JP2020514209A5 - - Google Patents
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- Publication number
- JP2020514209A5 JP2020514209A5 JP2019522394A JP2019522394A JP2020514209A5 JP 2020514209 A5 JP2020514209 A5 JP 2020514209A5 JP 2019522394 A JP2019522394 A JP 2019522394A JP 2019522394 A JP2019522394 A JP 2019522394A JP 2020514209 A5 JP2020514209 A5 JP 2020514209A5
- Authority
- JP
- Japan
- Prior art keywords
- type zeolite
- framework type
- polyethyleneimine
- mtw framework
- mtw
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229920002873 Polyethylenimine Polymers 0.000 claims 8
- 239000010457 zeolite Substances 0.000 claims 8
- 239000000203 mixture Substances 0.000 claims 3
- 239000011541 reaction mixture Substances 0.000 claims 3
- 238000002425 crystallisation Methods 0.000 claims 2
- 230000005712 crystallization Effects 0.000 claims 2
- -1 fluoride ions Chemical class 0.000 claims 1
- 239000011148 porous material Substances 0.000 claims 1
- 230000002194 synthesizing Effects 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
Claims (9)
- MTWフレームワーク型ゼオライトを合成する方法であって、
(a)以下を含む反応混合物を調製すること:
(1)FAUフレームワーク型ゼオライト;
(2)ポリエチレンイミン(Q);
(3)フッ化物イオン;及び
(4)水;ならびに
(b)該反応混合物を、該MTWフレームワーク型ゼオライトの結晶を形成するのに十分な結晶化条件に供することを含み、
該反応混合物が、モル比で以下の組成を有する、
上記方法。 - 前記ポリエチレンイミンが線状ポリエチレンイミンである、請求項1に記載の方法。
- 前記線状ポリエチレンイミンが、1500〜5000の範囲の数平均分子量を有する、請求項2に記載の方法。
- 前記結晶化条件が125℃〜200℃の温度を含む、請求項1に記載の方法。
- ポリエチレンイミンをその細孔構造内に含むMTWフレームワーク型ゼオライト。
- 合成されたままの無水の形態で、モル比で以下の組成を有する、請求項5記載のMTWフレームワーク型ゼオライト:
- 合成されたままの無水の形態で、モル比で以下の組成を有する、請求項5記載のMTWフレームワーク型ゼオライト:
- 前記ポリエチレンイミンが線状ポリエチレンイミンである、請求項5に記載のMTWフレームワーク型ゼオライト。
- 前記線状ポリエチレンイミンが、1500〜5000の範囲の数平均分子量を有する、請求項8に記載のMTWフレームワーク型ゼオライト。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201662423271P | 2016-11-17 | 2016-11-17 | |
US62/423,271 | 2016-11-17 | ||
PCT/US2017/056925 WO2018093510A1 (en) | 2016-11-17 | 2017-10-17 | Synthesis of mtw framework type zeolites via interzeolite transformation |
Publications (3)
Publication Number | Publication Date |
---|---|
JP2020514209A JP2020514209A (ja) | 2020-05-21 |
JP2020514209A5 true JP2020514209A5 (ja) | 2020-10-22 |
JP6912564B2 JP6912564B2 (ja) | 2021-08-04 |
Family
ID=60409332
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2019522394A Active JP6912564B2 (ja) | 2016-11-17 | 2017-10-17 | ゼオライト転換によるmtwフレームワーク型ゼオライトの合成 |
Country Status (6)
Country | Link |
---|---|
US (1) | US10478811B2 (ja) |
EP (1) | EP3541749B1 (ja) |
JP (1) | JP6912564B2 (ja) |
KR (1) | KR102413863B1 (ja) |
CN (1) | CN109890757B (ja) |
WO (1) | WO2018093510A1 (ja) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113772855A (zh) * | 2020-06-10 | 2021-12-10 | 中国石油化工股份有限公司 | 含镍铬废水的处理方法 |
Family Cites Families (35)
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US3832449A (en) | 1971-03-18 | 1974-08-27 | Mobil Oil Corp | Crystalline zeolite zsm{14 12 |
US4452769A (en) | 1979-03-21 | 1984-06-05 | Mobil Oil Corporation | Method of preparing crystalline zeolite |
US4537758A (en) | 1979-03-21 | 1985-08-27 | Mobil Oil Corporation | Process for preparing highly siliceous porous ZSM-12 type crystalline material |
GB2079735A (en) | 1980-07-07 | 1982-01-27 | Chevron Res | Novel zeolite designated CZH-5 |
EP0059059B2 (en) | 1981-02-23 | 1990-04-18 | Imperial Chemical Industries Plc | Zeolites |
US4391785A (en) | 1981-12-21 | 1983-07-05 | Mobil Oil Corporation | Preparation of ZSM-12 type zeolites |
US4557919A (en) | 1983-04-12 | 1985-12-10 | Teijin Petrochemical Industries Ltd. | Production of crystalline zeolites |
US4482531A (en) | 1983-04-29 | 1984-11-13 | Mobil Oil Corporation | Synthesis of ZSM-12 zeolite |
US4552739A (en) | 1983-12-09 | 1985-11-12 | Mobil Oil Corporation | Method of preparing crystalline zeolite ZSM-12 and product |
US4539193A (en) | 1984-05-23 | 1985-09-03 | Mobil Oil Corporation | Synthesis of crystalline silicate ZSM-12 |
GB8413370D0 (en) | 1984-05-24 | 1984-06-27 | British Petroleum Co Plc | Theta-3 |
US4552738A (en) | 1984-05-25 | 1985-11-12 | Mobil Oil Corporation | Synthesis of crystalline silicate ZSM-12 |
US4636373A (en) | 1984-06-26 | 1987-01-13 | Mobil Oil Corporation | Synthesis of crystalline silicate ZSM-12 using dibenzyldimethylammonium cations and the product produced |
US4585637A (en) | 1984-06-26 | 1986-04-29 | Mobil Oil Corporation | Synthesis of crystalline silicate ZSM-12 |
US4585746A (en) | 1984-06-27 | 1986-04-29 | Mobil Oil Corporation | Synthesis of crystalline silicate ZSM-12 |
US5021141A (en) | 1990-09-14 | 1991-06-04 | Mobil Oil Corp. | Synthesis of crystalline ZSM-12 type structure |
FR2670772B1 (fr) | 1990-12-21 | 1993-04-09 | Inst Francais Du Petrole | Zeolithe de type mtw et son procede de preparation. |
US5137705A (en) | 1991-04-08 | 1992-08-11 | Mobil Oil Corp. | Synthesis of crystalline silicate ZSM-12 |
US5192521A (en) | 1991-11-19 | 1993-03-09 | Mobil Oil Corp. | Synthesis of crystalline silicate ZSM-12 |
DE19939416A1 (de) * | 1999-08-20 | 2001-02-22 | Basf Ag | Verfahren zur Herstellung eines kristallinen, zeolithischen Feststoffs |
US6652832B2 (en) | 2001-02-05 | 2003-11-25 | Exxonmobil Oil Corporation | Synthesis of ZSM-12 |
US6660682B2 (en) * | 2001-11-30 | 2003-12-09 | Exxon Mobil Chemical Patents Inc. | Method of synthesizing molecular sieves |
US7211239B2 (en) * | 2005-04-22 | 2007-05-01 | Basf Aktiengesellschaft | Process for preparing a nanosized zeolitic material |
FR2936790B1 (fr) * | 2008-10-07 | 2010-09-24 | Inst Francais Du Petrole | Procede de preparation d'une zeolithe de type structural mtw |
AU2010233109B2 (en) * | 2009-04-09 | 2014-10-30 | California Institute Of Technology | Molecular sieves and related methods and structure directing agents |
US20110034749A1 (en) * | 2009-08-07 | 2011-02-10 | Exxonmobil Research And Engineering Company | Synthesis and use of ZSM-12 |
US8202506B2 (en) | 2009-11-17 | 2012-06-19 | Exxonmobil Research And Engineering Company | High activity small crystal ZSM-12 |
US8679451B2 (en) * | 2009-11-20 | 2014-03-25 | Chevron U.S.A. Inc. | Method for making aluminosilicate ZSM-12 |
JP5615530B2 (ja) * | 2009-11-20 | 2014-10-29 | ユニゼオ株式会社 | Mtw型ゼオライトの製造方法 |
EP2928826B1 (en) * | 2012-12-10 | 2017-12-20 | ExxonMobil Research and Engineering Company | Synthesis of molecular sieve itq-32 |
JP2014122142A (ja) * | 2012-12-21 | 2014-07-03 | Mitsubishi Plastics Inc | 遷移金属含有ゼオライト、及びその製造方法 |
US9233856B2 (en) * | 2013-04-20 | 2016-01-12 | Uop Llc | Use of zeolitic materials for removing mercury (+2) ions from liquid streams |
US9126190B2 (en) * | 2013-07-30 | 2015-09-08 | Chevron U.S.A. Inc. | Zeolite SSZ-70 having enhanced external surface area |
US9802831B2 (en) * | 2014-07-23 | 2017-10-31 | Chevron U.S.A. Inc. | Synthesis of high silica zeolite via interzeolite transformation without OSDAs |
US9938157B2 (en) * | 2014-07-23 | 2018-04-10 | Chevron U.S.A. Inc. | Interzeolite transformation and metal encapsulation in the absence of an SDA |
-
2017
- 2017-10-17 EP EP17801129.2A patent/EP3541749B1/en active Active
- 2017-10-17 KR KR1020197017225A patent/KR102413863B1/ko active IP Right Grant
- 2017-10-17 JP JP2019522394A patent/JP6912564B2/ja active Active
- 2017-10-17 WO PCT/US2017/056925 patent/WO2018093510A1/en unknown
- 2017-10-17 CN CN201780067627.0A patent/CN109890757B/zh active Active
- 2017-10-17 US US15/785,546 patent/US10478811B2/en active Active
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