JP2020522865A - 封止フィルム - Google Patents
封止フィルム Download PDFInfo
- Publication number
- JP2020522865A JP2020522865A JP2019567992A JP2019567992A JP2020522865A JP 2020522865 A JP2020522865 A JP 2020522865A JP 2019567992 A JP2019567992 A JP 2019567992A JP 2019567992 A JP2019567992 A JP 2019567992A JP 2020522865 A JP2020522865 A JP 2020522865A
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- JP
- Japan
- Prior art keywords
- organic electronic
- layer
- resin
- sealing
- electronic device
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 238000007789 sealing Methods 0.000 title claims abstract description 120
- 238000004519 manufacturing process Methods 0.000 claims abstract description 12
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- 239000011347 resin Substances 0.000 claims description 111
- 239000003795 chemical substances by application Substances 0.000 claims description 48
- 229910052751 metal Inorganic materials 0.000 claims description 45
- 239000002184 metal Substances 0.000 claims description 44
- 239000003463 adsorbent Substances 0.000 claims description 41
- 239000000203 mixture Substances 0.000 claims description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 28
- 239000002245 particle Substances 0.000 claims description 26
- 150000001875 compounds Chemical class 0.000 claims description 20
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- 238000001179 sorption measurement Methods 0.000 claims description 12
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 11
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 10
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 8
- 229910052742 iron Inorganic materials 0.000 claims description 8
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- 150000004706 metal oxides Chemical class 0.000 claims description 7
- 238000003775 Density Functional Theory Methods 0.000 claims description 6
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- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 4
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- 238000002161 passivation Methods 0.000 claims description 4
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- 229910052802 copper Inorganic materials 0.000 claims description 3
- 239000010949 copper Substances 0.000 claims description 3
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims description 3
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- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 2
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- 229910000423 chromium oxide Inorganic materials 0.000 claims description 2
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- PJXISJQVUVHSOJ-UHFFFAOYSA-N indium(iii) oxide Chemical compound [O-2].[O-2].[O-2].[In+3].[In+3] PJXISJQVUVHSOJ-UHFFFAOYSA-N 0.000 claims description 2
- AMGQUBHHOARCQH-UHFFFAOYSA-N indium;oxotin Chemical compound [In].[Sn]=O AMGQUBHHOARCQH-UHFFFAOYSA-N 0.000 claims description 2
- BPUBBGLMJRNUCC-UHFFFAOYSA-N oxygen(2-);tantalum(5+) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[Ta+5].[Ta+5] BPUBBGLMJRNUCC-UHFFFAOYSA-N 0.000 claims description 2
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- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 claims description 2
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- URLJKFSTXLNXLG-UHFFFAOYSA-N niobium(5+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[Nb+5].[Nb+5] URLJKFSTXLNXLG-UHFFFAOYSA-N 0.000 claims 1
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- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 4
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- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 4
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- XJHCXCQVJFPJIK-UHFFFAOYSA-M caesium fluoride Chemical compound [F-].[Cs+] XJHCXCQVJFPJIK-UHFFFAOYSA-M 0.000 description 4
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- CQOZJDNCADWEKH-UHFFFAOYSA-N 2-[3,3-bis(2-hydroxyphenyl)propyl]phenol Chemical class OC1=CC=CC=C1CCC(C=1C(=CC=CC=1)O)C1=CC=CC=C1O CQOZJDNCADWEKH-UHFFFAOYSA-N 0.000 description 3
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- 125000000217 alkyl group Chemical group 0.000 description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
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Images
Classifications
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- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K50/00—Organic light-emitting devices
- H10K50/80—Constructional details
- H10K50/84—Passivation; Containers; Encapsulations
- H10K50/846—Passivation; Containers; Encapsulations comprising getter material or desiccants
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- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K50/00—Organic light-emitting devices
- H10K50/80—Constructional details
- H10K50/84—Passivation; Containers; Encapsulations
- H10K50/844—Encapsulations
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B32B27/00—Layered products comprising a layer of synthetic resin
- B32B27/06—Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material
- B32B27/08—Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material of synthetic resin
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B27/00—Layered products comprising a layer of synthetic resin
- B32B27/18—Layered products comprising a layer of synthetic resin characterised by the use of special additives
- B32B27/20—Layered products comprising a layer of synthetic resin characterised by the use of special additives using fillers, pigments, thixotroping agents
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2264/00—Composition or properties of particles which form a particulate layer or are present as additives
- B32B2264/10—Inorganic particles
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- Optics & Photonics (AREA)
- Electroluminescent Light Sources (AREA)
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- Piezo-Electric Or Mechanical Vibrators, Or Delay Or Filter Circuits (AREA)
- Apparatuses And Processes For Manufacturing Resistors (AREA)
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Abstract
Description
本出願は、2017年6月9日付けの韓国特許出願第10−2017−0072500号に基づく優先権の利益を主張し、当該韓国特許出願の文献に開示されたすべての内容は、本明細書の一部として含まれる。
本出願は、封止フィルム、これを含む有機電子装置および前記有機電子装置の製造方法に関する。
また、前記活性エネルギー線重合性化合物は、封止樹脂100重量部に対して5重量部〜30重量部、5重量部〜25重量部、8重量部〜20重量部、10重量部〜18重量部または12重量部〜18重量部で含まれ得る。本出願は、前記範囲内で、高温高湿など苛酷条件でも耐久信頼性に優れた封止フィルムを提供する。
封止層の製造
第1層溶液を製造するためにブチルゴム樹脂(BT−20、Sunwoo Chem−tech)180gおよびDCPD(dicyclopentadiene)系石油樹脂(SU5270、Sunwoo Chem−tech)60gをトルエンで希釈した溶液(固形分33%)を製造した後、溶液を均質化した。前記均質化した溶液に多官能性アクリレート(トリメチロールプロパントリアクリレート、MIWON)10gおよび光開始剤(Irgacure 819、Ciba)3gを投入して均質化した後、1時間の間高速撹拌して、第1層溶液を製造した。
あらかじめ準備されたメタル層(アルミニウム箔、厚さ70μm)上に、封止層の第2層に付着した離型処理されたPETを剥離させ、ロール・ツー・ロール(Roll−to−Roll)工程で70℃でラミネーションして、第2層がメタル層と接するように封止フィルムを製造した。
輝点防止剤を表1のように変更したことを除いて、実施例1と同じ方法で封止フィルムを製造した。
実施例および比較例で使用した輝点防止剤のアウトガスに対する吸着エネルギーを密度汎関数理論(density functional theory)基盤の電子構造計算を用いて計算した。結晶型構造を有する輝点防止剤の最密充填面が表面に露出する2次元スラブ構造を作った後、構造最適化を進め、この真空状態の表面上に輝点原因分子が吸着した構造に対する構造最適化を進めた後、これらの二つのシステムの総エネルギーの差異から輝点原因分子の総エネルギーを抜いた値を吸着エネルギーと定義した。それぞれのシステムに対する総エネルギー計算のために電子−電子間の相互作用を模写する交換相関(exchange−correlation)でGGA(generalized gradient approximation)系の関数であるrevised−PBE関数を使用し、電子運動エネルギーのカットオフは、500eVを使用し、逆格子空間の原点に該当するガンマ点のみを含ませて計算した。各システムの原子構造を最適化するために共役勾配法を使用し、原子間の力が0.01eV/Å以下となるまで反復計算を行った。一連の計算は、常用コードであるVASPを用いて行われた。
ガラス基板上に有機電子素子を蒸着した後、前記実施例および比較例で製造した封止フィルムを真空接合器を用いて50℃、真空度50mTorr、0.4MPaの条件で前記素子上に接合して、有機電子パネルを製造した。
2、4、6 封止層
3 輝点防止剤
5 水分吸着剤
7 磁性体粒子
21 基板
23 有機電子素子
Claims (20)
- 少なくとも2以上の封止層を含む有機電子素子封止フィルムであり、前記封止層は、前記有機電子素子と接する第1層と、前記有機電子素子と接しない第2層とを含み、前記第2層は、密度汎関数理論近似法(Density Functional Theory)により計算された、アウトガスに対する吸着エネルギーが0eV以下の輝点防止剤を含む有機電子素子封止フィルム。
- アウトガスは、H+ガス、H2ガスまたはNH3ガスを含む、請求項1に記載の有機電子素子封止フィルム。
- 第1層は、封止フィルム内の全体輝点防止剤の質量を基準として15%以下で輝点防止剤を含むか、または含まない、請求項1または2に記載の有機電子素子封止フィルム。
- 封止層は、封止樹脂および/または水分吸着剤を含む、請求項1〜3のいずれか一項に記載の有機電子素子封止フィルム。
- 水分吸着剤は、化学反応性水分吸着剤を含む、請求項4に記載の有機電子素子封止フィルム。
- 水分吸着剤に対する輝点防止剤の重量比が0.05〜0.8の範囲内である、請求項4または5に記載の有機電子素子封止フィルム。
- 水分吸着剤は、粒径が100〜15,000nmの範囲内である、請求項4〜6のいずれか一項に記載の有機電子素子封止フィルム。
- 輝点防止剤の粒径は、10nm〜30μmの範囲内である、請求項1に記載の有機電子素子封止フィルム。
- 輝点防止剤は、封止層内の樹脂成分100重量部に対して3〜150重量部で含まれる、請求項1〜8のいずれか一項に記載の有機電子素子封止フィルム。
- 封止層が基板上に形成された有機電子素子の前面を密封する、請求項1〜9のいずれか一項に記載の有機電子素子封止フィルム。
- 第2層上に形成されたメタル層をさらに含む、請求項1〜10のいずれか一項に記載の有機電子素子封止フィルム。
- メタル層は、50〜800W/m・Kの熱伝導度を有する、請求項11に記載の有機電子素子封止フィルム。
- メタル層は、金属、酸化金属、窒化金属、炭化金属、オキシ窒化金属、オキシホウ化金属、およびそれらの配合物のうちいずれか一つを含む、請求項11に記載の有機電子素子封止フィルム。
- メタル層は、鉄、クロム、アルミニウム、銅、ニッケル、酸化鉄、酸化クロム、酸化シリコン、酸化アルミニウム、酸化チタン、酸化インジウム、酸化スズ、酸化スズインジウム、酸化タンタル、酸化ジルコニウム、酸化ニオビウム、およびこれらの配合物のうちいずれか一つを含む、請求項11に記載の有機電子素子封止フィルム。
- 封止層は、磁性体粒子を含む磁性層をさらに含み、前記磁性層は、第2層とメタル層との間に形成されるか、または前記メタル層上に形成される、請求項11〜14のいずれか一項に記載の有機電子素子封止フィルム。
- 磁性層は、バインダー樹脂を含む、請求項15に記載の有機電子素子封止フィルム。
- バインダー樹脂は、磁性体粒子100重量部に対して5重量部〜30重量部で含まれる、請求項16に記載の有機電子素子封止フィルム。
- 基板と;基板上に形成された有機電子素子と;前記有機電子素子を封止する請求項1〜17のいずれか一項に記載の封止フィルムとを含む有機電子装置。
- 有機電子素子は、一対の電極と、少なくとも発光層を含む有機層と、パッシベーション膜とを含む、請求項18に記載の有機電子装置。
- 上部に有機電子素子が形成された基板に請求項1〜18のいずれか一項に記載の封止フィルムが前記有機電子素子をカバーするように適用する段階を含む有機電子装置の製造方法。
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JP6953062B2 (ja) | 2021-10-27 |
TW201919891A (zh) | 2019-06-01 |
KR20180134776A (ko) | 2018-12-19 |
WO2018226077A1 (ko) | 2018-12-13 |
CN110731017A (zh) | 2020-01-24 |
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