JP4808038B2 - Hairdressing fee - Google Patents
Hairdressing fee Download PDFInfo
- Publication number
- JP4808038B2 JP4808038B2 JP2006040979A JP2006040979A JP4808038B2 JP 4808038 B2 JP4808038 B2 JP 4808038B2 JP 2006040979 A JP2006040979 A JP 2006040979A JP 2006040979 A JP2006040979 A JP 2006040979A JP 4808038 B2 JP4808038 B2 JP 4808038B2
- Authority
- JP
- Japan
- Prior art keywords
- hair
- oil
- mass
- hair styling
- polyoxyethylene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
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- -1 polyoxyethylene Polymers 0.000 claims description 43
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- IUJAMGNYPWYUPM-UHFFFAOYSA-N hentriacontane Chemical group CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCC IUJAMGNYPWYUPM-UHFFFAOYSA-N 0.000 claims description 7
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- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 description 1
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Description
本発明は、頭髪につや(艶)を与えると共に望みの髪型に整えるために使用する整髪料に関するものであり、特にべたつき感が少なく自然な仕上がり感が得られると共に、整髪力(セット力)および再整髪性(再セット性)にも優れた整髪料に関するものである。 The present invention relates to a hair styling agent that is used to give gloss (gloss) to the hair and to prepare a desired hairstyle, and in particular, provides a natural finish feeling with little stickiness, The present invention relates to a hair styling material having excellent hair styling properties (resetting properties).
頭髪につや(艶)を与えると共に望みの髪型に整えるために使用する整髪料としては、これまで様々な形態のものが使用されている。こうした整髪料の一つとして、ポマードが古くから知られている。ポマードは、植物性の油脂成分を用いたものと鉱物性の油脂成分を用いたものに大別され、これらの成分の違いによって毛髪の整髪力(セット力)も異なり、毛髪の特性の違いによって使い分けられている。例えば、植物性の油脂成分を主に用いたものでは、粘着性と進展性に優れたものとなり、太くて硬い毛髪に主に用いられている。また、鉱物性の油脂成分を主に用いたものでは、粘着性が弱くなるので、細くて柔らかい毛髪に主に用いられている。 Various hair styling materials have been used so far to give the hair a gloss (gloss) and to make a desired hairstyle. Pomade has long been known as one of these hair-styling products. Pomade is roughly divided into those using vegetable oil components and those using mineral oil components, and the hair styling power (setting power) of the hair differs depending on the difference of these components, and the difference in the characteristics of the hair It is used properly. For example, those mainly using vegetable oil and fat components have excellent adhesiveness and progress, and are mainly used for thick and hard hair. In addition, those mainly using mineral oil and fat components are mainly used for thin and soft hair because the tackiness is weakened.
上記植物性の油脂成分としては、ヒマシ油、モクロウ、硬化油、オリーブ油、ツバキ油等が使用され、鉱物性の油脂成分としては、ワセリン、流動パラフィン、パラフィン、マイクロクリスタリンワックス、硬化油等が使用される(例えば、非特許文献1)。 Castor oil, mole, hardened oil, olive oil, camellia oil, etc. are used as the vegetable oil component, and petrolatum, liquid paraffin, paraffin, microcrystalline wax, hardened oil, etc. are used as the mineral oil component. (For example, Non-Patent Document 1).
上記のような油脂成分は、毛髪のセット力を良好にするだけでなく、毛髪につや感を付与する上でも有用な成分であるが、つや感を高めるために、多量に油脂成分を配合すると毛髪塗布時にベタつきが生じ、使用後の洗髪性が著しく悪くなることがある。こうした問題を解決するために、例えば特許文献1には、界面活性剤を含有させることも提案されている。 The oil and fat component as described above is a component that is useful not only for improving the setting power of the hair but also for imparting a glossy feeling to the hair. When the hair is applied, stickiness occurs, and the shampooability after use may be remarkably deteriorated. In order to solve such a problem, for example, Patent Document 1 proposes to contain a surfactant.
ところで、上記のような油脂成分を使用することの利点としては、ヘアスタイルが乱れてしまった場合でも、再整髪することが容易であること(再セット性)も挙げられる。しかしながら、再セット性を良好にするため多量の油脂成分を配合すると、毛髪塗布時にベタつきが著しくなる。 By the way, as an advantage of using the oil and fat component as described above, it is easy to re-hair even if the hairstyle is disturbed (resetability). However, when a large amount of oil and fat components are blended in order to improve the resetting property, the stickiness becomes remarkable when the hair is applied.
最近では、ベタつき感を抑えた自然な仕上がり感が求められており、油脂成分はできるだけ減少させる傾向にある。こうした油脂成分の減少が、毛髪のセット力および再セット性を低下させることになる。油脂成分の減少による毛髪のセット力や再セット性の低下を抑制するために、高分子樹脂を配合した整髪料も提案されている(上記特許文献1)。 Recently, there has been a demand for a natural finish feeling that suppresses the sticky feeling, and the oil and fat components tend to be reduced as much as possible. Such a reduction in the fat and oil components reduces the setting power and resetting ability of the hair. A hair styling compounded with a polymer resin has also been proposed in order to suppress a reduction in hair setting force and resetting property due to a decrease in oil and fat components (Patent Document 1).
高分子樹脂を配合することによって、毛髪のセット力は向上することになるが、その配合量が多くなると、毛髪にパサつきやバリ感が生じるという問題がある。また、高分子樹脂を配合することによって毛髪のセット力は非常に高いものとなるが、髪型が乱れてしまった場合の再セット性は却って低下することになる。 By blending the polymer resin, the setting power of the hair is improved. However, when the blending amount is increased, there is a problem that the hair feels dry and has a burr feeling. Moreover, although the setting power of hair becomes very high by mix | blending polymer resin, the resetting property when a hairstyle is disturb | confused will fall on the contrary.
そこで、前述のような油脂成分と高分子樹脂を併用することによって、セット力や再セット性を高めることは一般に行なわれているのであるが、油脂成分の配合量を増加させて再セット性を高めることはベタつき感が増し、また高分子樹脂の配合量を増してセット力を高めるとバリ感が高くなる傾向がある。こうしたことから、油脂成分と高分子樹脂を併用するだけでは、セット力および再セット性とバリ感を適度に調整することは困難であった。 Therefore, it is generally practiced to increase the setting power and resetability by using the oil and fat component and the polymer resin as described above. Increasing the feeling increases the stickiness, and increasing the amount of the polymer resin to increase the setting force tends to increase the burr feeling. For these reasons, it has been difficult to appropriately adjust the setting power, the resetting property and the burr feeling only by using the oil and fat component and the polymer resin in combination.
また自然な仕上がり感と再セット性に加え、毛髪を奇麗に見せるためのつや感(艶感)も従来から求められている。特に、最近では毛髪にカラー処理やパーマ処理をすることが一般的であり、これらの処理によってダメージを受けてつや感が低下していることが多く、より高いつや感を付与することが望まれているのが実情である。 In addition to a natural finish and resetting ability, there has also been a demand for a glossy feeling (luster) for making hair look beautiful. In particular, recently, it is common to color and perm the hair, and these treatments are often damaged to reduce the gloss, and it is desired to impart a higher gloss. The fact is.
こうしたつや感を毛髪に付与する方法として、例えば特許文献2〜4には、整髪料に油性成分として各種シリコーン類を配合することも提案されている。このようなシリコーン類を配合した整髪料を用いると、毛髪につや感を与えると同時に毛髪表面の滑り性も高くなる。しかしながら、良好なつや感が付与されても、滑り性が同時に高いものとなるので、良好なつや感を付与できるだけの多量の配合量(3質量%以上)では、セット性が却って低下してしまうという問題がある。
本発明はこうした状況の下でなされたものであり、その目的は、ベタつき感を与えることなく、一定のセット力を維持しつつ再セット性も良好であり、しかも良好なつや感を与えることのできる整髪料を提供することにある。 The present invention has been made under such circumstances, and its purpose is not to give a sticky feeling, to maintain a constant setting force, to have a good resetting property, and to give a good gloss feeling. It is to provide a hairdressing material that can be used.
上記目的を達成することができた本発明の整髪料とは、少なくとも、(a)ポリオキシエチレンを含有する水溶性非イオン界面活性剤:25〜50.0質量%(整髪料全体に対する割合、以下同じ)、(b)1,2−ヘキサンジオールおよび1,2−オクタンジオールよりなる群から選ばれる1種以上:0.1〜10.0質量%、および(c)常温で固形のワックス類:0.1〜15.0質量%、を配合したものである点に要旨を有するものである。 The hair styling composition of the present invention that has achieved the above object is at least (a) a water-soluble nonionic surfactant containing polyoxyethylene: 25 to 50.0% by mass (ratio to the total hair styling composition, The same shall apply hereinafter), (b) one or more selected from the group consisting of 1,2-hexanediol and 1,2-octanediol: 0.1 to 10.0% by mass, and (c) waxes that are solid at room temperature : 0.1 to 15.0% by mass.
本発明で用いる「ポリオキシエチレンを含有する水溶性非イオン界面活性剤」としては、ポリオキシエチレン硬化ヒマシ油が最も好ましいものとして挙げられる。 As the “water-soluble nonionic surfactant containing polyoxyethylene” used in the present invention, polyoxyethylene hydrogenated castor oil is most preferable.
また、「常温で固形のワックス類」としては、キャンデリラロウが最も好ましいものとして挙げられる。
As the “solid waxes at normal temperature”, candelilla wax is most preferable.
本発明では、少なくとも、(a)ポリオキシエチレンを含有する水溶性非イオン界面活性剤、(b)アルカンジオール類、および(c)常温で固形のワックス類を含有することによって、ベタつき感を与えることなく、一定のセット力を維持しつつ再セット性も良好であり、しかも良好なつや感を与えることのできる整髪料が実現できた。 In the present invention, at least (a) a water-soluble nonionic surfactant containing polyoxyethylene, (b) alkanediols, and (c) waxes that are solid at normal temperature give a sticky feeling. Thus, a hair styling material that can maintain a certain setting force, has good re-setting property, and can give a good gloss feeling can be realized.
上述の如く、油脂成分を多くすればベタツキ感が生じることが知られており、そのために油脂成分を極力低下させて高分子樹脂を配合すれば、毛髪にパサつき感やバリ感が生じることになる。こうしたことから、本発明者は、パサつき感やバリ感が生じ易い高分子樹脂を用いることなく、毛髪のセット力を向上させ得る物質について様々な角度から検討した。その結果、ポリオキシエチレンを含有する水溶性非イオン界面活性剤と、常温(25℃)で固形のワックスとを併用すれば、油脂成分を極力低減させた場合であっても良好なセット性が実現できることを見出した。特に、常温で固形のワックスは、セット力を向上させると共に、毛髪に適度のつや感をも付与する作用を発揮するものである。 As mentioned above, it is known that if the oil and fat components are increased, a sticky feeling is generated. Therefore, if the oil and fat components are reduced as much as possible and a polymer resin is blended, the hair feels dry and burrs. Become. For these reasons, the present inventor has examined a substance that can improve the hair setting force from various angles without using a polymer resin that is prone to a feeling of softness or burr. As a result, if a water-soluble nonionic surfactant containing polyoxyethylene and a solid wax at room temperature (25 ° C.) are used in combination, good setting properties can be obtained even when the oil and fat components are reduced as much as possible. I found out that it could be realized. In particular, a wax that is solid at room temperature exhibits an effect of improving the setting power and imparting an appropriate gloss to the hair.
一方、セット力および再セット性を良好に維持させつつ、つや感をも向上させる物質についても様々検討したところ、アルカンジオール類がこうした作用を発揮させ得ることが判明したのである。そして、これらの物質を適切に組み合わせて配合することによって、上記目的が達成できる整髪料が実現できることを見出し、本発明を完成した。 On the other hand, as a result of various investigations on substances that improve glossiness while maintaining good setting power and resetting ability, it has been found that alkanediols can exert such effects. And it discovered that the hair dressing which can achieve the said objective was realizable by mix | blending combining these substances appropriately, and completed this invention.
本発明の整髪料では、(a)ポリオキシエチレンを含有する水溶性非イオン界面活性剤、(b)アルカンジオール類、および(c)常温で固形のワックス類を配合したものである。このうちポリオキシエチレンを含有する水溶性非イオン界面活性剤[以下、(a)成分と呼ぶことがある]は、適度な粘性を保つために必要な物質である。また、本発明の整髪料を使用した後の洗髪性を向上させるという観点から、この(a)成分中にポリオキシエチレンを含有することが必要な要件となる。 The hair styling composition of the present invention comprises (a) a water-soluble nonionic surfactant containing polyoxyethylene, (b) alkanediols, and (c) waxes that are solid at room temperature. Among these, a water-soluble nonionic surfactant containing polyoxyethylene [hereinafter sometimes referred to as component (a)] is a substance necessary for maintaining an appropriate viscosity. In addition, from the viewpoint of improving the hair washability after using the hairdressing material of the present invention, it is a necessary requirement to contain polyoxyethylene in the component (a).
本発明で用いる(a)成分としては、具体的には、ポリオキシエチレンラウリルエーテル、ポリオキシエチレンセチルエーテル、ポリオキシエチレンステアリルエーテル、ポリオキシエチレンオレイルエーテル、ポリオキシエチレンオクチルフェニルエーテル、ポリオキシエチレンノニルフェニルエーテル、ポリオキシエチレンソルビタンモノラウレート、ポリオキシエチレンソルビタンモノパルミテート、ポリオキシエチレンソルビタンモノステアレート、ポリオキシエチレンソルビタンモノオレエート、ポリオキシエチレンソルビタントリオレエート、テトラオレイン酸ポリオキシエチレンソルビット、ポリエチレングリコールモノラウレート、ポリエチレングリコールモノステアレート、ポリエチレングリコールジステアレート、ポリエチレングリコールモノオレエート、ポリオキシエチレンアルキルアミン、ポリオキシエチレン硬化ヒマシ油等が挙げられる。このうち、少なくともポリオキシエチレン硬化ヒマシ油を用いることが好ましく、このポリオキシエチレン硬化ヒマシ油の単独若しくは他の(a)成分との併用によって、(a)成分による効果が有効に達成される。 Specific examples of the component (a) used in the present invention include polyoxyethylene lauryl ether, polyoxyethylene cetyl ether, polyoxyethylene stearyl ether, polyoxyethylene oleyl ether, polyoxyethylene octyl phenyl ether, and polyoxyethylene. Nonylphenyl ether, polyoxyethylene sorbitan monolaurate, polyoxyethylene sorbitan monopalmitate, polyoxyethylene sorbitan monostearate, polyoxyethylene sorbitan monooleate, polyoxyethylene sorbitan trioleate, polyoxyethylene sorbite tetraoleate , Polyethylene glycol monolaurate, polyethylene glycol monostearate, polyethylene glycol distearate, poly Chi glycol monooleate, polyoxyethylene alkyl amines, polyoxyethylene hardened castor oil, and the like. Of these, at least polyoxyethylene hydrogenated castor oil is preferably used, and the effect of component (a) is effectively achieved by using this polyoxyethylene hydrogenated castor oil alone or in combination with other components (a).
上記(a)成分は、整髪料全体に対する割合で、20.0〜50.0質量%程度で配合することが好ましい。この配合量が20.0質量%未満では、十分なセット力が得られず、50.0質量%を超えると、整髪料の剤質が硬くなって手のひらで伸ばす際に伸び難くなるばかりか、ベタツキが生じる。上記(a)成分のより好ましい下限は30.0質量%程度である。 The component (a) is preferably blended at a ratio of about 20.0 to 50.0% by mass with respect to the total hair styling material. If the blending amount is less than 20.0% by mass, sufficient setting force cannot be obtained. If the blending amount exceeds 50.0% by mass, not only does the composition of the hairdressing agent become hard and it becomes difficult to stretch when stretched with the palm of the hand, Stickiness occurs. The more preferable lower limit of the component (a) is about 30.0% by mass.
本発明で用いるアルカンジオール類[以下、(b)成分と呼ぶことがある]は、セット力および再セット性を良好に維持させつつ、つや感をも向上させるのに有効に作用する。アルカンジオール類は、抗菌剤として使用されることは知られているが(例えば、特開平10−53510号、特開2001−48702号、特開2003−89623号等)、本発明者が検討したところ、こうしたアルカンジオール類を所定量含有させると、セット力および再セット性を良好に維持しつつ、つや感をも向上させるのに有効であることが判明したのである。 The alkanediols used in the present invention (hereinafter sometimes referred to as the component (b)) effectively act to improve the glossiness while maintaining good setting power and resetting property. Although alkanediols are known to be used as antibacterial agents (for example, JP-A-10-53510, JP-A-2001-48702, JP-A-2003-89623, etc.), the present inventors have studied. However, it has been found that the inclusion of a predetermined amount of such alkanediols is effective in improving glossiness while maintaining good setting power and resetting property.
本発明で用いる(b)成分としては、具体的には、エタンジオール、2−アミノ−2−メチル−1,3−プロパンジオール、1,2−プロパンジオール、1,3−プロパンジオール、1,2−ブタンジオール、1,3−ブタンジオール、1,4−ブタンジオール、イソペンタンジオール、1,2−ペンタンジオール、1,3−ペンタンジオール、1,4−ペンタンジオール、1,5−ペンタンジオール、1,2−ヘキサンジオール、1,3−ヘキサンジオール、1,4−ヘキサンジオール、1,5−ヘキサンジオール、1,6−ヘキサンジオール、1,2−ヘプタンジオール、1,7−ヘプタンジオール、1,2−オクタンジオール、1,8−オクタンジオール、1,2−ノナンジオール、1,9−ノナンジオール、1,2−デカンジオール、1,10−デカンジオール、1,2−ウンデカンジオール、1,11−ウンデカンジオール、1,2−ドデカンジオール、1,12−ドデカンジオール、2−メチル−2,4−ペンタンジオール、2,2,4−トリメチル−1,3−ペンタンジオール等が挙げられる。これらのうち、1,2−ペンタンジオール、1,2−ヘキサンジオール、1,2−オクタンジオールよりなる群から選ばれる1種以上を少なくとも配合することが好ましい。 Specific examples of the component (b) used in the present invention include ethanediol, 2-amino-2-methyl-1,3-propanediol, 1,2-propanediol, 1,3-propanediol, 1, 2-butanediol, 1,3-butanediol, 1,4-butanediol, isopentanediol, 1,2-pentanediol, 1,3-pentanediol, 1,4-pentanediol, 1,5-pentanediol, 1,2-hexanediol, 1,3-hexanediol, 1,4-hexanediol, 1,5-hexanediol, 1,6-hexanediol, 1,2-heptanediol, 1,7-heptanediol, 1 , 2-octanediol, 1,8-octanediol, 1,2-nonanediol, 1,9-nonanediol, 1,2-decanediol 1,10-decanediol, 1,2-undecanediol, 1,11-undecanediol, 1,2-dodecanediol, 1,12-dodecanediol, 2-methyl-2,4-pentanediol, 2,2, Examples include 4-trimethyl-1,3-pentanediol. Among these, it is preferable to blend at least one selected from the group consisting of 1,2-pentanediol, 1,2-hexanediol, and 1,2-octanediol.
上記(b)成分による効果を発揮させるためには、整髪料全体に対する割合で0.1〜10.0質量%程度配合することが好ましい。この配合量が0.1質量%未満になると、十分なつや感が得られず、10.0質量%を超えると、セット力が低下することになる。この(b)成分のより好ましい下限は0.3質量%程度であり、より好ましい上限は4.0質量%程度(更に好ましくは2.0質量%)である。 In order to exert the effect of the component (b), it is preferable to blend about 0.1 to 10.0% by mass with respect to the entire hairdressing material. When the amount is less than 0.1% by mass, sufficient gloss cannot be obtained, and when it exceeds 10.0% by mass, the setting force is reduced. The more preferable lower limit of the component (b) is about 0.3% by mass, and the more preferable upper limit is about 4.0% by mass (more preferably 2.0% by mass).
アルカンジオール類を配合することによって上記の効果が得られる理由については、その全てを明らかにした訳ではないが、おそらく次のように考えることができた。アルカンジオール類は、構造上親油基と親水基をバランスよく持つ。即ち、油性成分と同等のつやを向上させる性質を持ち、また親水性のヒドロキシル基をもつことにより、髪にもベタつかず、セット力を低下させることなく毛髪につやを付与できると考えられる。こうした傾向は、アルカンの構造が長いほど顕著に出る。 The reason why the above effects can be obtained by blending alkanediols is not clarified, but could be considered as follows. Alkanediols have a lipophilic group and a hydrophilic group in a balanced structure. In other words, it has the property of improving the gloss equivalent to that of the oil component and has a hydrophilic hydroxyl group, so it is considered that the hair is not sticky and can be given gloss without lowering the setting power. This tendency becomes more prominent as the alkane structure is longer.
本発明で用いる常温で固形のワックス類[以下、(c)成分と呼ぶことがある]は、毛髪につや感とセット力を付与する上で重要な物質である。この(c)成分は、十分なセット力を付与するという観点から常温(25℃)で固形のものとする必要がある。 The waxes that are solid at normal temperature used in the present invention (hereinafter sometimes referred to as the component (c)) are important substances for imparting gloss and setting power to the hair. This component (c) needs to be solid at room temperature (25 ° C.) from the viewpoint of providing a sufficient setting force.
本発明で用いる(c)成分としては、具体的には、ミツロウ、キャンデリラロウ、カルナウバロウ、米ぬかロウ、ラノリン、鯨ロウ、セラック、綿ロウ、モクロウ、水添ホホバ油等のロウ類:セレシン、パラフィンロウ、ポリエチレン、マイクロクリスタリンワックス、ワセリン等の炭化水素油類が挙げられる。このうち、最も好ましいものは、キャンデリラロウである。 Specific examples of the component (c) used in the present invention include beeswax, candelilla wax, carnauba wax, rice bran wax, lanolin, whale wax, shellac, cotton wax, molasses, hydrogenated jojoba oil and other waxes: ceresin, Examples include hydrocarbon oils such as paraffin wax, polyethylene, microcrystalline wax, and petroleum jelly. Of these, the most preferred is candelilla wax.
上記(c)成分による効果を発揮させるためには、整髪料全体に対する割合で0.1〜15.0質量%程度配合することが好ましい。この配合量が0.1質量%未満になると、セット力およびつや感が乏しくなり、15.0質量%を超えると、手のひらで伸ばす際に伸ばし難くなるばかりか、ベタつきが生じる。この(c)成分のより好ましい下限は0.3質量%であり、好ましい上限は10.0質量%(更に好ましくは7.0質量%)である。 In order to exert the effect of the component (c), it is preferable to blend approximately 0.1 to 15.0% by mass with respect to the total hair styling. When the blending amount is less than 0.1% by mass, the setting power and glossiness are poor. When the blending amount exceeds 15.0% by mass, it becomes difficult to stretch with a palm and stickiness occurs. The more preferable lower limit of the component (c) is 0.3% by mass, and the preferable upper limit is 10.0% by mass (more preferably 7.0% by mass).
本発明の整髪料は、少なくとも上記(a)〜(c)成分を配合したものであり、残部は基本的に水(精製水)やエタノール等の溶媒であるが(整髪料全体に対する割合で30〜70質量%程度)、整髪料に通常含まれる添加剤を含むものであっても良い。 The hairdressing composition of the present invention is a mixture of at least the above components (a) to (c), and the remainder is basically a solvent such as water (purified water) or ethanol (30 in proportion to the total hairdressing composition). About 70% by mass), or additives that are usually included in hair styling products.
こうした添加剤としては、例えば保湿剤、常温で液状の油脂類、高級アルコール類、ラノリン類、フッ素化合物、シリコーン類、カチオン化ポリマー類、界面活性剤(陽イオン界面活性剤・陰イオン界面活性剤・ポリオキシエチレンを含まない非イオン界面活性剤・両性界面活性剤)、増粘・ゲル化剤、防腐剤、キレート剤、pH調整剤・酸・アルカリ、紫外線吸収剤、酸化防止剤、溶剤、抗炎症剤、香料、色素等を配合することができる。 Examples of such additives include humectants, oils and fats that are liquid at room temperature, higher alcohols, lanolins, fluorine compounds, silicones, cationized polymers, surfactants (cationic surfactants / anionic surfactants).・ Nonionic surfactants and amphoteric surfactants that do not contain polyoxyethylene), thickeners / gelling agents, preservatives, chelating agents, pH adjusters, acids / alkalis, UV absorbers, antioxidants, solvents, An anti-inflammatory agent, a fragrance | flavor, a pigment | dye, etc. can be mix | blended.
これらの添加剤を例示すると、保湿剤としては、1,3−ブチレングリコ−ル、プロピレングリコール、グリセリン等の多価アルコール類、トリメチルグリシン、コラーゲン、ゼラチン、エラスチン、コラーゲン分解ペプチド、エラスチン分解ペプチド、ケラチン分解ペプチド、シルク蛋白分解ペプチド、大豆蛋白分解ペプチド、小麦蛋白分解ペプチド、カゼイン分解ペプチド等の蛋白質・ペプチド類およびその誘導体、アルギニン、セリン、グリシン、グルタミン酸等のアミノ酸類、アロエ抽出物、ハマメリス水、ヘチマ水、カモミラエキス、カンゾウエキス等の植物抽出成分、ヒアルロン酸ナトリウム、クエン酸塩、コンドロイチン硫酸、乳酸ナトリウム、2−ピロリドン−5−カルボン酸ナトリウム等が挙げられる。 Examples of these additives include moisturizers such as 1,3-butylene glycol, propylene glycol, glycerin and other polyhydric alcohols, trimethylglycine, collagen, gelatin, elastin, collagen degrading peptide, elastin degrading peptide, Proteins and peptides such as keratin peptides, silk proteolytic peptides, soybean proteolytic peptides, wheat proteolytic peptides, casein degrading peptides, and derivatives thereof, amino acids such as arginine, serine, glycine, and glutamic acid, aloe extract, Hamamelis water Plant extract components such as loofah water, chamomile extract, licorice extract, sodium hyaluronate, citrate, chondroitin sulfate, sodium lactate, sodium 2-pyrrolidone-5-carboxylate and the like.
常温で液状の油脂類としては、ヒマシ油、ヤシ油、パーム油、パーム核油、サフラワー油、オリーブ油、アボカド油、ゴマ油、月見草油、小麦胚芽油、マカデミアナッツ油、ヘーゼルナッツ油、ローズヒップ油、メドウフォーム油、ティーツリー油、ハッカ油、トウモロコシ油、ナタネ油、ヒマワリ油、小麦胚芽油、綿実油、大豆油、落花生油、コメヌカ油、液状シア脂、ホホバ油等の植物油脂類、流動パラフィン、スクワラン、水添ポリイソブテン等の炭化水素等が挙げられる。 Liquid oils and fats at room temperature include castor oil, palm oil, palm oil, palm kernel oil, safflower oil, olive oil, avocado oil, sesame oil, evening primrose oil, wheat germ oil, macadamia nut oil, hazelnut oil, rosehip oil, Meadow foam oil, tea tree oil, mint oil, corn oil, rapeseed oil, sunflower oil, wheat germ oil, cottonseed oil, soybean oil, peanut oil, rice bran oil, liquid shea fat, jojoba oil and other vegetable oils, liquid paraffin, And hydrocarbons such as squalane and hydrogenated polyisobutene.
高級アルコールとしては、ラウリルアルコール、セチルアルコール、ステアリルアルコール、ベヘニルアルコール、ミリスチルアルコール、オレイルアルコール、セトステアリルアルコール等の直鎖アルコール、モノステアリルグリセリンエーテル(バチルアルコール)、2−デシルテトラデシノール、ラノリンアルコール、コレステロール、フィトステロール、ヘキシルドデカノール、イソステアリルアルコール、オクチルドデカノール等の分枝鎖アルコール等が挙げられる。 As higher alcohols, linear alcohols such as lauryl alcohol, cetyl alcohol, stearyl alcohol, behenyl alcohol, myristyl alcohol, oleyl alcohol, cetostearyl alcohol, monostearyl glycerol ether (batyl alcohol), 2-decyltetradecinol, lanolin alcohol, Examples thereof include branched chain alcohols such as cholesterol, phytosterol, hexyl decanol, isostearyl alcohol, and octyl dodecanol.
ラノリン類としては、液状ラノリン、還元ラノリン、吸着精製ラノリン等のラノリン類が挙げられる。フッ素系化合物としては、パーフルオロポリエーテル、ポリパーフルオロエトキシメトキシジフルオロヒドロキシエチル、ポリパーフルオロエトキシメトキシジフルオロメチルジステアリルアミド、ポリパーフルオロエトキシメトキシジフルオロエチルポリエチレングリコールリン酸等のフッ素系化合物誘導体が挙げられる。 Examples of lanolins include lanolins such as liquid lanolin, reduced lanolin and adsorption-purified lanolin. Examples of the fluorine compound include fluorine compound derivatives such as perfluoropolyether, polyperfluoroethoxymethoxydifluorohydroxyethyl, polyperfluoroethoxymethoxydifluoromethyl distearyl amide, polyperfluoroethoxymethoxydifluoroethyl polyethylene glycol phosphoric acid, and the like. It is done.
シリコーン類としては、低粘度ジメチルポリシロキサン、高粘度ジメチルポリシロキサン、環状ジメチルシロキサン(デカメチルシクロペンタシロキサン)、メチルフェニルポリシロキサン、ジフェニルポリシロキサン、シリコーン樹脂、シリコーンゴム、アミノ変性ポリシロキサン、カチオン変性ポリシロキサン、ポリエーテル変性ポリシロキサン、フッ素変性ポリシロキサン等が挙げられる。但し、これらのシリコーン類は、その配合量が多くなりすぎるとセット力および再セット性が乏しくなるので、3質量%以下程度とすべきである。 Silicones include low-viscosity dimethylpolysiloxane, high-viscosity dimethylpolysiloxane, cyclic dimethylsiloxane (decamethylcyclopentasiloxane), methylphenylpolysiloxane, diphenylpolysiloxane, silicone resin, silicone rubber, amino-modified polysiloxane, and cation-modified. Examples include polysiloxane, polyether-modified polysiloxane, and fluorine-modified polysiloxane. However, these silicones should have a content of about 3% by mass or less because the setting power and the resetting property are poor when the blending amount is too large.
カチオン化ポリマー類としては、カチオン化セルロース誘導体、カチオン化澱粉、カチオン化グアーガム、ジアリル4級アンモニウムの重合体または共重合体、4級化ポリビニルピロリドン誘導体等が挙げられる。 Examples of the cationized polymers include cationized cellulose derivatives, cationized starches, cationized guar gums, diallyl quaternary ammonium polymers or copolymers, and quaternized polyvinylpyrrolidone derivatives.
陽イオン界面活性剤としては、塩化セチルトリメチルアンモニウム、塩化ステアリルトリメチルアンモニウム、塩化ベヘニルトリメチルアンモニウム、塩化アルキルトリメチルアンモニウム、塩化ジステアリルジメチルアンモニウム、エチル硫酸ラノリン脂肪酸アミノプロピルエチルジメチルアンモニウム等が挙げられる。 Examples of the cationic surfactant include cetyltrimethylammonium chloride, stearyltrimethylammonium chloride, behenyltrimethylammonium chloride, alkyltrimethylammonium chloride, distearyldimethylammonium chloride, ethyl lanolin sulfate fatty acid aminopropylethyldimethylammonium, and the like.
陰イオン界面活性剤としては、脂肪酸塩、アルキル硫酸エステル塩、アルキルベンゼンスルホン酸塩、ポリオキシエチレンアルキル硫酸塩、ポリオキシエチレン脂肪アミン硫酸塩、アシルN−メチルタウリン塩、アルキルエーテルリン酸エステル塩、N−アシルアミノ酸塩等が挙げられる。 As an anionic surfactant, fatty acid salt, alkyl sulfate ester salt, alkylbenzene sulfonate, polyoxyethylene alkyl sulfate, polyoxyethylene fatty amine sulfate, acyl N-methyl taurate, alkyl ether phosphate ester salt, N-acyl amino acid salts and the like can be mentioned.
ポリオキシエチレンを含有しない非イオン界面活性剤としては、多価アルコール脂肪酸部分エステル、ポリグリセリン脂肪酸エステル、アルキルジメチルアミンオキサイド、アルキルポリグリコシド、アルキルグルコシド等が挙げられる。 Examples of the nonionic surfactant that does not contain polyoxyethylene include polyhydric alcohol fatty acid partial esters, polyglycerin fatty acid esters, alkyldimethylamine oxides, alkylpolyglycosides, and alkylglucosides.
両性界面活性剤としては、アルキルジメチルアミノ酢酸ベタイン、アルキルアミドジメチルアミノ酢酸ベタイン、2−アルキル−N−カルボキシ−N−ヒドロキシイミダゾリニウムベタイン等を挙げることができる。 Examples of amphoteric surfactants include alkyldimethylaminoacetic acid betaines, alkylamidodimethylaminoacetic acid betaines, and 2-alkyl-N-carboxy-N-hydroxyimidazolinium betaines.
増粘・ゲル化剤としては、グアーガム、キサンタンガム、カラギーナン、アルギン酸、トラガントガム、デンプン誘導体、カルボキシメチルセルロースナトリウム、カルボキシビニルポリマー、アクリル酸・メタアクリル酸エステル共重合体、アクリル酸・メタアクリル酸アルキル共重合体、ポリビニルアルコール等を挙げることができる。 Thickening and gelling agents include guar gum, xanthan gum, carrageenan, alginic acid, tragacanth gum, starch derivatives, sodium carboxymethylcellulose, carboxyvinyl polymer, acrylic acid / methacrylic acid ester copolymer, acrylic acid / alkyl methacrylate acrylic copolymer Examples include coalescence and polyvinyl alcohol.
防腐剤としては、p−ヒドロキシ安息香酸エステル類、安息香酸塩類、フェノキシエタノール、四級アンモニウム塩類等を挙げることができる。 Examples of the preservative include p-hydroxybenzoates, benzoates, phenoxyethanol, quaternary ammonium salts and the like.
キレート剤としては、エデト酸塩、ホスホン酸類、ポリアミノ酸類等を挙げることができる。 Examples of chelating agents include edetates, phosphonic acids, polyamino acids and the like.
pH調整剤・酸・アルカリとしては、リン酸、リンゴ酸、酒石酸、炭酸、フマル酸、クエン酸、乳酸、グリコール酸、コハク酸、塩酸、硫酸、硝酸若しくはそれらの塩類、水酸化ナトリウム、水酸化カリウム、リン酸水素二ナトリウム、モノエタノールアミン、ジエタノールアミン、トリエタノールアミン、アルギニン、アンモニア水、アミノメチルプロパノール若しくはそれらの塩類等を挙げることができる。 As pH adjusters / acids / alkalis, phosphoric acid, malic acid, tartaric acid, carbonic acid, fumaric acid, citric acid, lactic acid, glycolic acid, succinic acid, hydrochloric acid, sulfuric acid, nitric acid or salts thereof, sodium hydroxide, hydroxide Examples thereof include potassium, disodium hydrogen phosphate, monoethanolamine, diethanolamine, triethanolamine, arginine, aqueous ammonia, aminomethylpropanol, and salts thereof.
紫外線吸収剤としては、オキシベンゾン等のベンゾフェノン誘導体やベンズトリアゾール誘導体等を挙げることができる。 Examples of the ultraviolet absorber include benzophenone derivatives such as oxybenzone and benztriazole derivatives.
酸化防止剤としては、アスコルビン酸およびその塩類、またはアスコルビン酸誘導体、亜硫酸ナトリウム、チオグリコール酸およびその塩類、システイン、トコフェロールおよびその誘導体、ブチルヒドロキシトルエン、ブチルヒドロキシアニソール等が挙げられる。 Examples of the antioxidant include ascorbic acid and its salts, or ascorbic acid derivatives, sodium sulfite, thioglycolic acid and its salts, cysteine, tocopherol and its derivatives, butylhydroxytoluene, butylhydroxyanisole and the like.
溶剤類としては、上記した水やエタノールの他にも、2−プロパノール等の低級アルコール類等を使用することができる。抗炎症剤としては、グリチルリチン酸およびその誘導体、グアイアズレン等を例示することができる。 As the solvents, in addition to the water and ethanol described above, lower alcohols such as 2-propanol can be used. Examples of the anti-inflammatory agent include glycyrrhizic acid and its derivatives, guaiazulene and the like.
本発明の整髪料は、日常的に毛髪をセットするために用いることができ、その剤型は液状、ミスト状、クリーム状、ゲル状、泡状、エアゾール状(フォーム、スプレー他)など種々のタイプが可能で、特に限定されるものではない。 The hair conditioner of the present invention can be used for setting hair on a daily basis, and its dosage form is various such as liquid, mist, cream, gel, foam, aerosol (foam, spray, etc.). The type is possible and is not particularly limited.
次に、実施例によって本発明をより具体的に示すが、下記実施例は本発明を制限するものではなく、前・後記の趣旨を逸脱しない範囲で変更実施することは、全て本発明の技術的範囲に包含される。 Next, the present invention will be described more specifically by way of examples. However, the following examples are not intended to limit the present invention, and all modifications can be made without departing from the spirit of the above and following descriptions. To be included in the scope.
[実施例1]
下記表1に示す配合割合で原料を配合して、各種整髪料を調製した(処方例1〜11)。これらの整髪料を用い、専門のパネラー10名によって、「手のひらでの伸びやすさ」、「手のベタつき感」、「つや感」、「セット力」および「再セット性」について、下記の基準で評価を行い、その評価の割合によってその良否を判定した。その結果を、下記表1に併記する。
[Example 1]
Various hair styling agents were prepared by blending raw materials at the blending ratios shown in Table 1 below (Prescription Examples 1 to 11). Using these hair styling agents, the following criteria were set by 10 professional panelists regarding “easiness of stretching with the palm”, “stickiness of hand”, “gloss”, “setting power” and “resetability”. Evaluation was performed, and the quality was determined by the ratio of the evaluation. The results are also shown in Table 1 below.
[手のひらでの伸びやすさ、手のベタつき感]
各処方例の整髪料0.3gを、手のひらに乗せ、両手を合わせて十分に整髪料を練り、その伸びやすさを下記の基準で評価した。このとき同時に、手のベタつき感も下記の基準で評価した。
(手のひらでの伸びやすさの評価基準)
◎:非常に伸びやすい
○:伸びやすい
△:伸びにくい
×:非常に伸びにくい
(手のベタつき感の評価基準)
◎:ベタつきがない
○:ほとんどベタつかない
△:ややベタつく
×:非常にベタつく
[Ease of stretching in the palm of the hand, stickiness of the hand]
The hair styling material 0.3g of each prescription example was put on the palm, and both hands were put together to knead the hair styling material sufficiently. The ease of elongation was evaluated according to the following criteria. At the same time, the stickiness of the hands was also evaluated according to the following criteria.
(Evaluation criteria for ease of elongation in the palm of your hand)
◎: Very easy to stretch ○: Easily stretched △: Difficult to stretch ×: Very difficult to stretch (Evaluation criteria for stickiness of hands)
◎: No stickiness ○: Almost no stickiness △: Slightly sticky ×: Very sticky
[つや感(艶感)]
各処方例の整髪料1.0gを、30gの人毛束に塗布し、ドライヤーにて乾燥させた後、官能的につや感を下記の基準で評価した。
(つや感の評価基準)
◎:非常につやがある
○:つやがある
△:つやが弱い
×:つやがない
[Glossy (Glossy)]
After applying 1.0 g of the hair styling agent of each formulation example to a 30-g human hair bundle and drying it with a dryer, the glossiness was sensorily evaluated according to the following criteria.
(Evaluation criteria for glossiness)
◎: Very glossy ○: Shiny △: Shiny weak ×: No gloss
[セット力]
各処方例の整髪料1.0gを、30gの人毛束に塗布し、毛髪の毛束間に指を入れて毛先まで通した際の、毛髪間の接着力をセット力として下記の基準で評価した。
(セット力の評価基準)
◎:非常にセット力がある
○:セット力がある
△:セット力が弱い
×:セット力がない
[Set power]
Applying 1.0g of the hair styling agent of each prescription example to a 30g human hair bundle, putting the finger between the hair bundles and passing it through the hair tip, the adhesive strength between the hairs as a set force, based on the following criteria evaluated.
(Evaluation criteria for set power)
◎: Very good set power ○: High set power △: Low set power ×: No set power
[再セット性]
各処方例の整髪料1.0gを、30gの人毛束に塗布し、毛髪の毛束間に指を入れて毛先まで通した後、人毛束を3回振り10分間放置し、その後再び毛髪の毛束間に指を入れて毛先まで通し、毛髪間の接着力を再セット性として下記の基準で評価した。
(再セット性の評価基準)
◎:非常に良い
○:良い
△:普通
×:非常に悪い
[Resetability]
After applying 1.0 g of the hair styling agent of each prescription example to a 30 g human hair bundle, putting a finger between the hair bundles and passing it through the hair tips, the human hair bundle is shaken 3 times and left for 10 minutes, and then again. A finger was inserted between the hair bundles and passed through the ends of the hair, and the adhesive strength between the hairs was evaluated according to the following criteria as a resetting property.
(Evaluation criteria for resetability)
◎: Very good ○: Good △: Normal ×: Very bad
表1の結果は、キャンデリラロウの配合量を変化させて、「手のひらでの伸びやすさ」、「手のベタつき感」、「つや感」、「セット力」および「再セット性」の変化を調査したものであるが、特に0.1〜7質量%配合したものでは(処方例4〜8)、良好な特性を発揮していることがわかる。また、キャンデリラロウを3質量%含有させたものでは最も良好な結果が得られていた。 The results in Table 1 indicate that the amount of candelilla wax is changed, and changes in "easiness of stretching with palms", "stickiness of hands", "glossiness", "setting power" and "resetability" However, it can be seen that particularly 0.1 to 7% by mass (Prescription Examples 4 to 8) exhibits good characteristics. Moreover, the best results were obtained with 3% by mass of candelilla wax.
[実施例2]
下記表2に示す配合割合で原料を配合して、各種整髪料を調製した(処方例7、12〜15:処方例7は表1の処方例7と同じ)。これらの整髪料を用い、専門のパネラー10名によって、「手のひらでの伸びやすさ」、「手のベタつき感」、「つや感」、「セット力」および「再セット性」について、実施例1と同様にして評価を行い、その良否を判定した。その結果を、下記表2に併記する。
[Example 2]
Various hair styling agents were prepared by blending raw materials at the blending ratio shown in Table 2 below (Prescription Examples 7, 12 to 15: Prescription Example 7 is the same as Prescription Example 7 in Table 1). Using these hair styling agents, 10 professional panelists evaluated the “easiness of stretching with palms”, “stickiness of hands”, “glossiness”, “setting power” and “resetability” in Example 1. Evaluation was performed in the same manner as above, and the quality was judged. The results are also shown in Table 2 below.
表2の結果は、ワックス類の種類を変えてその性能を評価したものである。この結果から明らかなように、ワックスの種類としてキャンデリラロウを用いたときが最も良好な結果が得られているが、他のものを用いた場合であっても一応の成果が得られていることが分かる。 The results in Table 2 are the results of evaluating the performance by changing the types of waxes. As is clear from this result, the best result was obtained when candelilla wax was used as the type of wax, but a temporary result was obtained even when another was used. I understand that.
[実施例3]
下記表3に示す配合割合で原料を配合して、各種整髪料を調製した(処方例16〜25)。これらの整髪料を用い、専門のパネラー10名によって、「手のひらでの伸びやすさ」、「手のベタつき感」、「つや感」、「セット力」および「再セット性」について、実施例1と同様にして評価を行い、その良否を判定した。その結果を、下記表3に併記する。
[Example 3]
Various hair styling agents were prepared by blending the raw materials at the blending ratio shown in Table 3 below (Prescription Examples 16 to 25). Using these hair styling agents, 10 professional panelists evaluated the “easiness of stretching with palms”, “stickiness of hands”, “glossiness”, “setting power” and “resetability” in Example 1. Evaluation was performed in the same manner as above, and the quality was judged. The results are also shown in Table 3 below.
表3の結果は、アルカンジオール類の種類を変化させて、「セット力」、「再セット性」および「つや感」に与える影響を調査したものであるが、これらのうち、1,2−ペンタンジオール、1,2−ヘキサンジオール、1,2−オクタンジオールよりなる群から選ばれる1種以上を配合したもの(処方例20〜25)では、いずれの特性においても良好は結果が得られていることがわかる。 The results in Table 3 were obtained by investigating the influence on the “setting power”, “resetting property” and “shininess” by changing the type of alkanediols. Good results were obtained in any of the characteristics obtained by blending one or more selected from the group consisting of pentanediol, 1,2-hexanediol, and 1,2-octanediol (Prescription Examples 20 to 25). I understand that.
[実施例4]
下記表4に示す配合割合で原料を配合して、各種整髪料を調製した(処方例16、26〜31:処方例16,25は表3の処方例16,25と同じ、処方例7は表1、2の処方例7と同じ)。これらの整髪料を用い、専門のパネラー10名によって、「手のひらでの伸びやすさ」、「手のベタつき感」、「つや感」、「セット力」および「再セット性」について、実施例1と同様にして評価を行い、その良否を判定した。その結果を、下記表4に併記する。
[Example 4]
Various hair styling agents were prepared by blending raw materials at the blending ratio shown in Table 4 below (Prescription Examples 16, 26 to 31: Prescription Examples 16 and 25 are the same as Prescription Examples 16 and 25 in Table 3, Prescription Example 7 is Same as Formulation Example 7 in Tables 1 and 2.) Using these hair styling agents, 10 professional panelists evaluated the “easiness of stretching with palms”, “stickiness of hands”, “glossiness”, “setting power” and “resetability” in Example 1. Evaluation was performed in the same manner as above, and the quality was judged. The results are also shown in Table 4 below.
表4の結果は、アルカンジオール類の配合量を変化させてセット力やつや感の影響について調査したものであるが、特にアルカンジオール類の配合量を0.1〜2.0質量%程度配合したものでは(処方例7、25、27、28)、セット性および再セット性を維持しつつ良好なつや感が得られていることがわかる。 The results in Table 4 are the results of investigating the influence of setting power and glossiness by changing the blending amount of alkanediols, and the blending amount of alkanediols is particularly blended by about 0.1 to 2.0% by mass. In the case of (Prescription Examples 7, 25, 27, 28), it can be seen that a good gloss feeling is obtained while maintaining the setting property and the resetting property.
[実施例5]
下記表5に示す配合割合で原料を配合して、各種整髪料を調製した(処方例32〜37)。これらの整髪料を用い、専門のパネラー10名によって、「手のひらでの伸びやすさ」、「手のベタつき感」、「つや感」、「セット力」および「再セット性」について、実施例1と同様にして評価を行い、その良否を判定した。その結果を、下記表5に併記する。
[Example 5]
Various hair styling agents were prepared by blending the raw materials at the blending ratios shown in Table 5 below (Prescription Examples 32-37). Using these hair styling agents, 10 professional panelists evaluated the “easiness of stretching with palms”, “stickiness of hands”, “glossiness”, “setting power” and “resetability” in Example 1. Evaluation was performed in the same manner as above, and the quality was judged. The results are also shown in Table 5 below.
表5の結果は、水溶性非イオン界面活性剤の量を変化させてセット力、伸びやすさおよびベタつき感の変化を調査したものであるが、20.0〜50.0質量%程度含有させたもの(処方例33〜36)ではいずれも良好な結果を示していることがわかる。 The results in Table 5 were obtained by investigating changes in setting force, easiness of elongation, and stickiness feeling by changing the amount of the water-soluble nonionic surfactant, and contained about 20.0 to 50.0% by mass. It can be seen that all the samples (prescription examples 33 to 36) show good results.
[実施例6]
下記表6に示す配合割合で原料を配合して、各種整髪料を調製した(処方例38、39)。これらの整髪料を用い、専門のパネラー10名によって、「手のひらでの伸びやすさ」、「手のベタつき感」、「つや感」、「セット力」および「再セット性」について、実施例1と同様にして評価を行い、その良否を判定した。その結果を、下記表6に併記する。
[Example 6]
Various hair styling agents were prepared by blending the raw materials at the blending ratios shown in Table 6 below (Prescription Examples 38 and 39). Using these hair styling agents, 10 professional panelists evaluated the “easiness of stretching with palms”, “stickiness of hands”, “glossiness”, “setting power” and “resetability” in Example 1. Evaluation was performed in the same manner as above, and the quality was judged. The results are also shown in Table 6 below.
表6の結果は、剤型を変えた場合を示したものであるが、いずれの剤型においても、良好な効果が得られていることが分かる。尚、処方例38のものは、LPG等のプロペラントを用いた容器に充填することによってフォーム状として使用することができ、こうした形態で用いた場合であっても同様の効果が得られることが確認できた。一方、処方例39のものは、ミスト状として使用することができ、またLPG等のプロペラントを用いた容器に充填することによってスプレー状として使用することができ、これらの形態で用いた場合であっても同様の効果が得られることが確認できた。 The results in Table 6 show the case where the dosage form is changed, but it can be seen that good effects are obtained in any dosage form. In addition, the thing of the prescription example 38 can be used as a foam by filling a container using a propellant such as LPG, and the same effect can be obtained even when used in such a form. It could be confirmed. On the other hand, those in Formulation Example 39 can be used as a mist, and can be used as a spray by filling a container using a propellant such as LPG. Even if it exists, it has confirmed that the same effect was acquired.
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