JP2021518473A - 潤滑剤組成物 - Google Patents
潤滑剤組成物 Download PDFInfo
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- JP2021518473A JP2021518473A JP2020550802A JP2020550802A JP2021518473A JP 2021518473 A JP2021518473 A JP 2021518473A JP 2020550802 A JP2020550802 A JP 2020550802A JP 2020550802 A JP2020550802 A JP 2020550802A JP 2021518473 A JP2021518473 A JP 2021518473A
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- 239000000203 mixture Substances 0.000 title claims abstract description 125
- 239000000314 lubricant Substances 0.000 title claims abstract description 71
- 239000000654 additive Substances 0.000 claims abstract description 74
- 229910052717 sulfur Inorganic materials 0.000 claims abstract description 69
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims abstract description 68
- 239000011593 sulfur Substances 0.000 claims abstract description 67
- 239000002199 base oil Substances 0.000 claims abstract description 64
- DMBHHRLKUKUOEG-UHFFFAOYSA-N diphenylamine Chemical compound C=1C=CC=CC=1NC1=CC=CC=C1 DMBHHRLKUKUOEG-UHFFFAOYSA-N 0.000 claims abstract description 56
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 54
- 230000000996 additive effect Effects 0.000 claims abstract description 37
- XQVWYOYUZDUNRW-UHFFFAOYSA-N N-Phenyl-1-naphthylamine Chemical compound C=1C=CC2=CC=CC=C2C=1NC1=CC=CC=C1 XQVWYOYUZDUNRW-UHFFFAOYSA-N 0.000 claims abstract description 29
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 19
- 230000001590 oxidative effect Effects 0.000 claims abstract description 9
- -1 t-octyl Chemical group 0.000 claims description 92
- 239000003921 oil Substances 0.000 claims description 51
- 235000019198 oils Nutrition 0.000 claims description 51
- 150000002148 esters Chemical class 0.000 claims description 49
- 238000000034 method Methods 0.000 claims description 38
- 125000000217 alkyl group Chemical group 0.000 claims description 31
- 239000002253 acid Substances 0.000 claims description 23
- 229910052799 carbon Inorganic materials 0.000 claims description 19
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims description 19
- 229920013639 polyalphaolefin Polymers 0.000 claims description 18
- 229910052739 hydrogen Inorganic materials 0.000 claims description 16
- 229910052751 metal Inorganic materials 0.000 claims description 15
- 239000002184 metal Substances 0.000 claims description 15
- 125000003342 alkenyl group Chemical group 0.000 claims description 14
- CXYRUNPLKGGUJF-OZVSTBQFSA-M pamine Chemical compound [Br-].C1([C@@H](CO)C(=O)OC2C[C@@H]3[N+]([C@H](C2)[C@@H]2[C@H]3O2)(C)C)=CC=CC=C1 CXYRUNPLKGGUJF-OZVSTBQFSA-M 0.000 claims description 14
- 150000001875 compounds Chemical class 0.000 claims description 13
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims description 12
- 230000001050 lubricating effect Effects 0.000 claims description 12
- 239000010687 lubricating oil Substances 0.000 claims description 11
- 125000000304 alkynyl group Chemical group 0.000 claims description 9
- 239000005077 polysulfide Substances 0.000 claims description 9
- 229920001021 polysulfide Polymers 0.000 claims description 9
- 150000008117 polysulfides Polymers 0.000 claims description 9
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 8
- 125000003118 aryl group Chemical group 0.000 claims description 8
- 239000003085 diluting agent Substances 0.000 claims description 8
- 229910052725 zinc Inorganic materials 0.000 claims description 8
- 239000011701 zinc Substances 0.000 claims description 8
- 125000001400 nonyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 7
- 239000007800 oxidant agent Substances 0.000 claims description 7
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 claims description 7
- 239000003607 modifier Substances 0.000 claims description 6
- 230000003449 preventive effect Effects 0.000 claims description 6
- 125000003545 alkoxy group Chemical group 0.000 claims description 5
- 125000003282 alkyl amino group Chemical group 0.000 claims description 5
- 125000004414 alkyl thio group Chemical group 0.000 claims description 5
- 239000012141 concentrate Substances 0.000 claims description 5
- 125000004663 dialkyl amino group Chemical group 0.000 claims description 5
- 239000002270 dispersing agent Substances 0.000 claims description 4
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 4
- 150000003839 salts Chemical class 0.000 claims description 4
- RYYWUUFWQRZTIU-UHFFFAOYSA-K thiophosphate Chemical compound [O-]P([O-])([O-])=S RYYWUUFWQRZTIU-UHFFFAOYSA-K 0.000 claims description 4
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 4
- 239000008158 vegetable oil Substances 0.000 claims description 4
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 claims description 3
- 239000007983 Tris buffer Substances 0.000 claims description 3
- 125000005037 alkyl phenyl group Chemical group 0.000 claims description 3
- IKXFIBBKEARMLL-UHFFFAOYSA-N triphenoxy(sulfanylidene)-$l^{5}-phosphane Chemical compound C=1C=CC=CC=1OP(OC=1C=CC=CC=1)(=S)OC1=CC=CC=C1 IKXFIBBKEARMLL-UHFFFAOYSA-N 0.000 claims description 3
- BIGYLAKFCGVRAN-UHFFFAOYSA-N 1,3,4-thiadiazolidine-2,5-dithione Chemical class S=C1NNC(=S)S1 BIGYLAKFCGVRAN-UHFFFAOYSA-N 0.000 claims description 2
- YXIWHUQXZSMYRE-UHFFFAOYSA-N 1,3-benzothiazole-2-thiol Chemical class C1=CC=C2SC(S)=NC2=C1 YXIWHUQXZSMYRE-UHFFFAOYSA-N 0.000 claims description 2
- RPLXHDXNCZNHRA-UHFFFAOYSA-N 2,6-bis(dodecylsulfanylmethyl)-4-nonylphenol Chemical compound CCCCCCCCCCCCSCC1=CC(CCCCCCCCC)=CC(CSCCCCCCCCCCCC)=C1O RPLXHDXNCZNHRA-UHFFFAOYSA-N 0.000 claims description 2
- UDFARPRXWMDFQU-UHFFFAOYSA-N 2,6-ditert-butyl-4-[(3,5-ditert-butyl-4-hydroxyphenyl)methylsulfanylmethyl]phenol Chemical compound CC(C)(C)C1=C(O)C(C(C)(C)C)=CC(CSCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)=C1 UDFARPRXWMDFQU-UHFFFAOYSA-N 0.000 claims description 2
- LBOGPIWNHXHYHN-UHFFFAOYSA-N 2-(2-hydroxy-5-octylphenyl)sulfanyl-4-octylphenol Chemical compound CCCCCCCCC1=CC=C(O)C(SC=2C(=CC=C(CCCCCCCC)C=2)O)=C1 LBOGPIWNHXHYHN-UHFFFAOYSA-N 0.000 claims description 2
- QLMGIWHWWWXXME-UHFFFAOYSA-N 2-(3,5-ditert-butyl-4-hydroxyphenyl)acetic acid Chemical compound CC(C)(C)C1=CC(CC(O)=O)=CC(C(C)(C)C)=C1O QLMGIWHWWWXXME-UHFFFAOYSA-N 0.000 claims description 2
- KXPXKNBDCUOENF-UHFFFAOYSA-N 2-(Octylthio)ethanol Chemical compound CCCCCCCCSCCO KXPXKNBDCUOENF-UHFFFAOYSA-N 0.000 claims description 2
- GAODDBNJCKQQDY-UHFFFAOYSA-N 2-methyl-4,6-bis(octylsulfanylmethyl)phenol Chemical compound CCCCCCCCSCC1=CC(C)=C(O)C(CSCCCCCCCC)=C1 GAODDBNJCKQQDY-UHFFFAOYSA-N 0.000 claims description 2
- ZYJXQDCMXTWHIV-UHFFFAOYSA-N 2-tert-butyl-4,6-bis(octylsulfanylmethyl)phenol Chemical compound CCCCCCCCSCC1=CC(CSCCCCCCCC)=C(O)C(C(C)(C)C)=C1 ZYJXQDCMXTWHIV-UHFFFAOYSA-N 0.000 claims description 2
- YFHKLSPMRRWLKI-UHFFFAOYSA-N 2-tert-butyl-4-(3-tert-butyl-4-hydroxy-5-methylphenyl)sulfanyl-6-methylphenol Chemical compound CC(C)(C)C1=C(O)C(C)=CC(SC=2C=C(C(O)=C(C)C=2)C(C)(C)C)=C1 YFHKLSPMRRWLKI-UHFFFAOYSA-N 0.000 claims description 2
- HXIQYSLFEXIOAV-UHFFFAOYSA-N 2-tert-butyl-4-(5-tert-butyl-4-hydroxy-2-methylphenyl)sulfanyl-5-methylphenol Chemical compound CC1=CC(O)=C(C(C)(C)C)C=C1SC1=CC(C(C)(C)C)=C(O)C=C1C HXIQYSLFEXIOAV-UHFFFAOYSA-N 0.000 claims description 2
- MQWCQFCZUNBTCM-UHFFFAOYSA-N 2-tert-butyl-6-(3-tert-butyl-2-hydroxy-5-methylphenyl)sulfanyl-4-methylphenol Chemical compound CC(C)(C)C1=CC(C)=CC(SC=2C(=C(C=C(C)C=2)C(C)(C)C)O)=C1O MQWCQFCZUNBTCM-UHFFFAOYSA-N 0.000 claims description 2
- DBHUTHZPCWZNRW-UHFFFAOYSA-N 3-(3,5-dicyclohexyl-4-hydroxyphenyl)propanoic acid Chemical compound OC=1C(C2CCCCC2)=CC(CCC(=O)O)=CC=1C1CCCCC1 DBHUTHZPCWZNRW-UHFFFAOYSA-N 0.000 claims description 2
- WPMYUUITDBHVQZ-UHFFFAOYSA-N 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoic acid Chemical compound CC(C)(C)C1=CC(CCC(O)=O)=CC(C(C)(C)C)=C1O WPMYUUITDBHVQZ-UHFFFAOYSA-N 0.000 claims description 2
- BCZQMWDTKGBZFG-UHFFFAOYSA-N 4-[(4-hydroxy-2,6-dimethylphenyl)disulfanyl]-3,5-dimethylphenol Chemical compound CC1=CC(O)=CC(C)=C1SSC1=C(C)C=C(O)C=C1C BCZQMWDTKGBZFG-UHFFFAOYSA-N 0.000 claims description 2
- QVXGXGJJEDTQSU-UHFFFAOYSA-N 4-[4-hydroxy-2,5-di(pentan-2-yl)phenyl]sulfanyl-2,5-di(pentan-2-yl)phenol Chemical compound C1=C(O)C(C(C)CCC)=CC(SC=2C(=CC(O)=C(C(C)CCC)C=2)C(C)CCC)=C1C(C)CCC QVXGXGJJEDTQSU-UHFFFAOYSA-N 0.000 claims description 2
- VJMAITQRABEEKP-UHFFFAOYSA-N [6-(phenylmethoxymethyl)-1,4-dioxan-2-yl]methyl acetate Chemical compound O1C(COC(=O)C)COCC1COCC1=CC=CC=C1 VJMAITQRABEEKP-UHFFFAOYSA-N 0.000 claims description 2
- XYRMLECORMNZEY-UHFFFAOYSA-B [Mo+4].[Mo+4].[Mo+4].[O-]P([O-])([S-])=S.[O-]P([O-])([S-])=S.[O-]P([O-])([S-])=S.[O-]P([O-])([S-])=S Chemical compound [Mo+4].[Mo+4].[Mo+4].[O-]P([O-])([S-])=S.[O-]P([O-])([S-])=S.[O-]P([O-])([S-])=S.[O-]P([O-])([S-])=S XYRMLECORMNZEY-UHFFFAOYSA-B 0.000 claims description 2
- 239000005078 molybdenum compound Substances 0.000 claims description 2
- 150000002752 molybdenum compounds Chemical class 0.000 claims description 2
- CWQXQMHSOZUFJS-UHFFFAOYSA-N molybdenum disulfide Chemical compound S=[Mo]=S CWQXQMHSOZUFJS-UHFFFAOYSA-N 0.000 claims description 2
- 229910052982 molybdenum disulfide Inorganic materials 0.000 claims description 2
- KHYKFSXXGRUKRE-UHFFFAOYSA-J molybdenum(4+) tetracarbamodithioate Chemical compound C(N)([S-])=S.[Mo+4].C(N)([S-])=S.C(N)([S-])=S.C(N)([S-])=S KHYKFSXXGRUKRE-UHFFFAOYSA-J 0.000 claims description 2
- 239000003960 organic solvent Substances 0.000 claims description 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 2
- 229920001515 polyalkylene glycol Polymers 0.000 claims description 2
- HVGINUIPKBCAQD-UHFFFAOYSA-N trihydroxy-[[3-(2-methylpropyl)-2-phenylphenyl]-phenyl-lambda4-sulfanylidene]-lambda5-phosphane Chemical compound CC(C)CC1=C(C(=CC=C1)S(=P(O)(O)O)C2=CC=CC=C2)C3=CC=CC=C3 HVGINUIPKBCAQD-UHFFFAOYSA-N 0.000 claims description 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 claims 2
- KEXRSLVRFLEMHJ-UHFFFAOYSA-N 1-o,4-o-bis[(4-tert-butyl-3-hydroxy-2,6-dimethylphenyl)methyl] benzene-1,4-dicarbothioate Chemical compound CC1=CC(C(C)(C)C)=C(O)C(C)=C1COC(=S)C1=CC=C(C(=S)OCC=2C(=C(O)C(=CC=2C)C(C)(C)C)C)C=C1 KEXRSLVRFLEMHJ-UHFFFAOYSA-N 0.000 claims 1
- NCWTZPKMFNRUAK-UHFFFAOYSA-N 2-ethyl-4,6-bis(octylsulfanylmethyl)phenol Chemical compound CCCCCCCCSCC1=CC(CC)=C(O)C(CSCCCCCCCC)=C1 NCWTZPKMFNRUAK-UHFFFAOYSA-N 0.000 claims 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims 1
- MAOGTIAUZWTWSQ-UHFFFAOYSA-N [(2,3-diphenylphenyl)-nonyl-lambda4-sulfanylidene]-trihydroxy-lambda5-phosphane Chemical compound CCCCCCCCCS(=P(O)(O)O)C1=CC=CC(=C1C2=CC=CC=C2)C3=CC=CC=C3 MAOGTIAUZWTWSQ-UHFFFAOYSA-N 0.000 claims 1
- JDOHKUJYBKIYSN-UHFFFAOYSA-N dodecan-1-amine;3-hydroxy-1,3$l^{5}-thiaphosphetane 3-oxide Chemical compound OP1(=O)CSC1.CCCCCCCCCCCCN JDOHKUJYBKIYSN-UHFFFAOYSA-N 0.000 claims 1
- JVVNYJRBHYLUNQ-UHFFFAOYSA-N ethyl 5-carbamothioylsulfanylnonanoate Chemical compound CCCCC(SC(N)=S)CCCC(=O)OCC JVVNYJRBHYLUNQ-UHFFFAOYSA-N 0.000 claims 1
- 235000019260 propionic acid Nutrition 0.000 claims 1
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 claims 1
- YODZTKMDCQEPHD-UHFFFAOYSA-N thiodiglycol Chemical compound OCCSCCO YODZTKMDCQEPHD-UHFFFAOYSA-N 0.000 claims 1
- 239000000463 material Substances 0.000 abstract description 24
- 230000009972 noncorrosive effect Effects 0.000 abstract description 3
- 238000010586 diagram Methods 0.000 abstract 1
- 241000894007 species Species 0.000 description 48
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- 150000001336 alkenes Chemical class 0.000 description 28
- 150000005690 diesters Chemical class 0.000 description 28
- 150000005691 triesters Chemical class 0.000 description 25
- 125000004432 carbon atom Chemical group C* 0.000 description 20
- 229930195733 hydrocarbon Natural products 0.000 description 19
- 150000002430 hydrocarbons Chemical class 0.000 description 19
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 18
- 239000003054 catalyst Substances 0.000 description 16
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- 238000005260 corrosion Methods 0.000 description 13
- 230000008569 process Effects 0.000 description 13
- VHYFNPMBLIVWCW-UHFFFAOYSA-N 4-Dimethylaminopyridine Chemical compound CN(C)C1=CC=NC=C1 VHYFNPMBLIVWCW-UHFFFAOYSA-N 0.000 description 12
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 12
- 239000003795 chemical substances by application Substances 0.000 description 12
- 239000004215 Carbon black (E152) Substances 0.000 description 11
- 150000002009 diols Chemical class 0.000 description 11
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
- 229910001868 water Inorganic materials 0.000 description 11
- 239000004711 α-olefin Substances 0.000 description 11
- 125000001183 hydrocarbyl group Chemical group 0.000 description 10
- 229920005862 polyol Polymers 0.000 description 10
- 125000004434 sulfur atom Chemical group 0.000 description 10
- 230000007797 corrosion Effects 0.000 description 9
- 239000003112 inhibitor Substances 0.000 description 9
- 239000007788 liquid Substances 0.000 description 9
- 230000003647 oxidation Effects 0.000 description 9
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- 238000012360 testing method Methods 0.000 description 9
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
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- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 8
- 150000001266 acyl halides Chemical class 0.000 description 8
- 150000001491 aromatic compounds Chemical class 0.000 description 8
- 150000001735 carboxylic acids Chemical class 0.000 description 8
- 230000032050 esterification Effects 0.000 description 8
- 238000005886 esterification reaction Methods 0.000 description 8
- 229940059574 pentaerithrityl Drugs 0.000 description 8
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 8
- 239000000047 product Substances 0.000 description 8
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- AFFLGGQVNFXPEV-UHFFFAOYSA-N 1-decene Chemical compound CCCCCCCCC=C AFFLGGQVNFXPEV-UHFFFAOYSA-N 0.000 description 4
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- 238000005727 Friedel-Crafts reaction Methods 0.000 description 4
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- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 4
- 150000001298 alcohols Chemical class 0.000 description 4
- WTEOIRVLGSZEPR-UHFFFAOYSA-N boron trifluoride Chemical compound FB(F)F WTEOIRVLGSZEPR-UHFFFAOYSA-N 0.000 description 4
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- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- 239000003930 superacid Substances 0.000 description 1
- 229940042055 systemic antimycotics triazole derivative Drugs 0.000 description 1
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
- 229940095068 tetradecene Drugs 0.000 description 1
- 125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- 239000011135 tin Substances 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 239000013638 trimer Substances 0.000 description 1
- 125000004417 unsaturated alkyl group Chemical group 0.000 description 1
- 239000004034 viscosity adjusting agent Substances 0.000 description 1
- 239000003039 volatile agent Substances 0.000 description 1
- 239000007762 w/o emulsion Substances 0.000 description 1
- 238000004018 waxing Methods 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
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Abstract
Description
基油、又は潤滑性基油若しくはベースストックは、完成した完全に配合された潤滑油の重量で最大の成分である。
Rは、H、C1〜C18アルキル、C2〜C18アルケニル、C2〜C18アルキニル、-C(O)C1〜C18アルキル又は-C(O)アリールであり、及び
R1、R2、R3及びR4は、それぞれ独立して、H、C1〜C18アルキル、C1〜C18アルコキシ、C1〜C18アルキルアミノ、C1〜C18ジアルキルアミノ、C1〜C18アルキルチオ、C2〜C18アルケニル、C2〜C18アルキニル又はC7〜C21アラルキルである]。
R1及びR2は、それぞれ独立して、H又はC1〜C18アルキルである]。特定の実施形態では、R2は、Hであり、R1は、分岐鎖C4〜C12アルキル、例えば、t-ブチル、t-オクチル又は分岐ノニルである。
Rは、H、C1〜C18アルキル、C2〜C18アルケニル、C2〜C18アルキニル、-C(O)C1〜C18アルキル又は-C(O)アリールであり、及び
R1、R2、R3及びR4は、それぞれ独立して、H、C1〜C18アルキル、C1〜C18アルコキシ、C1〜C18アルキルアミノ、C1〜C18ジアルキルアミノ、C1〜C18アルキルチオ、C2〜C18アルケニル、C2〜C18アルキニル又はC7〜C21アラルキルである]。
配合物A〜Fを提供するために、タービン基油を、以下に概説するように添加剤と一緒に配合する。添加剤の量は、配合物の総重量に基づいて、重量ppm(百万分率)である。総重量の残部は、群III基油である。配合物B、D及びFは本発明である。配合物A、C及びEは比較である。PANAは、アルキル化N-α-ナフチル-N-フェニルアミン酸化防止剤である。DPAは、アルキル化ジフェニルアミン酸化防止剤である。硫黄添加剤は、ジ-tert-アルキルポリスルフィドである。腐食防止剤A及びBは、それぞれ、アルケニルコハク酸ハーフエステル+アミンリン酸塩及びカルボン酸+アミンリン酸塩である。金属不活性化剤は、トリアゾール誘導体である。希釈剤は、グリコールタイプの希釈剤である。
配合物A〜Eを提供するために、タービン基油を、以下に概説するように添加剤と一緒に配合する。添加剤の量は、配合物の総重量に基づいて、重量ppm(百万分率)である。総重量の残部は、群III基油である。配合物A〜Dは本発明である。配合物Eは比較である。
Claims (30)
- 基油、
N-α-ナフチル-N-フェニルアミン酸化防止剤及びジフェニルアミン酸化防止剤からなる群から選択される1つ以上の酸化防止剤; 及び
1つ以上の硫黄含有添加剤
を含む、潤滑剤組成物。 - N-α-ナフチル-N-フェニルアミン酸化防止剤及びジフェニルアミン酸化防止剤が、合計で、潤滑剤組成物の総重量に基づいて、約0.2wt%〜約0.8wt%存在する、請求項1に記載の潤滑剤組成物。
- 硫黄含有添加剤によって提供される硫黄濃度が、合計で、潤滑剤組成物の総重量に基づいて、約50重量ppm〜約1000重量ppmの範囲である、請求項1又は2に記載の潤滑剤組成物。
- N-α-ナフチル-N-フェニルアミン酸化防止剤が、式
Rは、H、C1〜C18アルキル、C2〜C18アルケニル、C2〜C18アルキニル、-C(O)C1〜C18アルキル又は-C(O)アリールであり、及び
R1、R2、R3及びR4は、それぞれ独立して、H、C1〜C18アルキル、C1〜C18アルコキシ、C1〜C18アルキルアミノ、C1〜C18ジアルキルアミノ、C1〜C18アルキルチオ、C2〜C18アルケニル、C2〜C18アルキニル又はC7〜C21アラルキルである]
のものであり; 及び
ジフェニルアミン酸化防止剤が、式
Rは、H、C1〜C18アルキル、C2〜C18アルケニル、C2〜C18アルキニル、-C(O)C1〜C18アルキル又は-C(O)アリールであり、及び
R1、R2、R3及びR4は、それぞれ独立して、H、C1〜C18アルキル、C1〜C18アルコキシ、C1〜C18アルキルアミノ、C1〜C18ジアルキルアミノ、C1〜C18アルキルチオ、C2〜C18アルケニル、C2〜C18アルキニル又はC7〜C21アラルキルである]
のものである、請求項1〜3のいずれか一項に記載の潤滑剤組成物。 - 硫黄含有添加剤が、硫黄含有ヒンダードフェノール系化合物、硫黄含有防錆剤、硫黄含有摩擦調整剤、及び硫黄含有耐摩耗添加剤からなる群から選択される、請求項1〜6のいずれか一項に記載の潤滑剤組成物。
- 2,4-ジ-オクチルチオメチル-6-tert-ブチルフェノール、2,4-ジ-オクチルチオメチル-6-メチルフェノール、2,4-ジ-オクチルチオメチル-6-エチルフェノール又は2,6-ジ-ドデシルチオメチル-4-ノニルフェノール、2,2'-チオビス(6-tert-ブチル-4-メチルフェノール)、2,2'-チオビス(4-オクチルフェノール)、4,4'-チオビス(6-tert-ブチル-3-メチルフェノール)、4,4'-チオビス-(6-tert-ブチル-2-メチルフェノール)、4,4'-チオビス(3,6-ジ-sec-アミルフェノール)、4,4'-ビス(2,6-ジメチル-4-ヒドロキシフェニル)ジスルフィド、オクタデシル4-ヒドロキシ-3,5-ジメチルベンジルメルカプトアセテート、トリデシル4-ヒドロキシ-3,5-ジ-tert-ブチルベンジルメルカプトアセテート、ビス(4-tert-ブチル-3-ヒドロキシ-2,6-ジメチルベンジル)ジチオテレフタレート、ビス(3,5-ジ-tert-ブチル-4-ヒドロキシベンジル)スルフィド、イソオクチル3,5-ジ-tert-ブチル-4-ヒドロキシ-ベンジルメルカプトアセテート、並びにβ-(3,5-ジ-tert-ブチル-4-ヒドロキシフェニル)プロピオン酸、β-(5-tert-ブチル-4-ヒドロキシ-3-メチルフェニル)プロピオン酸、β-(3,5-ジシクロヘキシル-4-ヒドロキシフェニル)-プロピオン酸、3,5-ジ-tert-ブチル-4-ヒドロキシフェニル酢酸若しくはβ-(5-tert-ブチル-4-ヒドロキシフェニル)-3-チア酪酸と、チオジエチレングリコール、3-チアウンデカノール若しくはチアペンタデカノールとのエステルからなる群から選択される1つ以上の硫黄含有添加剤を含む、請求項1〜7のいずれか一項に記載の潤滑剤組成物。
- 有機モリブデンジチオカルバメート、有機モリブデンジチオホスフェート、並びに分散剤及び二硫化モリブデンに基づく有機モリブデン化合物からなる群から選択される1つ以上の硫黄含有添加剤を含む、請求項1〜8のいずれか一項に記載の潤滑剤組成物。
- 硫化オレフィン、硫化植物油、ジアルキルジチオホスフェートエステル、ジアルキルジチオリン酸亜鉛、アルキル又はアリールジ-及びトリ-スルフィド、2,5-ジメルカプト-1,3,4-チアジアゾールの誘導体、エチル(ビスイソプロピルオキシホスフィノチオイル)-チオプロピオネート、トリフェニルチオホスフェート、トリス(アルキルフェニル)ホスホロチオエート、ジフェニルモノノニルフェニルホスホロチオエート、イソブチルフェニルジフェニルホスホロチオエート、3-ヒドロキシ-1,3-チアホスフェタン3-オキシドのドデシルアミン塩、トリチオリン酸5,5,5-トリス-イソオクチル2-アセテート、2-メルカプトベンゾチアゾールの誘導体、エトキシカルボニル5-オクチルジチオカルバメート及びジヒドロカルビルジチオホスフェート金属塩からなる群から選択される1つ以上の硫黄含有添加剤を含む、請求項1〜9のいずれか一項に記載の潤滑剤組成物。
- 硫化オレフィンからなる群から選択される1つ以上の硫黄含有添加剤を含む、請求項1〜10のいずれか一項に記載の潤滑剤組成物。
- 硫化イソブチレンからなる群から選択される1つ以上の硫黄含有添加剤を含む、請求項1〜11のいずれか一項に記載の潤滑剤組成物。
- ジ-tert-アルキルポリスルフィドからなる群から選択される1つ以上の硫黄含有添加剤を含む、請求項1〜12のいずれか一項に記載の潤滑剤組成物。
- ジ-tert-ブチルポリスルフィド、ジ-tert-ドデシルポリスルフィド及びジ-tert-ノニルポリスルフィドからなる群から選択される1つ以上の硫黄含有添加剤を含む、請求項1〜13のいずれか一項に記載の潤滑剤組成物。
- 群II、群III及び群IVの基油からなる群から選択される基油を含む、請求項1〜14のいずれか一項に記載の潤滑剤組成物。
- ポリアルファオレフィンからなる群から選択される基油を含む、請求項1〜15のいずれか一項に記載の潤滑剤組成物。
- 合成エステルからなる群から選択される基油を含む、請求項1〜16のいずれか一項に記載の潤滑剤組成物。
- 基油が、1つ以上のポリアルファオレフィン及び1つ以上の合成エステルを含む、請求項1〜17のいずれか一項に記載の潤滑剤組成物。
- 基油が、1つ以上のポリアルキレングリコールを含む、請求項1〜18のいずれか一項に記載の潤滑剤組成物。
- 1つ以上のN-α-ナフチル-N-フェニルアミン酸化防止剤及び1つ以上のジフェニルアミン酸化防止剤を含み、N-α-ナフチル-N-フェニルアミン酸化防止剤とジフェニルアミン酸化防止剤との重量/重量比は、約1/9〜約9/1である、請求項1〜19のいずれか一項に記載の潤滑剤組成物。
- 基油が、潤滑剤組成物の総重量に基づいて、約80wt%〜約99.7wt%存在する、請求項1〜20のいずれか一項に記載の潤滑剤組成物。
- ジアルキルジチオリン酸亜鉛を実質的に含まない、請求項1〜21のいずれか一項に記載の潤滑剤組成物。
- a)1つ以上のN-α-ナフチル-N-フェニルアミン酸化防止剤、及び/又はb)1つ以上のジフェニルアミン酸化防止剤; 及び
c)1つ以上の硫黄含有添加剤
を含む、添加剤パッケージ。 - c)が、a)+b)+c)の総重量に基づいて、約2wt%〜約30wt%存在する、請求項23に記載の添加剤パッケージ。
- a)及びb)を含み、a)対b)の重量/重量比が、約1/1〜約1/9である、請求項23又は24に記載の添加剤パッケージ。
- 請求項23〜25に記載の添加剤パッケージと、有機溶媒、ベースストック及び液体潤滑剤添加剤からなる群から選択される希釈剤とを含む、添加剤濃縮物。
- N-α-ナフチル-N-フェニルアミン酸化防止剤及びジフェニルアミン酸化防止剤からなる群から選択される1つ以上の酸化防止剤; 及び
1つ以上の硫黄含有添加剤
を、基油に組み込むステップを含む、潤滑剤組成物を調製する方法。 - N-α-ナフチル-N-フェニルアミン酸化防止剤及びジフェニルアミン酸化防止剤が、合計で、潤滑剤組成物の総重量に基づいて、約0.2wt%〜約0.8wt%存在する、請求項27に記載の方法。
- 硫黄含有添加剤によって提供される硫黄濃度が、合計で、潤滑剤組成物の総重量に基づいて、約50重量ppm〜約1000重量ppmの範囲である、請求項27又は28に記載の方法。
- 請求項1〜22のいずれか一項に記載の潤滑剤組成物を、タービンギアボックス及び/若しくはタービンベアリングに、又はエンジンに添加するステップを含む、タービン又はエンジンを潤滑化させる方法。
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EP4130207B1 (de) | 2021-08-03 | 2024-03-06 | LANXESS Deutschland GmbH | Additivmischung für turbinenöle |
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CN114164031A (zh) * | 2021-12-03 | 2022-03-11 | 东莞太平洋博高润滑油有限公司 | 一种长寿型合成空压机油及其制备方法 |
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