JP5591966B2 - 酸化物超電導体用組成物、及び酸化物超電導線材の製造方法 - Google Patents
酸化物超電導体用組成物、及び酸化物超電導線材の製造方法 Download PDFInfo
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- JP5591966B2 JP5591966B2 JP2013039810A JP2013039810A JP5591966B2 JP 5591966 B2 JP5591966 B2 JP 5591966B2 JP 2013039810 A JP2013039810 A JP 2013039810A JP 2013039810 A JP2013039810 A JP 2013039810A JP 5591966 B2 JP5591966 B2 JP 5591966B2
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- Prior art keywords
- oxide
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- heat treatment
- acid
- oxide superconductor
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- 239000002887 superconductor Substances 0.000 title claims description 77
- 239000000203 mixture Substances 0.000 title claims description 37
- 238000004519 manufacturing process Methods 0.000 title claims description 17
- 238000010438 heat treatment Methods 0.000 claims description 44
- 238000000034 method Methods 0.000 claims description 42
- 239000000758 substrate Substances 0.000 claims description 40
- 125000004432 carbon atom Chemical group C* 0.000 claims description 22
- 239000002904 solvent Substances 0.000 claims description 20
- 239000002243 precursor Substances 0.000 claims description 18
- 239000003960 organic solvent Substances 0.000 claims description 15
- 150000003839 salts Chemical class 0.000 claims description 15
- 239000010949 copper Substances 0.000 claims description 14
- 150000001879 copper Chemical class 0.000 claims description 13
- -1 alicyclic carboxylic acids Chemical class 0.000 claims description 12
- 238000001354 calcination Methods 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 11
- 239000002184 metal Substances 0.000 claims description 10
- 229910052751 metal Inorganic materials 0.000 claims description 10
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- 229910052693 Europium Inorganic materials 0.000 claims description 9
- 229910052688 Gadolinium Inorganic materials 0.000 claims description 9
- 229910052689 Holmium Inorganic materials 0.000 claims description 9
- 229910052779 Neodymium Inorganic materials 0.000 claims description 9
- 229910052772 Samarium Inorganic materials 0.000 claims description 9
- 230000008569 process Effects 0.000 claims description 9
- 229910052727 yttrium Inorganic materials 0.000 claims description 9
- 229910052691 Erbium Inorganic materials 0.000 claims description 8
- 229910052777 Praseodymium Inorganic materials 0.000 claims description 8
- 229910052769 Ytterbium Inorganic materials 0.000 claims description 8
- 125000000468 ketone group Chemical group 0.000 claims description 7
- 125000003277 amino group Chemical group 0.000 claims description 6
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 claims description 5
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- 229920006395 saturated elastomer Polymers 0.000 claims description 5
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- 125000001153 fluoro group Chemical group F* 0.000 claims description 3
- BQJILRFOGPBJQJ-UHFFFAOYSA-L barium(2+);2,2,2-trifluoroacetate Chemical compound [Ba+2].[O-]C(=O)C(F)(F)F.[O-]C(=O)C(F)(F)F BQJILRFOGPBJQJ-UHFFFAOYSA-L 0.000 claims description 2
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- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- SJWFXCIHNDVPSH-UHFFFAOYSA-N octan-2-ol Chemical group CCCCCCC(C)O SJWFXCIHNDVPSH-UHFFFAOYSA-N 0.000 description 4
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- 239000001301 oxygen Substances 0.000 description 4
- 229910052760 oxygen Inorganic materials 0.000 description 4
- JYVLIDXNZAXMDK-UHFFFAOYSA-N pentan-2-ol Chemical compound CCCC(C)O JYVLIDXNZAXMDK-UHFFFAOYSA-N 0.000 description 4
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- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 4
- 238000004544 sputter deposition Methods 0.000 description 4
- OBETXYAYXDNJHR-SSDOTTSWSA-M (2r)-2-ethylhexanoate Chemical compound CCCC[C@@H](CC)C([O-])=O OBETXYAYXDNJHR-SSDOTTSWSA-M 0.000 description 3
- AVQQQNCBBIEMEU-UHFFFAOYSA-N 1,1,3,3-tetramethylurea Chemical compound CN(C)C(=O)N(C)C AVQQQNCBBIEMEU-UHFFFAOYSA-N 0.000 description 3
- HNNQYHFROJDYHQ-UHFFFAOYSA-N 3-(4-ethylcyclohexyl)propanoic acid 3-(3-ethylcyclopentyl)propanoic acid Chemical compound CCC1CCC(CCC(O)=O)C1.CCC1CCC(CCC(O)=O)CC1 HNNQYHFROJDYHQ-UHFFFAOYSA-N 0.000 description 3
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- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
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- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 3
- 239000005456 alcohol based solvent Substances 0.000 description 3
- OBETXYAYXDNJHR-UHFFFAOYSA-N alpha-ethylcaproic acid Natural products CCCCC(CC)C(O)=O OBETXYAYXDNJHR-UHFFFAOYSA-N 0.000 description 3
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- 238000002425 crystallisation Methods 0.000 description 3
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- 238000010304 firing Methods 0.000 description 3
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- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 2
- OYHQOLUKZRVURQ-NTGFUMLPSA-N (9Z,12Z)-9,10,12,13-tetratritiooctadeca-9,12-dienoic acid Chemical compound C(CCCCCCC\C(=C(/C\C(=C(/CCCCC)\[3H])\[3H])\[3H])\[3H])(=O)O OYHQOLUKZRVURQ-NTGFUMLPSA-N 0.000 description 2
- QEGNUYASOUJEHD-UHFFFAOYSA-N 1,1-dimethylcyclohexane Chemical compound CC1(C)CCCCC1 QEGNUYASOUJEHD-UHFFFAOYSA-N 0.000 description 2
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- JOLQKTGDSGKSKJ-UHFFFAOYSA-N 1-ethoxypropan-2-ol Chemical compound CCOCC(C)O JOLQKTGDSGKSKJ-UHFFFAOYSA-N 0.000 description 2
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- REHQLKUNRPCYEW-UHFFFAOYSA-N 1-methylcyclohexane-1-carboxylic acid Chemical compound OC(=O)C1(C)CCCCC1 REHQLKUNRPCYEW-UHFFFAOYSA-N 0.000 description 2
- HFZLSTDPRQSZCQ-UHFFFAOYSA-N 1-pyrrolidin-3-ylpyrrolidine Chemical compound C1CCCN1C1CNCC1 HFZLSTDPRQSZCQ-UHFFFAOYSA-N 0.000 description 2
- ULQISTXYYBZJSJ-UHFFFAOYSA-N 12-hydroxyoctadecanoic acid Chemical compound CCCCCCC(O)CCCCCCCCCCC(O)=O ULQISTXYYBZJSJ-UHFFFAOYSA-N 0.000 description 2
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- 229910000990 Ni alloy Inorganic materials 0.000 description 2
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 2
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- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
- 125000001931 aliphatic group Chemical group 0.000 description 2
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- 230000008901 benefit Effects 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 2
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- SEKCXMNFUDONGJ-UHFFFAOYSA-L copper;2-ethylhexanoate Chemical compound [Cu+2].CCCCC(CC)C([O-])=O.CCCCC(CC)C([O-])=O SEKCXMNFUDONGJ-UHFFFAOYSA-L 0.000 description 2
- KLKMXKACEROVRH-UHFFFAOYSA-L copper;3,5,5-trimethylhexanoate Chemical compound [Cu+2].[O-]C(=O)CC(C)CC(C)(C)C.[O-]C(=O)CC(C)CC(C)(C)C KLKMXKACEROVRH-UHFFFAOYSA-L 0.000 description 2
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- 238000004090 dissolution Methods 0.000 description 2
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- 239000003759 ester based solvent Substances 0.000 description 2
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- 239000011737 fluorine Substances 0.000 description 2
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- HFPZCAJZSCWRBC-UHFFFAOYSA-N p-cymene Chemical compound CC(C)C1=CC=C(C)C=C1 HFPZCAJZSCWRBC-UHFFFAOYSA-N 0.000 description 1
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- DKOUNIUITOMUNM-UHFFFAOYSA-K propanoate;yttrium(3+) Chemical compound [Y+3].CCC([O-])=O.CCC([O-])=O.CCC([O-])=O DKOUNIUITOMUNM-UHFFFAOYSA-K 0.000 description 1
- IHIQOKFJGANDOX-UHFFFAOYSA-N propyl 2-ethylhexanoate Chemical compound CCCCC(CC)C(=O)OCCC IHIQOKFJGANDOX-UHFFFAOYSA-N 0.000 description 1
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- GQKZRWSUJHVIPE-UHFFFAOYSA-N sec-amyl acetate Natural products CCCC(C)OC(C)=O GQKZRWSUJHVIPE-UHFFFAOYSA-N 0.000 description 1
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- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
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- UWHZIFQPPBDJPM-BQYQJAHWSA-N trans-vaccenic acid Chemical compound CCCCCC\C=C\CCCCCCCCCC(O)=O UWHZIFQPPBDJPM-BQYQJAHWSA-N 0.000 description 1
- UBOXGVDOUJQMTN-UHFFFAOYSA-N trichloroethylene Natural products ClCC(Cl)Cl UBOXGVDOUJQMTN-UHFFFAOYSA-N 0.000 description 1
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- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B12/00—Superconductive or hyperconductive conductors, cables, or transmission lines
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G3/00—Compounds of copper
- C01G3/006—Compounds containing, besides copper, two or more other elements, with the exception of oxygen or hydrogen
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
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- H01B12/06—Films or wires on bases or cores
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
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- H10N60/00—Superconducting devices
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- H10N60/0268—Manufacture or treatment of devices comprising copper oxide
- H10N60/0296—Processes for depositing or forming copper oxide superconductor layers
- H10N60/0548—Processes for depositing or forming copper oxide superconductor layers by deposition and subsequent treatment, e.g. oxidation of pre-deposited material
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- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
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- H10N60/00—Superconducting devices
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- H10N60/855—Ceramic superconductors
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
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Description
ジオール系溶剤としては、エチレングリコール、プロピレングリコール、1,2−ブタンジオール、1,3−ブタンジオール、1,4−ブタンジオール、1,5−ペンタンジオール、ネオペンチルグリコール、イソプレングリコール(3−メチル−1,3−ブタンジオール)、1,2−ヘキサンジオール、1,6−ヘキサンジオール、3−メチル−1,5−ペンタンジオール、1,2−オクタンジオール、オクタンジオール(2−エチル−1,3−ヘキサンジオール)、2−ブチル−2−エチル−1,3−プロパンジオール、2,5−ジメチル−2,5−ヘキサンジオール、1,2−シクロヘキサンジオール、1,4−シクロヘキサンジオール、1,4−シクロヘキサンジメタノール等が挙げられる。
ケトン系溶剤としては、アセトン、エチルメチルケトン、メチルイソプロピルケトン、メチルブチルケトン、メチルイソブチルケトン、メチルアミルケトン、メチルヘキシルケトン、エチルブチルケトン、ジエチルケトン、ジプロピルケトン、ジイソブチルケトン、メチルアミルケトン、シクロヘキサノン、メチルシクロヘキサノン等が挙げられる。
エステル系溶剤としては、ギ酸メチル、ギ酸エチル、酢酸メチル、酢酸エチル、酢酸イソプロピル、酢酸ブチル、酢酸イソブチル、酢酸第2ブチル、酢酸第3ブチル、酢酸アミル、酢酸イソアミル、酢酸第3アミル、酢酸フェニル、プロピオン酸メチル、プロピオン酸エチル、プロピオン酸イソプロピル、プロピオン酸ブチル、プロピオン酸イソブチル、プロピオン酸第2ブチル、プロピオン酸第3ブチル、プロピオン酸アミル、プロピオン酸イソアミル、プロピオン酸第3アミル、プロピオン酸フェニル、2−エチルヘキサン酸メチル、2−エチルヘキサン酸エチル、2−エチルヘキサン酸プロピル、2−エチルヘキサン酸イソプロピル、2−エチルヘキサン酸ブチル、乳酸メチル、乳酸エチル、メトキシプロピオン酸メチル、エトキシプロピオン酸メチル、メトキシプロピオン酸エチル、エトキシプロピオン酸エチル、エチレングリコールモノメチルエーテルアセテート、ジエチレングリコールモノメチルエーテルアセテート、エチレングリコールモノエチルエーテルアセテート、エチレングリコールモノプロピルエーテルアセテート、エチレングリコールモノイソプロピルエーテルアセテート、エチレングリコールモノブチルエーテルアセテート、エチレングリコールモノ第2ブチルエーテルアセテート、エチレングリコールモノイソブチルエーテルアセテート、エチレングリコールモノ第3ブチルエーテルアセテート、プロピレングリコールモノメチルエーテルアセテート、プロピレングリコールモノエチルエーテルアセテート、プロピレングリコールモノプロピルエーテルアセテート、プロピレングリコールモノイソプロピルエーテルアセテート、プロピレングリコールモノブチルエーテルアセテート、プロピレングリコールモノ第2ブチルエーテルアセテート、プロピレングリコールモノイソブチルエーテルアセテート、プロピレングリコールモノ第3ブチルエーテルアセテート、ブチレングリコールモノメチルエーテルアセテート、ブチレングリコールモノエチルエーテルアセテート、ブチレングリコールモノプロピルエーテルアセテート、ブチレングリコールモノイソプロピルエーテルアセテート、ブチレングリコールモノブチルエーテルアセテート、ブチレングリコールモノ第2ブチルエーテルアセテート、ブチレングリコールモノイソブチルエーテルアセテート、ブチレングリコールモノ第3ブチルエーテルアセテート、アセト酢酸メチル、アセト酢酸エチル、オキソブタン酸メチル、オキソブタン酸エチル、γ−ラクトン、マロン酸ジメチル、コハク酸ジメチル、プロピレングリコールジアセテート、δ−ラクトン等が挙げられる。
エーテル系溶剤としては、テトラヒドロフラン、テトラヒドロピラン、モルホリン、エチレングリコールジメチルエーテル、ジエチレングリコールジメチルエーテル、ジプロピレングリコールジメチルエーテル、トリエチレングリコールジメチルエーテル、ジブチルエーテル、ジエチルエーテル、ジオキサン等が挙げられる。
脂肪族又は脂環族炭化水素系溶剤としては、ペンタン、ヘキサン、シクロヘキサン、メチルシクロヘキサン、ジメチルシクロヘキサン、エチルシクロヘキサン、ヘプタン、オクタン、デカリン、ソルベントナフサ、テレピン油、D−リモネン、ピネン、ミネラルスピリット、スワゾール#310(コスモ松山石油(株)、ソルベッソ#100(エクソン化学(株))等が挙げられる。
芳香族炭化水素系溶剤としては、ベンゼン、トルエン、エチルベンゼン、キシレン、メシチレン、ジエチルベンゼン、クメン、イソブチルベンゼン、シメン、テトラリン等が挙げられる。
シアノ基を有する炭化水素溶剤としては、アセトニトリル、1−シアノプロパン、1−シアノブタン、1−シアノヘキサン、シアノシクロヘキサン、シアノベンゼン、1,3−ジシアノプロパン、1,4−ジシアノブタン、1,6−ジシアノヘキサン、1,4−ジシアノシクロヘキサン、1,4−ジシアノベンゼン等が挙げられる。
ハロゲン化芳香族炭化水素系溶媒としては、四塩化炭素、クロロホルム、トリクロロエチレン、塩化メチレン等が挙げられる。
その他の有機溶剤としては、N−メチル−2−ピロリドン、ジメチルスルホキシド、ジメチルホルムアミド、アニリン、トリエチルアミン、ピリジン等が挙げられる。
上記の有機溶剤としては、沸点が80℃以上であるものが均一な塗布性を与えるので好ましい。また、アルコール系溶剤は、様々な基材に対する濡れ性が良好なので好ましい。特に1−ブタノール、イソブタノール、2−ブタノール、第3ブタノール、ペンタノール、イソペンタノール、2−ペンタノール、ネオペンタノール、第3ペンタノール、ヘキサノール、2−ヘキサノール、ヘプタノール、2−ヘプタノール、オクタノール、2―エチルヘキサノール、2−オクタノール、エチレングリコールモノエチルエーテル、プロピレングリコールモノメチルエーテル、プロピレングルコールモノエチルエーテル、ジエチレングルコールモノメチルエーテル等の炭素数4〜8のアルコール系溶剤が好適である。
図1は、MOD法によるREBaCuO(REは、Y、Nd、Sm、Gd、Dy、Eu、Er、Yb、Pr及びHoからなる群から選択された少なくとも1種以上の元素)系超電導層を備えるテープ状酸化物超電導線材(以下、「YBCO超電導線材」ともいう)の製造方法の概略を示したものである。
これに対し、プロピオン液でディップコートする本実施の形態では、アミノ基を有する可溶化剤を含有するため、蒸発しにくい(飛びにくい)。このため、プロピオン液を塗布して引き上げた基材上の塗布膜は、軸方向で見て両端部及び中央部共に均一な膜体として塗布された状態で乾燥する。
実施例1では、本実施の形態の酸化物超電導体用組成物を用いて、テープ状の基材上に、REBaCu系の酸化物超電導体(YBCO超電導体)を図1に示すMOD法により形成した。この実施例1の基材は、基板としてのハステロイ(登録商標)と、このハステロイ(登録商標)上に、順に、GZO、MgO、LMO、CeO2を積層することで形成された中間層とを備える。ディップコート法で用いられる混合溶液30(図1参照)は、フッ素原子を含まないY−プロピオン酸、Ba−TFA、Cu−2−エチルヘキサン酸と、これらY−プロピオン酸、Ba−TFA、Cu−2−エチルヘキサン酸の成分を溶かす有機溶剤とを含有する。加えて有機溶剤には、プロピオン酸を溶かすアミノ基を有する可溶化剤(ここでは、テトラメチル尿素)が含まれる。ディップコート法では、超電導体の臨界1回塗布膜厚は、1.2[μm/coat](塗布速度5[m/h])であり、1回の塗布膜厚は、0.49[μm/coat]であった。これを所望の膜厚(ここでは、2.5[μm]を超える膜厚)になるまで複数回繰り返した。
MOD法で実施例1と同様にYBCO超電導体を形成する際に、実施例1と比較して、塗布工程において、塗布速度を2倍の10[m/h]として、基材に混合溶液30(図1参照)をディップコートして、YBCO超電導体を形成した。実施例2では、一回の塗布膜厚は、0.77[μm/coat]であった。これを所望の膜厚(ここでは、2.0[μm]を超える膜厚)になるまで複数回繰り返した。
実施例1で用いた混合溶液の有機溶液において、アミノ基を有する可溶化剤を含まない構成の混合溶液を、ディップコート法で、実施例1の基材と同じ基材に塗布し、塗布してなる塗布膜に対して、仮焼成熱処理、本焼成熱処理を施して、酸化物超電導線材を形成した。塗布速度は、5[m/h]とし、その他、塗布、仮焼成熱処理及び本焼成熱処理における条件は、実施例と同じ条件で行った。
参考例として、TFA−MOD原料溶液としてY−TFA、Ba−TFA、Cu−2−エチルヘキサン酸を含有する混合溶液を用いて、実施例1と同様に、テープ状の基材に、MOD法でYBCO超電導体を形成した。塗布速度5[m/h])であり、一回の塗布膜厚は、0.11(約0.1)[μm/coat]であり、塗布工程及び仮焼成工程を繰り返して所望の膜厚(ここでは20回繰り返して、膜厚2[μm]とした)にした。その他、塗布、仮焼成熱処理及び本焼成熱処理における条件は、実施例と同じ条件で行った。
49、50 線材
60 YBCO超電導線材
Claims (6)
- REBaCuO(REは、Y、Nd、Sm、Gd、Dy、Eu、Er、Yb、Pr及びHoからなる群から選択された少なくとも1種以上の元素)系酸化物超電導体を形成するための組成物であって、
RE成分としてケトン基を含まない炭素原子数3〜8のカルボン酸のRE塩と、
Ba成分としてトリフルオロ酢酸バリウムと、
Cu成分として炭素原子数6〜16の分岐飽和脂肪族カルボン酸の銅塩及び炭素原子数6〜16の脂環族カルボン酸の銅塩からなる群から選ばれる1種類以上の銅塩と、
これらの金属塩成分を溶解させる有機溶剤と、
を必須成分として含有する、
酸化物超電導体用組成物。 - 前記RE成分がイットリウム塩からなる、
請求項1記載の酸化物超電導体用組成物。 - 前記RE成分がフッ素原子を含まないプロピオン酸塩からなる、
請求項1又は2に記載の酸化物超電導体用組成物。 - 前記有機溶剤は、アミノ基を有する可溶化剤を含む、
請求項1〜3のいずれかに記載の酸化物超電導体用組成物。 - 請求項1から4のいずれか1項に記載の酸化物超電導体用組成物の溶液が収容された容器から、テープ状の基材を引き上げることにより、前記基材の表面に前記溶液を塗布する塗布工程と、
塗布した前記溶液に仮焼焼成処理を施して、前記基材の表面に酸化物超電導体の前駆体を形成する仮焼成熱処理工程と、
前記前駆体に本焼成熱処理を行って結晶化させることで、前記基材の表面に、REBaCuO(REは、Y、Nd、Sm、Gd、Dy、Eu、Er、Yb、Pr及びHoからなる群から選択された少なくとも1種以上の元素)系の酸化物超電導体を形成する本焼成熱処理工程と、
を有する酸化物超電導線材の製造方法。 - 前記塗布工程と前記仮焼成熱処理工程とを1回以上10回以下繰り返して、前記前駆体を形成する、
請求項5に記載の酸化物超電導線材の製造方法。
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