700W、バイアス電力の電力値が3000W、混合ガスの流量比がC4F6:Ar:O2=30:1100:20sccm、処理継続時間が450秒間
その後、誘電体26の中心から半径方向に30mmの点、同100mmの点及び同150mmの点における消耗量を測定したところ、各点での消耗量は順に0.022mm、0.012mm及び0.000mmであり、誘電体26の全面に関するエッチレートの平均は0.25μm/時間であった。
W ウエハ
10 基板処理装置
11 チャンバ
12 サセプタ
24 上部電極
26 誘電体
Claims (7)
- プラズマが内部に発生する処理室と、該処理室内に配置されて基板を載置する載置台と、該載置台に対向する電極と、該電極において前記載置された基板に対向するように設けられた誘電体とを備え、該誘電体は二酸化硅素からなり、前記載置台には互いに周波数が異なる2つの高周波電力が印加され、前記基板に形成された二酸化硅素膜をプラズマでエッチングする基板処理装置における、誘電体の厚さ設定方法であって、
前記2つの高周波電力のうち周波数が低い高周波電力の電力値と、前記処理室内におけるアノード電極のカソード電極に対する面積比とに基づいて、前記電極に誘電体が設けられていない場合の前記電極に対向するプラズマの電位を推定し、
前記推定されたプラズマの電位へ、前記誘電体の容量及び該誘電体の表面近傍に生じるシースの容量を合成したときの容量低下率を乗じて得られるプラズマの電位が100eV以下となるように、前記誘電体の厚さを設定し、
前記カソード電極は、前記基板処理装置の構成部品であって、前記処理室内へ露出し且つ前記周波数が低い高周波電力の電源へ電気的に接続される構成部品の表面であり、前記アノード電極は、前記基板処理装置の構成部品であって、前記処理室内へ露出し且つ接地へ電気的に接続される構成部品の表面であることを特徴とする誘電体の厚さ設定方法。 - 前記容量低下率を算出する際、前記シース及び前記誘電体を互いに電気的に直列接続されたキャパシタとみなすことを特徴とする請求項1記載の誘電体の厚さ設定方法。
- 前記容量低下率を算出する際、前記誘電体の厚さを、該誘電体の誘電率が真空の誘電率となった場合の厚さに換算することを特徴とする請求項1又は2記載の誘電体の厚さ設定方法。
- 前記容量低下率を算出する際、前記推定されたプラズマの電位に基づいて前記シースの厚さを算出する請求項1乃至3のいずれか1項に記載の誘電体の厚さ設定方法。
- プラズマが内部に発生する処理室と、該処理室内に配置されて基板を載置する載置台と、該載置台に対向する電極と、該電極において前記載置された基板に対向するように設けられた誘電体とを備え、該誘電体は二酸化硅素からなり、前記載置台には互いに周波数が異なる2つの高周波電力が印加され、前記基板に形成された二酸化硅素膜をプラズマでエッチングする基板処理装置であって、
前記誘電体の厚さは、前記2つの高周波電力のうち周波数が低い高周波電力の電力値と、前記処理室内におけるアノード電極のカソード電極に対する面積比とに基づいて、前記電極に誘電体が設けられていない場合の前記電極に対向するプラズマの電位を推定し、前記推定されたプラズマの電位へ、前記誘電体の容量及び該誘電体の表面近傍に生じるシースの容量を合成したときの容量低下率を乗じて得られるプラズマの電位が100eV以下となるように、設定され、
前記カソード電極は、前記基板処理装置の構成部品であって、前記処理室内へ露出し且つ前記周波数が低い高周波電力の電源へ電気的に接続される構成部品の表面であり、前記アノード電極は、前記基板処理装置の構成部品であって、前記処理室内へ露出し且つ接地へ電気的に接続される構成部品の表面であることを特徴とする基板処理装置。 - 前記カソード電極は、前記載置台が有する静電チャック及びフォーカスリングの表面であり、前記アノード電極は、前記電極、前記誘電体、前記処理室の側壁、前記載置台の側壁及び排気プレートの表面であることを特徴とする請求項1記載の誘電体の厚さ設定方法。
- 前記カソード電極は、前記載置台が有する静電チャック及びフォーカスリングの表面であり、前記アノード電極は、前記電極、前記誘電体、前記処理室の側壁、前記載置台の側壁及び排気プレートの表面であることを特徴とする請求項5記載の基板処理装置。
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