JP3455814B2 - Vibration fluidizer for powder - Google Patents
Vibration fluidizer for powderInfo
- Publication number
- JP3455814B2 JP3455814B2 JP26833399A JP26833399A JP3455814B2 JP 3455814 B2 JP3455814 B2 JP 3455814B2 JP 26833399 A JP26833399 A JP 26833399A JP 26833399 A JP26833399 A JP 26833399A JP 3455814 B2 JP3455814 B2 JP 3455814B2
- Authority
- JP
- Japan
- Prior art keywords
- vibrating
- granular material
- powder
- flow
- vibration
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Crushing And Grinding (AREA)
- Disintegrating Or Milling (AREA)
- Coating Apparatus (AREA)
- Mixers With Rotating Receptacles And Mixers With Vibration Mechanisms (AREA)
Description
【0001】[0001]
【発明の属する技術分野】本発明は、凝集粉体の解砕、
粉粒体の分散、混合、乾燥、噴霧ガス等との反応、ある
いは粉粒体表面へのコーティング、蒸着などに用いられ
る粉粒体の振動流動装置に関する。TECHNICAL FIELD The present invention relates to crushing agglomerated powder,
The present invention relates to a vibrating and flowing device for powders and granules used for dispersing, mixing, drying, reacting with a spray gas or the like for powders or granules, coating on the surface of powders or granules, or vapor deposition.
【0002】[0002]
【従来技術】一般的に、所定の容器内に充填された粉粒
体(粉粒体層)に対して垂直振動を与えると、粉粒体層
は容器内で流動する。この流動の様子は、作用させる振
動の振動数と振幅に応じて多様に変化することが知られ
ている。そして、粉粒体層と容器との相対運動に起因し
て生じる振動流動の挙動については、図4の流動パター
ンに示す如く、振動による遠心効果の大きさに伴って、
まずパターンBのように粉粒体の移動が生じて粉粒体層
表面が傾斜し、次いでパターンC1のような粉体層中心
から容器壁に向かう循環流(対流)が発生する。このと
き、循環流の速度が遅ければ振動粉粒体表面が平坦であ
るが、活発になると粉粒体表面に若干の盛り上がりを生
じる。さらに遠心効果を増大させると、パターンC2の
ように循環流の向きが逆転し、続いて粉体層内にはパタ
ーンDのように局所的な循環流が発生し、粉粒体表面に
特有の波が現れるとされている。2. Description of the Related Art Generally, when vertical vibration is applied to a powder or granular material (a powder or granular material layer) filled in a predetermined container, the powder or granular material layer flows in the container. It is known that the state of this flow changes variously depending on the frequency and amplitude of the applied vibration. Regarding the behavior of the vibration flow caused by the relative movement between the granular material layer and the container, as shown in the flow pattern of FIG.
First, the movement of the granular material occurs as in the pattern B and the surface of the granular material layer inclines, and then a circulating flow (convection) from the center of the powder layer toward the container wall as in the pattern C1 occurs. At this time, the surface of the vibrating granular material is flat when the speed of the circulating flow is slow, but when it becomes active, a slight swelling occurs on the surface of the granular material. When the centrifugal effect is further increased, the direction of the circulation flow is reversed as in the pattern C2, and then the local circulation flow is generated in the powder layer as in the pattern D, which is peculiar to the surface of the granular material. Waves are said to appear.
【0003】しかしながら、粉粒体層における振動流動
の挙動は、上記した様な若干の盛り上がりを生じながら
所定の循環流を生じる程度の範疇に止まり、それらは容
器内の場所により異なる。一方、振動振幅、周波数に対
する粉粒体層の応答はいまだ充分に解析されておらず、
振動流動は予想の難しい現象でもあることから、容器内
の全ての粉粒体が、循環流によって均一に分散されなが
らその表面に隈無く現れる確約も存しない。循環流も混
合、反応、表面処理等の各種粉粒体処理に適した高速な
ものではなく、粉粒体の振動流動を直接利用した処理装
置としては、排出装置、篩い分け装置、輸送装置などが
あるのみで、その利用範囲が限られているのが実情であ
る。粉粒体処理技術の高速化、処理の均一化が要望され
ている昨今において、凝集粉体の解砕、粉粒体の分散、
混合、噴霧ガス等との反応や、粉粒体表面へのコーティ
ング、蒸着などの処理が行えると共に、これらの処理を
短時間に行える粉粒体の振動流動装置の出現が望まれて
いた。なお、特異な円振動により粉粒体を粉砕するよう
にした振動ミルなるものが知られているが、このものは
筒状容器内で球状等の媒体に円形となる振動軌跡を与え
て、容器内壁に球状媒体を衝突させ、容器内壁と球状媒
体との間で粉粒体を粉砕するようにしたものであり、か
かる観点からすれば、粉粒体そのものの循環流を利用し
たものでなく、採用することはできない。However, the behavior of the vibrating flow in the granular layer is limited to the extent that a predetermined circulating flow is generated while the above-mentioned slight rise occurs, and the behavior varies depending on the location in the container. On the other hand, the response of the granular layer to the vibration amplitude and frequency has not been fully analyzed yet,
Since oscillating flow is also a phenomenon that is difficult to predict, there is no guarantee that all the particles in the container will be uniformly dispersed by the circulating flow and appear on the surface of the particles. The circulating flow is not a high-speed one suitable for various powder and granule treatments such as mixing, reaction, and surface treatment.As a processing device that directly uses the vibrational flow of the powder and granules, a discharge device, a sieving device, a transportation device, etc. However, in reality, the range of use is limited. In recent years, there has been a demand for high-speed powder particle processing technology and uniform processing.
It has been desired to develop a vibrating and fluidizing device for powders and granules, which can perform processing such as mixing, reaction with spray gas, coating on the surface of powder and granules, vapor deposition, and the like, and can perform these processings in a short time. There is known a vibration mill that crushes powder particles by a unique circular vibration, but this one gives a circular vibration locus to a spherical medium in a cylindrical container, The spherical medium is made to collide with the inner wall so as to pulverize the granular material between the inner wall of the container and the spherical medium, and from this point of view, the circulating flow of the granular material itself is not used, It cannot be adopted.
【0004】[0004]
【発明が解決しようとする課題】本発明は、上記の如き
問題点を一掃すべく創案されたものであって、空気やガ
ス等の流動化媒体、あるいは衝撃球等の固体媒体などを
用いることなく、粉粒体層における粉粒体の循環挙動
を、粉粒体層の場所により異なる循環流が生じたとして
も、全ての粉粒体が循環流によって均一に分散されなが
らその層表面に隈無く、しかも瞬時に繰り返し現れるよ
うにすることができ、循環する粉粒体に対して直接的
に、凝集粉体の解砕、粉粒体の分散、混合、乾燥、噴霧
ガス等との反応、あるいは粉粒体表面へのコーティン
グ、蒸着などの複合的な処理を短時間に行うことができ
る。さらに、その循環挙動は、従来の如き僅かな盛り上
がり程度の循環流でなく、飛散状、あるいは飛柱状に噴
出させることができ、変化に富んだ循環流制御を可能と
し得るばかりか、かかる噴出粉粒体に対してのみ前記反
応や加工等の処理を行うことも可能となり、もって全体
の機械構成が殊更複雑なものとならず、小型化を容易な
らしめる粉粒体の振動流動装置を提供することを目的と
する。The present invention was devised to eliminate the above-mentioned problems, and uses a fluidizing medium such as air or gas, or a solid medium such as an impact ball. without Kuma circulation behavior of granular material in the particle layer, even as different circulating flow is caused by the location of the particle layer, on the layer surface with all granular material is uniformly dispersed by circulation It can be made to appear repeatedly without any time instantly, directly to the circulating powder and granules, crushing agglomerated powder, dispersing and mixing powder and granules, reaction with spray gas, etc., Alternatively, composite treatment such as coating or vapor deposition on the surface of the powder or granular material can be performed in a short time. Further, the circulation behavior of the sprayed powder is not limited to the conventional circulation flow with a slight rise, but can be ejected in a scattered or columnar shape, which enables a variety of circulation flow control, as well as the spray powder. It is also possible to perform the above-mentioned reaction, processing, etc. only on the granules, so that the overall mechanical structure does not become particularly complicated, and a vibration and fluidization apparatus for powder granules that facilitates miniaturization is provided. The purpose is to
【0005】[0005]
【課題を解決するための手段】上記課題を解決するため
に本発明が採用した技術手段は、容器内に充填された粉
粒体を粉粒体層とし、該粉粒体層に振動を与えて流動さ
せることで循環流を生成するに、粉粒体の処理手段を、
振動手段に連携してなる前記容器と該容器内に敷設状に
配設される振動媒体とからなる異種振動体を組として構
成し、該粉粒体の処理手段は、前記粉粒体層における粉
粒体の流動挙動を、前記異種振動体間に連続的に生ずる
共同振動作用により粉粒体層に振動を与えて、粉粒体が
容器底面から層表面に繰り返し出現する循環流を生成す
るよう循環流制御すべく構成されていることを特徴とす
るものである。[Means for Solving the Problems] The technical means adopted by the present invention for solving the above-mentioned problems is a powder filled in a container.
The granular material is made into a granular material layer, and the granular material layer is vibrated to be fluidized.
In order to generate a circulating flow by
Heterologous vibrator comprising a vibrating medium is <br/> arranged in laying shape made in conjunction with the container and said container to a vibration means configured as a set, the processing means of the powder and granular material, said powder the flow behavior of the powder particles in the particle layer, giving vibration to the particle layer by co-vibrating action occurring continuously between the different vibration body, granular material appears repeatedly from the container bottom surface of the layer circulation It is characterized in that it is arranged to control the circulation flow so as to generate a flow.
【0006】[0006]
【発明の実施の形態】以下、本発明の実施の形態を好適
な実施の形態として例示する粉粒体の振動流動装置に基
づいて詳細に説明する。図1〜図3において、図1は、
振動流動装置の一部破断全体図である。1は振動手段と
しての振動装置であり、該振動装置1は、特開平08−
193911号公報に開示された如きの電動型振動装置
で、振動台101の下面に一体的に設けられた円柱状の
中央磁極と、該中央磁極の外周面に駆動コイルを存して
対向配設された円環状磁極とによって構成される一方を
N極とし、他方をS極とする固定磁石機構を備え、前記
駆動コイルへ交流電流を供給することにより、前記固定
磁石における両磁極の相互間の磁界中で駆動コイルが上
下に振動し、加振力を振動台101に与える機構を備え
ている。加振力の増減は交流電流の周波数の増減によっ
て操作され、高周波領域における振動が得られる構成と
なっている。なお、振動の発生方法(原理)としては、
上記の電磁振動に限定されることなく、超音波振動、磁
歪振動、電動機のアンバランスによる振動や、これら振
動発生方法を適宜組み合わせても良く、また、上下振
動、左右振動およびこれらの複合振動等種々のものであ
っても良い。BEST MODE FOR CARRYING OUT THE INVENTION Hereinafter, an embodiment of the present invention will be described in detail based on a vibrating and flowing apparatus for powder and granules illustrated as a preferred embodiment. 1 to 3, FIG.
It is a partially broken whole view of a vibration flow device. Reference numeral 1 is a vibrating device as a vibrating means.
In the electric vibration device as disclosed in Japanese Patent No. 193911, a cylindrical central magnetic pole integrally provided on the lower surface of the vibrating table 101 and a drive coil are provided on the outer peripheral surface of the central magnetic pole so as to face each other. A fixed magnet mechanism having one pole as an N pole and the other pole as an S pole, and an alternating current is supplied to the drive coil so that the magnetic poles of the fixed magnet are connected to each other. The drive coil is vertically vibrated in a magnetic field, and a mechanism for applying an exciting force to the vibrating table 101 is provided. The increase / decrease of the excitation force is operated by the increase / decrease of the frequency of the alternating current, so that the vibration in the high frequency region is obtained. In addition, as a generation method (principle) of vibration,
Not limited to the above electromagnetic vibrations, ultrasonic vibrations, magnetostrictive vibrations, vibrations due to unbalance of electric motors, and methods of generating these vibrations may be appropriately combined, and vertical vibrations, lateral vibrations, and composite vibrations thereof. It may be various.
【0007】2は振動台101上に装着された容器であ
って、該容器2内には、粉粒体3が充填されており、底
部には振動媒体4としての複数の球体401が集合体と
して敷設状に投入されている。そして、前記振動装置1
の稼動に連携して発生する前記振動台101の振動が、
前記容器2に対して直接的に伝播され、前記球体401
に対しては容器2を介して間接的に伝播される構成とな
っている。すなわち、この容器2と球体401とは、夫
々異なる振動を処理すべき粉粒体3に与える一組の異種
振動体2、4となっており、異種振動体の一方を構成す
る容器2からの振動を、他方を構成する球体401が享
受する連携関係によって、両者の共同振動作用により粉
粒体3を流動処理する構成となっている。なお、振動媒
体4は、球体401に替えて多孔板体402や、棒体、
筒状体、メッシュ等網状体などを用いても良く、その形
状、材質は任意であり、また、多孔板体402などに振
動装置の振動を直接的に伝播し、当該振動を容器2ある
いは他の構成体に間接的に伝播する構成としても良い。
さらに、振動装置を容器2と振動媒体41のそれぞれに
直接連携させて、異なる振幅、周波数の振動を各々直接
伝播させる構成としても良く、要は、異種振動体を組と
して当該振動体の共同振動作用によって粉粒体3を処理
できる構成で有ればよい。Reference numeral 2 denotes a container mounted on the vibrating table 101. The container 2 is filled with powder particles 3, and a plurality of spheres 401 as the vibration medium 4 are aggregated at the bottom. Has been put into the laying state. Then, the vibration device 1
The vibration of the vibrating table 101 generated in association with the operation of
The sphere 401 is propagated directly to the container 2.
Is transmitted indirectly via the container 2. That is, the container 2 and the sphere 401 are a set of different kinds of vibrating bodies 2 and 4 which give different vibrations to the powdery or granular material 3 to be processed. By virtue of the cooperative relationship in which the sphere 401 that constitutes the other enjoys the vibration, the powder and granules 3 are fluidized by the joint vibration action of the two. The vibrating medium 4 is replaced with the spherical body 401, the perforated plate body 402, the rod body,
A tubular body, a mesh body such as a mesh may be used, and the shape and the material thereof are arbitrary, and the vibration of the vibrating device is directly propagated to the perforated plate body 402 and the like, and the vibration is transmitted to the container 2 or other. The configuration may be such that it is indirectly propagated to the structure.
Further, the vibrating device may be directly linked to each of the container 2 and the vibrating medium 41 so that vibrations of different amplitudes and frequencies are directly propagated. It suffices that the powder and granular material 3 can be processed by the action.
【0008】次に上記のように構成した振動流動装置を
用いた粉粒体の振動流動の挙動に対する実験例について
説明する。振動装置1としては、株式会社アカシ製の電
動型マイクロ加振機(MES451)を用いた。
(1)振動媒体に球体を用いた実験例
球体401を用いて粉粒体3を処理する場合において、
球体401としては平均粒径5mmのガラスビーズを用
い、粉粒体3としては平均粒径5μmのポリエチレン粒
子(白色)を容器2に約1cmの高さまで充填させて粉
粒体層を形成し、振動数1〜10kHz、振幅0.1〜
10mmの振動を与えてみた。而して、その振動流動の
挙動状態を図2(A)に図面代用写真として示すと共
に、その状態説明図を図2(B)に示す。図2(B)
は、図2(A)のものに粉粒体の噴出流301と球体4
01にそれぞれコントラストおよび明暗調の色調処理を
加えて、その流動状態を明確にしたものである。Next, an example of an experiment for the behavior of the vibrating flow of the granular material using the vibrating flow device configured as described above will be described. As the vibration device 1, an electric micro-exciter (MES451) manufactured by Akashi Co., Ltd. was used. (1) Experimental example in which spheres are used as the vibration medium In the case of treating the powdery particles 3 using the spheres 401,
Glass beads having an average particle diameter of 5 mm are used as the spheres 401, and polyethylene particles (white) having an average particle diameter of 5 μm are filled as the powder particles 3 into the container 2 to a height of about 1 cm to form a powder particle layer. Frequency 1-10 kHz, amplitude 0.1
I gave a vibration of 10 mm. Then, the behavioral state of the oscillating flow is shown in FIG. 2 (A) as a drawing substitute photograph, and the state explanatory view is shown in FIG. 2 (B). Figure 2 (B)
2A is the same as the one shown in FIG.
No. 01 is subjected to contrast and light / dark tone color processing to clarify the flow state.
【0009】まず、容器2内の粉粒体3に振動装置の上
下振動による加振力を与えると、粉粒体層の表面に存在
していた粉粒体が瞬時に容器2底部に移動し、2〜3秒
後には再び表面に現れる挙動を示した。この挙動の様子
は、粉粒体層の表面中央部分に平均粒径約100μmの
着色粒子(赤色)を少量乗せた状態から混合、分散に対
する流動挙動を観察したものであるが、これらの流動挙
動は、比較的小さな加振力である初期の振動段階におい
ても、前記着色粒子が容器2内全域で瞬時に、かつ均一
に分散されながら、再びその表面に隈無く現れる良好な
循環流が生成されていることで確認された。このよう
に、物性(粒径、密度等)が異なる粉粒体であっても、
短時間で均一に混合、分散されることが分かった。First, when a vibrating force is applied to the granular material 3 in the container 2 by the vertical vibration of the vibrating device, the granular material existing on the surface of the granular material layer instantly moves to the bottom of the container 2. After 2 to 3 seconds, the behavior again appeared on the surface. This behavior is observed by observing the flow behavior for mixing and dispersion from a state in which a small amount of colored particles (red) having an average particle size of about 100 μm are put on the central part of the surface of the granular material layer. In the initial vibrating stage, which is a relatively small exciting force, the colored particles are instantly and uniformly dispersed in the entire area of the container 2, and a good circulation flow that appears again on the surface is generated. Have been confirmed. In this way, even if the powder or granular material has different physical properties (particle size, density, etc.),
It was found that they were uniformly mixed and dispersed in a short time.
【0010】次に、加振力を徐々に高め高周波領域での
挙動を観察したところ、図2(A)の図面代用写真に示
す如きに、粉粒体3が球体401の間から上方に激しく
霧状に噴出する流動挙動が確認された。その状態を図2
(B)に基づいて説明すると、粉粒体3は、球体401
が敷設された領域において、噴出初期状態では、お湯が
沸騰した様な状態で至る所で間欠状の噴出流301が確
認され、さらに加振力を増大させると、容器2の中央域
では連続的な噴出流301となり、外周域では間欠状の
噴出流301となって噴出する挙動が確認された。その
際、球体401はランダムに回転しており、隣接する球
体401により囲繞された隙間から、粉粒体3の噴出と
容器2底部側への移動が繰り返し行なわれると共に、容
器2側壁面に飛散した粉粒体3は球体401の敷設周縁
域より容器2底部側へ移動する挙動を示した。同様に、
球体401を用いない従来の振動流動挙動について比較
観察した結果、着色粒子に対してその周縁の粉粒体3が
徐々に被さり、全ての着色粒子を覆って表面から視認で
きなくなるまでに約1分ほどの時間を要した。更に加振
力を増大した高周波領域の振動を与えても再び表面に現
れることが無く、分散、混合に良好な循環流が生成され
ないことが確認された。Next, when the vibration force was gradually increased and the behavior in the high frequency region was observed, as shown in the drawing-substitute photograph of FIG. 2 (A), the particles 3 were violently moved upward from between the spheres 401. The flow behavior of mist-like ejection was confirmed. Figure 2
Describing based on (B), the powder and granules 3 are the spheres 401
In the region where the slab was laid, an intermittent jet flow 301 was confirmed everywhere in a state where the hot water boiled in the initial state of jetting, and when the exciting force was further increased, it continued in the central region of the container 2. It was confirmed that the jet flow 301 was a normal jet flow and that the jet flow 301 was an intermittent jet flow in the outer peripheral region. At that time, the spheres 401 are randomly rotating, and the powder particles 3 are repeatedly ejected from the gap surrounded by the adjacent spheres 401 and moved to the bottom side of the container 2 and are scattered on the side wall surface of the container 2. The powdery granules 3 exhibited a behavior of moving from the laid peripheral region of the sphere 401 to the bottom side of the container 2. Similarly,
As a result of comparative observation of the conventional vibrating flow behavior that does not use the sphere 401, it takes about 1 minute before the colored particles 3 gradually cover the colored particles 3 and cover all the colored particles and become invisible from the surface. It took a while. Further, it was confirmed that even if a vibration in a high frequency region with an increased excitation force is applied, it does not appear again on the surface, and a good circulation flow for dispersion and mixing is not generated.
【0011】(2)振動媒体に多孔板体を用いた実験例
上記実験例(1)の条件下において、球体401に替え
てステンレス製で孔径が2mm、板厚が0.5mmの多
孔板体402を用いて粉粒体層に振動を与えてみた。而
して、その振動流動の挙動状態を図3(A)に図面代用
写真として示すと共に、その状態説明図を図3(B)に
示す。図3(B)は、図3(A)のものに粉粒体の噴出
流302と多孔板体402にコントラストおよび明暗調
の色調処理を加えて、その流動状態を明確にしたもので
ある。まず、容器2内の粉粒体3に振動装置の上下振動
による加振力を与えると、粉粒体層の表面に存在してい
た粉粒体が瞬時に容器2底部に移動し、2〜3秒後には
再び表面に現れるという上記実験例(1)と略同様の挙
動を示した。(2) Experimental example using a perforated plate as the vibration medium Under the conditions of the above experimental example (1), the perforated plate having a hole diameter of 2 mm and a plate thickness of 0.5 mm is made of stainless instead of the spherical body 401. 402 was used to apply vibration to the granular layer. Then, the behavior state of the oscillating flow is shown in FIG. 3 (A) as a drawing substitute photograph, and the state explanatory view is shown in FIG. 3 (B). FIG. 3 (B) shows the flow state of the powder / granule jet flow 302 and the perforated plate body 402 by applying contrast and light / dark tone color processing to that of FIG. 3 (A). First, when an exciting force is applied to the granular material 3 in the container 2 by the vertical vibration of the vibrating device, the granular material existing on the surface of the granular material layer instantly moves to the bottom of the container 2, The same behavior as that of the above-mentioned experimental example (1) was exhibited in which the surface appeared again after 3 seconds.
【0012】次に、加振力を徐々に高め高周波領域での
挙動を観察したところ、図3(A)の図面代用写真に示
す如きの粉粒体3が多孔板体402の孔から上方に激し
く柱状に噴出する流動挙動が確認された。その状態を図
3(B)に基づいて説明すると、粉粒体3は、多孔板体
402が設置された領域において、噴出初期状態では、
至る所で間欠状に噴出流302が確認され、さらに加振
力を増大させると、多孔板体の全域が一体となった状態
で間欠状の噴出流302となって噴出する挙動が確認さ
れた。その際、粉粒体3は、多孔板の下面域にある粉粒
体3が各孔から一気に飛び出す噴出と、容器2底部側へ
の移動が繰り返し行なわれると共に、容器2側壁面に飛
散した粉粒体3は多孔板体402の敷設周縁域より容器
2底部側へ移動する挙動を示した。更に、孔径が1cm
の多孔板を用いて噴出状態を確認したところ、各孔の円
周域からの噴出であったことが確認された。なお、多孔
板体402は網状のものであっても良い。また、上記実
験例において、流動環境を徐々に減圧すると、噴出流動
が減少することが確認されたが、本発明の装置構成を減
圧下(減圧された容器内)でも応用できることが分かっ
た。Next, when the vibration force was gradually increased and the behavior in the high frequency region was observed, powder particles 3 as shown in the drawing-substitute photograph of FIG. A violent columnar flow behavior was confirmed. The state will be described based on FIG. 3 (B). In the region in which the perforated plate body 402 is installed, the powdery or granular material 3 is
The jet flow 302 was confirmed to be intermittent everywhere, and when the vibration force was further increased, it was confirmed that the jet flow 302 was formed into an intermittent jet flow 302 with the entire area of the perforated plate being integrated. . At that time, the powdery particles 3 are ejected from the holes in the lower surface area of the perforated plate at a stroke, and the powdery particles 3 are repeatedly moved to the bottom side of the container 2 and scattered on the side wall surface of the container 2. The granules 3 showed a behavior of moving from the laid peripheral region of the perforated plate body 402 to the bottom side of the container 2. Furthermore, the hole diameter is 1 cm
When the ejection state was confirmed using the perforated plate of No. 3, it was confirmed that the ejection was from the circumferential region of each hole. In addition, the perforated plate body 402 may have a mesh shape. Further, in the above experimental example, it was confirmed that the jet flow was reduced when the flow environment was gradually reduced, but it was found that the apparatus configuration of the present invention can be applied even under reduced pressure (in a reduced pressure container).
【0013】上記技術手段によれば、凝集粉体の解砕、
粉粒体の分散、混合、乾燥等の粒子材料を処理するに必
要な振動流動を得るためには、粉粒体層に対して、振動
媒体から粉粒体が噴出するような加振力を与えなくと
も、殆どの粉粒体が瞬時にかつ均一に分散されながら、
粉粒体層表面に隈無く確実に出現する良好な循環流を得
ることができ、空気やガス等の流動媒体、あるいは衝撃
球等の固体媒体などを用いることなく、振動流動による
循環流のみで直接処理することができる。さらに、その
循環挙動は、粉粒体層表面を平滑なものから飛散状、あ
るいは飛柱状に噴出させるという、変化に富んだ循環流
制御が可能となり、かかる噴出粉粒体に対してのみ噴霧
ガス等との反応、コーティング、蒸着などの複合的な処
理を行うようにすることも可能となり、全体の機械構成
が殊更複雑なものとならず、小型化を容易ならしめるこ
ができる。According to the above technical means, crushing of agglomerated powder,
In order to obtain the vibrating flow necessary for processing the particulate material such as dispersion, mixing, and drying of the granular material, a vibrating force that ejects the granular material from the vibrating medium is applied to the granular material layer. Even if it is not given, most of the powders are instantly and uniformly dispersed,
It is possible to obtain a good circulating flow that reliably appears on the surface of the granular material layer without using a fluid medium such as air or gas, or a solid medium such as an impact ball, and only by the circulating flow due to oscillatory flow. It can be processed directly. In addition, its circulation behavior enables a variety of circulating flow control, such as spraying the surface of the granular material layer from a smooth surface to a scattered or columnar shape, and the spray gas can be sprayed only to the sprayed granular material. It is also possible to carry out complex treatments such as reaction with the like, coating, vapor deposition, etc., and the overall mechanical structure does not become particularly complicated, and miniaturization can be facilitated.
【0014】上記振動流動の挙動メカニズムについて
は、力学的に充分に解析あるいは解明されておらず、予
測の難しい現象であるが、次のような作用を有するもの
と思われる。
振動装置1に直接的に連携された振動体(容器2)
は、その上下振動エネルギーを粉粒体3、および振動装
置1に間接的に連携された振動体(振動媒体4)に伝播
する。振動媒体4は、それが有する質量や大きさ、形状
等の物性による上下運動や、球体、柱状体等の独立集合
体の場合には回転運動も加わり、独自の振動エネルギー
を誘発する。The behavior mechanism of the oscillating flow is a phenomenon which is difficult to predict because it has not been mechanically sufficiently analyzed or clarified, but it is considered to have the following action. A vibrating body (container 2) directly linked to the vibrating device 1.
Propagates its vertical vibration energy to the granular material 3 and the vibrating body (vibrating medium 4) indirectly linked to the vibrating device 1. The vibrating medium 4 induces its own vibrational energy by adding vertical movement due to physical properties such as mass, size and shape of the vibrating medium 4 and rotational movement in the case of an independent aggregate such as a sphere or a columnar body.
【0015】 容器2と振動媒体4は、それぞれ異な
る振動(異種振動)体を構成し、その共同振動作用によ
りミクロ的な衝突などによる複合的なエネルギーが両者
間に発生する。その際、容器2と振動媒体4の間に存在
する粉粒体3は、空気等の気体分子と共に激しく流動
し、内側から上方に押し出され、あるいは飛び出される
格好で、振動媒体4の隙間や孔から上方へ移動(噴出)
する加速度エネルギーが与えられる。The container 2 and the vibrating medium 4 respectively form different vibrating (different vibrating) bodies, and the combined vibration action generates complex energy between them due to a microscopic collision or the like. At that time, the granular material 3 existing between the container 2 and the vibrating medium 4 vigorously flows together with gas molecules such as air, and is pushed out or jumped out from the inside, and the gap of the vibrating medium 4 or Move upward from the hole (spout)
Acceleration energy is applied.
【0016】 振動媒体4の上方へ移動した粉粒体3
は、振動により拡散され、振動媒体4の下面で粉粒体3
の存在が少なくなった箇所、すなわち噴出流の小さい箇
所より再び下方へ移動する。この繰り返しによる循環流
が流動層を形成し、粉粒体3は、殆どの粉粒体が高速か
つ均一に分散されながら、粉粒体層表面に隈無く確実に
出現する挙動となって現れる。以上の異種振動による共
同振動作用によって、振動流動挙動に対する改善がなさ
れるものと推認される。The granular material 3 moved above the vibrating medium 4
Are diffused by the vibration, and the powder particles 3 are formed on the lower surface of the vibrating medium 4.
Moves to the lower part again from the place where there is less, that is, the place where the jet flow is small. The circulation flow due to this repetition forms a fluidized bed, and most of the powder and granules 3 are dispersed at high speed and evenly, and the powder and granules 3 appear in a reliable manner without appearing on the surface of the powder and granule layer. It is presumed that the above-mentioned joint vibration action due to different kinds of vibrations improves the vibrating flow behavior.
【図1】粉粒体の振動流動装置の全体構成図FIG. 1 is an overall configuration diagram of a vibrating fluidizer for powder and granular material
【図2】実験例1の挙動状態を例示した図面代用写真
(A)とその説明図(B)FIG. 2 is a drawing-substitute photograph (A) illustrating the behavioral state of Experimental Example 1 and its explanatory view (B).
【図3】実験例2の挙動状態を例示した図面代用写真
(A)とその説明図(B)FIG. 3 is a drawing-substituting photograph (A) illustrating the behavioral state of Experimental Example 2 and its explanatory view (B).
【図4】一般的な粉粒体の振動流動の挙動パターンを示
す説明図FIG. 4 is an explanatory diagram showing a behavioral pattern of vibration and flow of a general granular material.
1 振動装置 101 振動台 2 容器 3 粉粒体 301 粉粒体の噴出流 302 粉粒体の噴出流 4 振動媒体 401 球状体 402 多孔板体 1 Vibration device 101 Shaking table 2 containers 3 powder 301 Ejection flow of powder 302 Jet flow of powder 4 Vibration medium 401 spherical body 402 Perforated plate
Claims (5)
し、該粉粒体層に振動を与えて流動させることで循環流
を生成するに、粉粒体の処理手段を、振動手段に連携し
てなる前記容器と該容器内に敷設状に配設される振動媒
体とからなる異種振動体を組として構成し、該粉粒体の
処理手段は、前記粉粒体層における粉粒体の流動挙動
を、前記異種振動体間に連続的に生ずる共同振動作用に
より粉粒体層に振動を与えて、粉粒体が容器底面から層
表面に繰り返し出現する循環流を生成するよう循環流制
御すべく構成されていることを特徴とする粉粒体の振動
流動装置。1. A granular material filled in a container as a granular material layer.
Then, the circulating flow is achieved by vibrating the granular material layer to cause it to flow.
To generate the processing means particulate material, constitutes a heterogeneous vibrator comprising a vibrating medium disposed laying shape cooperation with the container and said container comprising a vibrating means as a set, powder processing means of the granules is the flow behavior of the powder particles in the particle layer, giving vibration to the particle layer by co-vibrating action occurring continuously between the different vibration body, granular material containers An oscillating flow device for powder and granular material, which is configured to control a circulating flow so as to generate a circulating flow repeatedly appearing from the bottom surface to the surface of the bed.
動手段への連携は、一方の振動体に振動手段を連動連結
した連携と、該一方の振動体からの振動を他方の振動体
が享受する連携とによって構成されていることを特徴と
する粉粒体の振動流動装置。2. The cooperation of the different vibrating body to the vibrating means according to claim 1, wherein the vibrating means is linked to one vibrating body in an interlocking manner, and the vibration from the one vibrating body is linked to the other vibrating body. An oscillating fluidizing device for powder and granular material, characterized in that it is configured with the cooperation to be enjoyed.
動手段への連携は、それぞれの振動体が異なる振動によ
って制御されるよう振動手段に連動連結された連携で構
成されていることを特徴とする粉粒体の振動流動装置。3. The cooperation according to claim 1, wherein the different vibrating body cooperates with the vibrating means by interlocking connection with the vibrating means so that the respective vibrating bodies are controlled by different vibrations. A vibrating fluidizer for powder and granules.
は、多孔板であることを特徴とする粉粒体の振動流動装
置。4. The vibrating fluidizer of claim 1, wherein the vibrating medium is a perforated plate.
は、複数の球状体等からなる集合体であることを特徴と
する粉粒体の振動流動装置。5. The vibrating fluidizer of claim 1, wherein the vibrating medium is an aggregate made up of a plurality of spherical bodies and the like.
Priority Applications (7)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP26833399A JP3455814B2 (en) | 1999-09-22 | 1999-09-22 | Vibration fluidizer for powder |
US10/088,781 US7264192B1 (en) | 1999-09-22 | 2000-09-20 | Particulate matter vibro-fluidizing apparatus |
PCT/JP2000/006405 WO2001021314A1 (en) | 1999-09-22 | 2000-09-20 | Vibro-fluidizing device for powder particles |
EP00961104A EP1219354B1 (en) | 1999-09-22 | 2000-09-20 | Vibro-fluidizing device for powder particles |
AU73171/00A AU7317100A (en) | 1999-09-22 | 2000-09-20 | Vibro-fluidizing device for powder particles |
AT00961104T ATE506121T1 (en) | 1999-09-22 | 2000-09-20 | DEVICE FOR VIBRO-FLUIDIZATION OF POWDER PARTICLES |
DE60045866T DE60045866D1 (en) | 1999-09-22 | 2000-09-20 | DEVICE FOR VIBRO FLUIDIZATION OF POWDER PARTS |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP26833399A JP3455814B2 (en) | 1999-09-22 | 1999-09-22 | Vibration fluidizer for powder |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2001087666A JP2001087666A (en) | 2001-04-03 |
JP3455814B2 true JP3455814B2 (en) | 2003-10-14 |
Family
ID=17457097
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JP26833399A Expired - Fee Related JP3455814B2 (en) | 1999-09-22 | 1999-09-22 | Vibration fluidizer for powder |
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JP4061573B2 (en) | 2001-05-18 | 2008-03-19 | ソニー株式会社 | Conductive catalyst particle manufacturing method, gas diffusing catalyst electrode manufacturing method, and apparatus used for conductive catalyst particle manufacturing method |
JP4061575B2 (en) | 2001-06-01 | 2008-03-19 | ソニー株式会社 | Conductive catalyst particles and method for producing the same, gas diffusive catalyst electrode, and electrochemical device |
JP2008100227A (en) * | 2001-06-01 | 2008-05-01 | Sony Corp | Conductive catalyst particle and its manufacturing method, gas-diffusing catalyst electrode, and electrochemical device |
JP2020104079A (en) * | 2018-12-28 | 2020-07-09 | 大有株式会社 | Container lid, container with lid fitted thereto, and mixing method with use of container |
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1999
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