JP3124518B2 - Cutting oil supply and recovery method and cutting oil - Google Patents
Cutting oil supply and recovery method and cutting oilInfo
- Publication number
- JP3124518B2 JP3124518B2 JP20057398A JP20057398A JP3124518B2 JP 3124518 B2 JP3124518 B2 JP 3124518B2 JP 20057398 A JP20057398 A JP 20057398A JP 20057398 A JP20057398 A JP 20057398A JP 3124518 B2 JP3124518 B2 JP 3124518B2
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- Japan
- Prior art keywords
- water
- oil
- cutting oil
- insoluble
- cutting
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Description
【0001】[0001]
【発明の属する技術分野】本発明は、切削加工に用いら
れる切削油、及び、切削油の供給方法に関し、特に、再
使用するのに適した不水溶性切削油に関するものであ
る。BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a cutting oil used for cutting and a method for supplying the cutting oil, and more particularly to a water-insoluble cutting oil suitable for reuse.
【0002】[0002]
【発明が解決しようとする課題】本出願人は、先に、不
水溶性油剤を用いて安定した切削加工を実現すると共
に、防災面での対策も万全である新規な切削加工方法を
提案している(特願平9−254167号)。この発明
は、不水溶性切削油とその他の水溶液を、同時にか又は
時間的に切り換えて使用すると共に、一の回収槽に回収
した後、比重差に基づいて両者を分離させるものであ
る。この方法は、画期的な切削加工方法として業界で注
目されているが、不水溶性切削油とその他の水溶液の分
離性を更に改善し、再使用する不水溶性切削油の純度を
高めることができれば更に好ましい。SUMMARY OF THE INVENTION The present applicant has previously proposed a novel cutting method which realizes stable cutting by using a water-insoluble oil agent, and which takes thorough measures against disasters. (Japanese Patent Application No. 9-254167). The present invention is to use a water-insoluble cutting oil and another aqueous solution at the same time or by switching over time, collect them in one collection tank, and then separate them based on a difference in specific gravity. Although this method has been attracting attention in the industry as a revolutionary cutting method, it further improves the separation of water-insoluble cutting oil from other aqueous solutions and increases the purity of water-insoluble cutting oil to be reused. It is even more preferable if this can be achieved.
【0003】本発明は、この点に鑑みてなされたもので
あって、再使用する不水溶性切削油の純度を更に高める
ことができる切削油供給方法を提供することを目的とす
る。また、水溶液との分離性が特に優れる不水溶性切削
油を提供することを目的とする。なお、本明細書では、
便宜上、切削加工や水溶液の文言を用いるが、切削加工
には研削加工その他の類似の加工も含み、水溶液には、
水道水などの水そのものも含むことにする。The present invention has been made in view of the above, and an object of the present invention is to provide a cutting oil supply method capable of further increasing the purity of a water-insoluble cutting oil to be reused. Another object of the present invention is to provide a water-insoluble cutting oil that is particularly excellent in the separability from an aqueous solution. In this specification,
For the sake of convenience, the terms cutting and aqueous solution are used, but cutting includes grinding and other similar processes, and aqueous solutions include
Water itself, such as tap water, will be included.
【0004】[0004]
【課題を解決するための手段】上記の課題を解決するた
め、本発明に係る切削油の回収供給方法では、ポリアル
ファオレフィンもしくは高度精製油を主成分とする不水
溶性切削油を使用する切削加工時に、水溶液を加工箇所
に供給すると共に、不水溶性切削油及び水溶液を一の回
収槽に回収貯留して、不水溶性切削油とその他の水溶液
を分離して、それぞれを切削加工時に再使用する方法で
あって、前記不水溶性切削油の吸い込み口を上向きに設
定して油面に合わせて上下させるようにしている。不水
溶性切削油とその他の水溶液を一の回収槽に回収して再
使用する場合、不水溶性切削油に混入した水分は、粘度
の関係もあって、直ぐには分離しない。しかしながら、
比重の関係から、一般に、油面に近いほど不水溶性切削
油に混入した水分が少なくなる。そこで、本発明では、
不水溶性切削油の吸い込み口を油面に合わせて上下させ
るようにして、油面に近いところから不水溶性切削油を
吸い上げるようにした。すなわち、本発明では、不水溶
性切削油を使用する切削加工時に、水溶液を加工箇所に
供給する(典型的には、噴霧または噴射する)切削加工
において、回収液を一の回収槽に回収貯留して、不水溶
性切削油とその他の水溶液を分離してそれぞれを再使用
するに際し、不水溶性切削油の吸い込み口を油面に合わ
せて上下させるようにしている。なお、吸い込み口を上
下させる方法としては、吸い込み口に近接してフロート
を付けるなどの方法があり、吸い込み口の位置は、設備
の状況に合わせて適宜に可変すれば良い。吸い込み口を
下向きに設定した場合、不水溶性切削油の分離度合いや
ポンプの吸引力などによっては、不水溶性切削油と水溶
液の境界部の液も含めて吸ってしまう恐れがあるが、吸
い込み口を上向きに設定すれば、確実に高純度の不水溶
性切削油を吸引することができる。本発明において、不
水溶性切削油とその他の水溶液を分離させるには、両者
の比重差を利用するのが簡易であるが、比重差を利用す
る方法に加えて、撥水性フィルターやバブリング装置を
用いてもよい。なお、撥水性フィルターとは、油分のみ
を通過させるフィルターであり、バブリング装置とは、
エアーの噴出によって水と油の分離を促進する装置であ
る。Means for Solving the Problems To solve the above problems,
In the method for recovering and supplying cutting oil according to the present invention,
Non-aqueous water based on farolefin or highly refined oil
During cutting using a soluble cutting oil, the aqueous solution
And water-insoluble cutting oil and aqueous solution once.
Collect and store in the collection tank, and use water-insoluble cutting oil and other aqueous solutions.
Are separated and reused at the time of cutting.
The suction port for the water-insoluble cutting oil is set upward.
It is set up and down according to the oil level . When the water-insoluble cutting oil and another aqueous solution are collected in one collection tank and reused, the water mixed in the water-insoluble cutting oil is not immediately separated due to the viscosity. However,
From the relation of the specific gravity, generally, the water mixed in the water-insoluble cutting oil decreases as the oil level increases. Therefore, in the present invention,
The suction port of the water-insoluble cutting oil was moved up and down in accordance with the oil level, so that the water-insoluble cutting oil was sucked up from a position near the oil level. That is, in the present invention, in a cutting process in which an aqueous solution is supplied to a processing location (typically, spraying or spraying) during a cutting process using a water-insoluble cutting oil, the collected liquid is collected and stored in one collection tank. When the water-insoluble cutting oil and other aqueous solutions are separated and reused, the suction port of the water-insoluble cutting oil is moved up and down in accordance with the oil level. In addition, as a method of moving the suction port up and down, there is a method of attaching a float near the suction port, and the position of the suction port may be appropriately changed according to the condition of the equipment. If the suction port is set downward, depending on the degree of separation of the water-insoluble cutting oil and the suction force of the pump, the liquid at the boundary between the water-insoluble cutting oil and the aqueous solution may be sucked. If the mouth is set upward, high-purity water-insoluble cutting oil can be reliably sucked. In the present invention, in order to separate the water-insoluble cutting oil and the other aqueous solution, it is easy to use the specific gravity difference between the two, but in addition to the method using the specific gravity difference, a water-repellent filter or a bubbling device is used. May be used. The water-repellent filter is a filter that allows only oil to pass through, and the bubbling device is
This device promotes separation of water and oil by blowing air.
【0005】また、本発明に係る切削油の回収供給方法
は、不水溶性切削油を使用する切削加工時に、水溶液を
加工箇所に供給すると共に、不水溶性切削油及び水溶液
を一の回収槽に回収貯留して、不水溶性切削油とその他
の水溶液を分離して、それぞれを切削加工時に再使用す
る方法であって、前記不水溶性切削油は、鉱物油と極性
の低い添加剤とで構成されており、前記鉱物油は、精製
度を高めて不飽和結合を極力抑えたものである。 [0005] A method for recovering and supplying cutting oil according to the present invention.
Is used during cutting using a water-insoluble cutting oil.
Water-insoluble cutting oil and aqueous solution supplied to the processing area
Is collected and stored in one collection tank, and water-insoluble cutting oil and other
Aqueous solutions are separated and reused during cutting.
Wherein the water-insoluble cutting oil comprises a mineral oil and a polar oil.
And the mineral oil is refined.
By increasing the degree, unsaturated bonds are suppressed as much as possible.
【0006】本発明のように、ポリアルファオレフィン
もしくは高度精製油を主成分とする不水溶性切削油を用
いると、水溶液との分離性において特に優れた効果を発
揮する。なお、本発明において高度精製油とは、芳香族
成分が4%未満、パラフィン成分が65%以上の精製油
を言う。このような不水溶性切削油を用いると、水溶液
を加工箇所に噴霧又は噴射しつつ不水溶性切削油を用い
て切削加工する場合において、不水溶性切削油とその他
の水溶液を一の回収槽にまとめて貯留しても、両者が迅
速に分離するのでそれぞれを高純度で再使用することが
できる。鉱物油と極性の低い添加剤とで構成した不水溶
性切削油は、一般に、水溶液との分離性に優れるが、本
発明者の研究によると、使用する鉱物油としては、芳香
族系成分が少ない方が良く、パラフィン系成分の多いも
の、中でも高度な溶剤処理や水素化処理により精製度を
高めて不飽和結合を極力抑えたものが良いことが明らか
となった。不飽和結合が無く不純物も殆どないものとし
ては、イソパラフィンやポリアルファオレフィンなどの
合成オイルがあるが、イソパラフィンは、高度精製油よ
り劣り、ポリアルファオレフィンは、非常に優れた分離
性が得られる。When a water-insoluble cutting oil containing polyalphaolefin or highly refined oil as a main component is used as in the present invention, a particularly excellent effect is exhibited in the separation property from an aqueous solution. In the present invention, the highly refined oil refers to a refined oil having an aromatic component of less than 4% and a paraffin component of 65% or more. When using such a water-insoluble cutting oil, when performing cutting using the water-insoluble cutting oil while spraying or spraying the aqueous solution to the processing location, the water-insoluble cutting oil and the other aqueous solution are collected into one collection tank. Even if they are collectively stored, they can be reused with high purity because they are quickly separated. A water-insoluble cutting oil composed of a mineral oil and a low-polarity additive generally has excellent separability from an aqueous solution, but according to the study of the present inventors, as a mineral oil to be used, an aromatic component is used. It was clarified that the smaller the better, the more the paraffinic component, and the better the degree of purification by high-level solvent treatment or hydrogenation treatment to suppress unsaturated bonds as much as possible. Synthetic oils such as isoparaffins and polyalphaolefins that have no unsaturated bonds and have few impurities are included, but isoparaffins are inferior to highly refined oils, and polyalphaolefins have very good separability.
【0007】[0007]
【発明の実施の形態】以下、実施例に基づいて、この発
明を更に詳細に説明する。図1〜図2は、不水溶性切削
油の吸い込み口を、油面LNに追従させる実施例を例示
している。図1について説明すると、回収タンクTに
は、水管1と油管2とが挿入されており、油管2とフロ
ートFとは、フレキシブルパイプ3を介して接続されて
いる。図2は、回収タンクTとサブタンクSとを用いる
実施例を図示したものであり、回収タンクTの不水溶性
切削油は、第1の油管2aを通してサブタンクSに伝え
られ、サブタンクSの不水溶性切削油は、第2の油管2
bを通して機器側に送られるようになっている。DESCRIPTION OF THE PREFERRED EMBODIMENTS Hereinafter, the present invention will be described in more detail based on embodiments. 1 and 2 exemplify an embodiment in which the suction port of the water-insoluble cutting oil follows the oil level LN. Referring to FIG. 1, a water pipe 1 and an oil pipe 2 are inserted into the collection tank T, and the oil pipe 2 and the float F are connected via a flexible pipe 3. FIG. 2 illustrates an embodiment in which the recovery tank T and the sub-tank S are used. The water-insoluble cutting oil in the recovery tank T is transmitted to the sub-tank S through the first oil pipe 2a. Cutting oil is supplied to the second oil pipe 2
b to the device side.
【0008】回収タンクTには、水管1が挿入されてお
り水溶液が機器側に送られるが、水管1に近接して緩衝
板4を設けられて液体の流動を阻止している。なお、サ
ブタンクSで満杯になった不水溶性切削油は、オーバー
フロー管5を通して回収タンクTに戻され、サブタンク
Sで分離された水溶液は、ドレン管6を通して回収タン
クTに戻されるようになっている。ところで、図1や図
2には表れていないが、フレキシブルパイプ3の吸い込
み口3aとフロートFとの間には、図3に略記するよう
な高さ調整機構4が設けられており、油面LNと吸い込
み口3aとの高度差hを適宜に調整できるようになって
いる。A water tube 1 is inserted into the recovery tank T, and an aqueous solution is sent to the equipment side. However, a buffer plate 4 is provided near the water tube 1 to prevent the liquid from flowing. The water-insoluble cutting oil filled in the sub tank S is returned to the collection tank T through the overflow pipe 5, and the aqueous solution separated in the sub tank S is returned to the collection tank T through the drain pipe 6. I have. By the way, although not shown in FIGS. 1 and 2, a height adjusting mechanism 4 as shown in FIG. 3 is provided between the suction port 3a of the flexible pipe 3 and the float F. The height difference h between the LN and the suction port 3a can be adjusted appropriately.
【0009】図4(a)と図4(b)とは、不水溶性切
削油とその他の水溶液を、より確実に分離させるために
撥水性フィルター7を用いた実施例を示している。撥水
性フィルター7は、油分は通過させるが、水分を通過さ
せないので、再使用する不水溶性切削油の純度を更に高
めることができる。図5は、サブタンクSにバブリング
装置8を設置した実施例を示している。バブリング装置
8は、細い穴を通してエアーが吹き出すように構成され
ており、油分と水分の分離が促進される。なお、図4や
図5に示す実施例でも、油の吸い込み口を上方を向ける
のが好ましい。FIGS. 4A and 4B show an embodiment in which a water-repellent filter 7 is used to more reliably separate a water-insoluble cutting oil and another aqueous solution. The water-repellent filter 7 allows oil to pass through but does not allow moisture to pass, so that the purity of the water-insoluble cutting oil to be reused can be further increased. FIG. 5 shows an embodiment in which the bubbling device 8 is installed in the sub tank S. The bubbling device 8 is configured such that air is blown out through a small hole, thereby promoting separation of oil and moisture. In the embodiment shown in FIGS. 4 and 5, it is preferable that the oil suction port is directed upward.
【0010】続いて、吸い込み方向を変化させた場合の
効果について説明する。実験内容としては、図6に示す
ように、60cm×30cm×45cmの水槽Tに底か
ら20cmまで水を入れ、その上に粘度10mm2/s の鉱
物油を水面から20cmまで入れた。これに、ポンプ
1,2を取り付け、揚水ポンプ1の吸い込み口をタンク
底から5cmの位置に、揚油ポンプ2の吸い込み口の位
置を油面から5cmの位置に設けた。揚油ポンプの吸い
込み口は、上向きと下向きの2通りとしその時の水分量
を比較すると表1の通りであった。なお、ポンプの流量
はそれぞれ、8〜10リットル/minであり、30分
運転、4時間運転、8時間運転した後で、油中の水分量
を計測した。Next, the effect when the suction direction is changed will be described. As shown in FIG. 6, water was poured into a water tank T of 60 cm × 30 cm × 45 cm up to 20 cm from the bottom, and a mineral oil having a viscosity of 10 mm 2 / s was poured on the water up to 20 cm from the water surface. Pumps 1 and 2 were attached thereto, and the suction port of the water pump 1 was provided at a position 5 cm from the tank bottom, and the suction port of the oil pump 2 was provided 5 cm from the oil level. Table 1 shows that the suction port of the oil pump was upward and downward, and the water content at that time was compared. The flow rates of the pumps were respectively 8 to 10 liter / min, and after operating for 30 minutes, 4 hours, and 8 hours, the amount of water in the oil was measured.
【0011】[0011]
【表1】 [Table 1]
【0012】次に、水分離性に特に優れる不水溶性切削
油についての確認データを説明する。実験内容として
は、500mlビーカーに鉱物油又は合成油を200m
lと水を200mlを入れ、台所用2軸ハンドミキサー
を使用して30秒撹拌し、停止してから時間毎の分離状
態を確認した。混合液の分離状態については、大半が油
である油層Aと、水と油が混ざり合った中間層Bと、水
の層Cに分けて観察し、油層Aと中間層Bの境界線L1
と、中間層Bと水の層Cの境界線L2とを判定した。そ
の結果は表2に示す通りであり、L1の位置が低いほ
ど、L2の位置が高いほど、両者L1,L2の位置が近
いほど分離が速い事になる。油は、粘度を9〜11に調
整し、水は水道水を使用した。なお、初期状態では、油
面が底面から75mmの位置、油と水の境界面が底面か
ら40mmの位置であった。Next, the confirmation data of the water-insoluble cutting oil which is particularly excellent in the water separating property will be described. The content of the experiment was as follows: mineral oil or synthetic oil 200m in a 500ml beaker
l and 200 ml of water were added, and the mixture was stirred for 30 seconds using a two-shaft hand mixer for kitchen. Regarding the separation state of the mixed liquid, the oil layer A, which is mostly oil, the intermediate layer B in which water and oil are mixed, and the water layer C are separately observed, and the boundary line L1 between the oil layer A and the intermediate layer B is observed.
And the boundary line L2 between the intermediate layer B and the water layer C were determined. The results are as shown in Table 2. The lower the position of L1, the higher the position of L2, and the closer the positions of L1 and L2, the faster the separation. For oil, the viscosity was adjusted to 9 to 11, and tap water was used as water. In the initial state, the oil level was 75 mm from the bottom surface, and the boundary between oil and water was 40 mm from the bottom surface.
【0013】[0013]
【表2】 [Table 2]
【0014】表2に示す通り、一般に、芳香族系成分が
少ないものの方が、また、パラフィン系成分の多いもの
の方が水分離性に優れている。特に、ポリアルファオレ
フィンや芳香族成分を抑えた高度精製油が水分離性に優
れている。なお、芳香族成分がやや多いニュートラル油
(通称)は、一見、水分離性に優れているが、1時間後
でも濁った状態が改善されず、比重差によって純度を高
めることは困難であった。As shown in Table 2, in general, those having less aromatic components and those having more paraffin components have better water separation properties. In particular, polyalphaolefins and highly refined oils containing less aromatic components have excellent water separation properties. It should be noted that neutral oil (commonly known) having a relatively large amount of aromatic components is apparently excellent in water separation properties, but the turbid state was not improved even after 1 hour, and it was difficult to increase the purity due to a difference in specific gravity. .
【0015】[0015]
【発明の効果】以上説明したように、本発明によれば、
不水溶性切削油とその他の水溶液の分離性を更に改善
し、再使用する不水溶性切削油の純度を高めることがで
きる。As described above, according to the present invention,
The separation property of the water-insoluble cutting oil and other aqueous solutions can be further improved, and the purity of the water-insoluble cutting oil to be reused can be increased.
【図1】フロートを用いて吸い込み口を昇降させる実施
例を図示したものである。FIG. 1 illustrates an embodiment in which a suction port is moved up and down using a float.
【図2】サブタンクを用いると共に、フロートによって
吸い込み口を昇降させる実施例を図示したものである。FIG. 2 shows an embodiment in which a sub tank is used and a suction port is moved up and down by a float.
【図3】高さ調整機構を略記したものである。FIG. 3 schematically shows a height adjusting mechanism.
【図4】撥水性フィルターを用いる実施例を図示したも
のである。FIG. 4 illustrates an embodiment using a water-repellent filter.
【図5】バブリング装置を用いる実施例を図示したもの
である。FIG. 5 illustrates an embodiment using a bubbling device.
【図6】吸い込み口の向きを変えた場合の対比実験を説
明する図面である。FIG. 6 is a diagram illustrating a comparison experiment when the direction of the suction port is changed.
フロントページの続き (56)参考文献 特開 平6−304841(JP,A) 特開 平7−155504(JP,A) 特開 平7−60600(JP,A) 特開 平6−313182(JP,A) 特開 昭52−114602(JP,A) 実開 平3−55142(JP,U) 特公 平3−183(JP,B2) (58)調査した分野(Int.Cl.7,DB名) B23Q 11/10 B01D 17/00 503 C10M 101/00 - 177/00 Continuation of front page (56) References JP-A-6-304841 (JP, A) JP-A-7-155504 (JP, A) JP-A-7-60600 (JP, A) JP-A-6-313182 (JP) JP-A-52-114602 (JP, A) JP-A-3-55142 (JP, U) JP-B 3-183 (JP, B2) (58) Fields investigated (Int. Cl. 7 , DB Name) B23Q 11/10 B01D 17/00 503 C10M 101/00-177/00
Claims (4)
製油を主成分とする不水溶性切削油を使用する切削加工
時に、水溶液を加工箇所に供給すると共に、不水溶性切削油及び水溶液 を一の回収槽に回収貯留し
て、不水溶性切削油とその他の水溶液を分離して、それ
ぞれを切削加工時に再使用する方法であって、 前記不水溶性切削油の吸い込み口を上向きに設定して油
面に合わせて上下させるようにした切削油の回収供給方
法。(1) a polyalphaolefin or a highly refined
Oil during cutting using a water-insoluble cutting oil machining mainly composed of, with supplying solution to the machining spot, and capture and storage on one collection tank of the water-insoluble cutting oil and aqueous, water-insoluble cutting oil and separating the other aqueous solution, a method of reusing each during cutting, the cutting oil so as to vertically fit said upwardly set the suction opening of the water-insoluble cutting oil to the oil surface Collection and supply method.
に、水溶液を加工箇所に供給すると共に、不水溶性切削油及び水溶液を一の回収槽に回収貯留し
て、不水溶性切削油とその他の水溶液を分離して、それ
ぞれを切削加工時に再使用する方法であって 、前記不水溶性切削油は、鉱物油と極性の低い添加剤とで
構成されており、前記鉱物油は、精製度を高めて不飽和
結合を極力抑えたものである切削油の回収供給方法。 2. A cutting process using a water-insoluble cutting oil.
At the same time, supply the aqueous solution to the processing location and collect and store the water-insoluble cutting oil and aqueous solution in one collection tank.
Water-insoluble cutting oil and other aqueous solutions
A method of reusing each of them at the time of cutting , wherein the water-insoluble cutting oil comprises mineral oil and a low-polarity additive.
The mineral oil is unsaturated and enhances the degree of refining.
A cutting oil recovery and supply method that minimizes coupling.
リアルファオレフィンである請求項2に記載の切削油の
回収供給方法。3. The mineral oil according to claim 1, wherein said mineral oil is isoparaffin or polyparaffin.
3. The cutting oil according to claim 2, which is a re-alpha olefin.
Collection and supply method .
に、水溶液を加工箇所に供給すると共に、不水溶性切削油及び水溶液を一の回収槽に回収貯留し
て、不水溶性切削油とその他の水溶液を分離して、それ
ぞれを切削加工時に再使用する方法に用いられる、ポリ
アルファオレフィンもしくは高度精製油を主成分とする
不水溶性切削油 。4. A cutting process using a water-insoluble cutting oil.
At the same time, supply the aqueous solution to the processing location and collect and store the water-insoluble cutting oil and aqueous solution in one collection tank.
Water-insoluble cutting oil and other aqueous solutions
These are used for the method of reusing each of them during cutting.
Mainly composed of alpha olefin or highly refined oil
Water-insoluble cutting oil .
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP20057398A JP3124518B2 (en) | 1998-07-15 | 1998-07-15 | Cutting oil supply and recovery method and cutting oil |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP20057398A JP3124518B2 (en) | 1998-07-15 | 1998-07-15 | Cutting oil supply and recovery method and cutting oil |
Publications (2)
Publication Number | Publication Date |
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JP2000024873A JP2000024873A (en) | 2000-01-25 |
JP3124518B2 true JP3124518B2 (en) | 2001-01-15 |
Family
ID=16426590
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Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP20057398A Expired - Lifetime JP3124518B2 (en) | 1998-07-15 | 1998-07-15 | Cutting oil supply and recovery method and cutting oil |
Country Status (1)
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JP (1) | JP3124518B2 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8671652B2 (en) | 2003-02-14 | 2014-03-18 | Eastman Chemical Company | Packages, packaging systems, methods for packaging and apparatus for packaging |
-
1998
- 1998-07-15 JP JP20057398A patent/JP3124518B2/en not_active Expired - Lifetime
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8671652B2 (en) | 2003-02-14 | 2014-03-18 | Eastman Chemical Company | Packages, packaging systems, methods for packaging and apparatus for packaging |
Also Published As
Publication number | Publication date |
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JP2000024873A (en) | 2000-01-25 |
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