JP2020180076A - 水性化粧料 - Google Patents
水性化粧料 Download PDFInfo
- Publication number
- JP2020180076A JP2020180076A JP2019084097A JP2019084097A JP2020180076A JP 2020180076 A JP2020180076 A JP 2020180076A JP 2019084097 A JP2019084097 A JP 2019084097A JP 2019084097 A JP2019084097 A JP 2019084097A JP 2020180076 A JP2020180076 A JP 2020180076A
- Authority
- JP
- Japan
- Prior art keywords
- mass
- cosmetics
- water
- aqueous
- carminic acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
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- 235000012730 carminic acid Nutrition 0.000 claims abstract description 66
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 72
- HOSGXJWQVBHGLT-UHFFFAOYSA-N 6-hydroxy-3,4-dihydro-1h-quinolin-2-one Chemical group N1C(=O)CCC2=CC(O)=CC=C21 HOSGXJWQVBHGLT-UHFFFAOYSA-N 0.000 claims description 2
- DGQLVPJVXFOQEV-JNVSTXMASA-N carminic acid Chemical compound OC1=C2C(=O)C=3C(C)=C(C(O)=O)C(O)=CC=3C(=O)C2=C(O)C(O)=C1[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O DGQLVPJVXFOQEV-JNVSTXMASA-N 0.000 description 59
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- ZADYMNAVLSWLEQ-UHFFFAOYSA-N magnesium;oxygen(2-);silicon(4+) Chemical compound [O-2].[O-2].[O-2].[Mg+2].[Si+4] ZADYMNAVLSWLEQ-UHFFFAOYSA-N 0.000 description 1
- 239000000594 mannitol Substances 0.000 description 1
- 235000010355 mannitol Nutrition 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 description 1
- 229920000609 methyl cellulose Polymers 0.000 description 1
- 235000010981 methylcellulose Nutrition 0.000 description 1
- 239000001923 methylcellulose Substances 0.000 description 1
- 230000001333 moisturizer Effects 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- BWOROQSFKKODDR-UHFFFAOYSA-N oxobismuth;hydrochloride Chemical compound Cl.[Bi]=O BWOROQSFKKODDR-UHFFFAOYSA-N 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 229960000292 pectin Drugs 0.000 description 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 1
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 description 1
- 229950009195 phenylpropanol Drugs 0.000 description 1
- 229920003229 poly(methyl methacrylate) Polymers 0.000 description 1
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 description 1
- 229920001515 polyalkylene glycol Polymers 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 239000004926 polymethyl methacrylate Substances 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
- 235000010409 propane-1,2-diol alginate Nutrition 0.000 description 1
- 239000000770 propane-1,2-diol alginate Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 1
- 229910010271 silicon carbide Inorganic materials 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 235000010413 sodium alginate Nutrition 0.000 description 1
- 239000000661 sodium alginate Substances 0.000 description 1
- 229940005550 sodium alginate Drugs 0.000 description 1
- 229940010747 sodium hyaluronate Drugs 0.000 description 1
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 description 1
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 235000010356 sorbitol Nutrition 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 150000003871 sulfonates Chemical class 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000000979 synthetic dye Substances 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- UJMBCXLDXJUMFB-GLCFPVLVSA-K tartrazine Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)C1=NN(C=2C=CC(=CC=2)S([O-])(=O)=O)C(=O)C1\N=N\C1=CC=C(S([O-])(=O)=O)C=C1 UJMBCXLDXJUMFB-GLCFPVLVSA-K 0.000 description 1
- 235000012756 tartrazine Nutrition 0.000 description 1
- 229960000943 tartrazine Drugs 0.000 description 1
- 239000004149 tartrazine Substances 0.000 description 1
- 229960003080 taurine Drugs 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- UJMBCXLDXJUMFB-UHFFFAOYSA-K trisodium;5-oxo-1-(4-sulfonatophenyl)-4-[(4-sulfonatophenyl)diazenyl]-4h-pyrazole-3-carboxylate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)C1=NN(C=2C=CC(=CC=2)S([O-])(=O)=O)C(=O)C1N=NC1=CC=C(S([O-])(=O)=O)C=C1 UJMBCXLDXJUMFB-UHFFFAOYSA-K 0.000 description 1
- 235000013799 ultramarine blue Nutrition 0.000 description 1
- 229920001285 xanthan gum Polymers 0.000 description 1
- 235000010493 xanthan gum Nutrition 0.000 description 1
- 239000000230 xanthan gum Substances 0.000 description 1
- 229940082509 xanthan gum Drugs 0.000 description 1
- 239000000811 xylitol Substances 0.000 description 1
- 235000010447 xylitol Nutrition 0.000 description 1
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 1
- 229960002675 xylitol Drugs 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 description 1
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- A61K2800/872—Pencils; Crayons; Felt-tip pens
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- General Health & Medical Sciences (AREA)
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- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
Description
5〜50mPa・s:BLアダプタ、回転数12rpm
50〜500mPa・s:ローターNo.1、回転数12rpm
250〜2500mPa・s:ローターNo.2、回転数12rpm
1000〜10000mPa・s:ローターNo.3、回転数12rpm
5000〜50000mPa・s:ローターNo.4、回転数12rpm
表1、2に示す成分を同表中に示す割合(質量%)で混合し、ボトルタイプ用水性化粧料を調製した。表中に示す成分は下記のものを使用した。なお、表中、水の割合は、pH調整剤の使用量等によって変動があるため、範囲によって示され、少なくとも表に示す範囲内に収まるものである。
カルミン酸:CARMIN SOLUBLE W3014(セイシェント製)。表中に示す割合はカルミン酸としての純量である。
皮膜形成性アクリル酸ポリマーエマルション:ダイトゾール5000SJ(大東化成工業株式会社製)。表中に示す割合は固形分換算値である。
皮膜形成性アクリル酸ポリマー:プラスサイズL−9540U(互応化学工業株式会社製)。表中に示す割合は固形分換算値である。
アクリル酸アミド系増粘剤:SEPINOV EMT 10(SEPPIC社製)
ブルックフィールド型粘度計を用いて、下記の条件で25℃での水性化粧料の粘度を測定した。
5〜50mPa・s:BLアダプタ、回転数12rpm
50〜500mPa・s:ローターNo.1、回転数12rpm
250〜2500mPa・s:ローターNo.2、回転数12rpm
1000〜10000mPa・s:ローターNo.3、回転数12rpm
5000〜50000mPa・s:ローターNo.4、回転数12rpm
水性化粧料の調製直後に、水性化粧料50gをスクリュー管に入れ、蓋を閉めた状態で25℃又は50℃で1ヶ月間保管した。25℃及び50℃ともに、1ヶ月保管後に析出物が目視で確認されないものを「○」、25℃で1週間以内に析出物が確認されたものを「×」とした。
水性化粧料の調製直後に水性化粧料50gをスクリュー管に入れ、スクリュー管内の水性化粧料に綿棒を浸し、綿棒により紙に線を描いた。描いた線の色味を目視で確認した。スクリュー管の蓋を閉めた状態で25℃又は50℃で1ヶ月間保管した。1ヶ月保管後に同様に綿棒を水性化粧料に浸して紙に線を描き、描いた線の色味を目視で確認し、調製直後に描いた線の当時の色味と比較した。保管後に25℃及び50℃ともに変色がなかったものを「○」、25℃保管で変色が見られないが50℃保管で変色が見られたものを「△」、25℃及び50℃ともに変色が見られたものを「×」とした。
オートペンに充填するアイブロウ化粧料として、表3及び表4に示す配合の水性化粧料を調製した。評価としては、上述のスクリュー管での評価に加え、オートペン充填品での評価を行った。具体的には、析出については、オートペンタイプのペン型容器に水性化粧料を充填し、蓋を閉めた状態で25℃又は50℃で1ヶ月保存した。25℃及び50℃ともにペン型容器の塗布体(筆)に1ヶ月間析出が見られないものを「○」とし、25℃で1週間以内に析出が観察されたものを「×」とした。色安定性については、水性化粧料を充填したペンで紙に線を描き、スクリュー管の場合と同様に、調製直後及び1ヶ月保存後に描いた色味を比較し、25℃及び50℃ともに調製直後及び1ヶ月保存後で変色が見られないものを「○」、25℃保管で変色が見られないが50℃保管で変色が見られたものを「△」、25℃及び50℃ともに変色が見られたものを「×」とした。
以下に、その他の水性化粧料の実施例を挙げる。上記試験例と同様に、pH、粘度、スクリュー管又はオートペン充填品での析出及び色安定性を評価した。
下記配合のチークを調製した。
ブチレングリコール 10.0質量%
カルミン酸 1.0質量%
青色1号 0.01質量%
黄色4号 0.1質量%
アクリル酸アミド系増粘剤 1.7質量%
防腐剤 0.8質量%
pH調整剤 適宜
水(残余) 81.19−86.19質量%
水に対するカルミン酸割合 1.160−1.232質量%
pH 7.5
粘度 1425mPa・s
析出(スクリュー管) ○
色安定性(スクリュー管) ○
下記配合のリップ用化粧料を調製した。
ブチレングリコール 10.0質量%
エタノール 1.0質量%
カルミン酸 1.4質量%
カルボマー 0.03質量%
皮膜形成性アクリル酸ポリマーエマルション 5.0質量%
防腐剤 0.8質量%
pH調整剤 適宜
水(残余) 76.43−81.43質量%
水に対するカルミン酸割合 1.719−1.832質量%
pH 7.5
粘度 3.25mPa・s
析出(スクリュー管) ○
色安定性(スクリュー管) ○
下記配合のアイライナーを調製した。
ブチレングリコール 10.0質量%
カルミン酸 0.6質量%
青色1号 0.075質量%
黄色4号 0.075質量%
皮膜形成性アクリル酸ポリマーエマルション 10.0質量%
防腐剤 0.8質量%
pH調整剤 適宜
水(残余) 73.28−78.28質量%
水に対するカルミン酸割合 0.766−0.819質量%
pH 7.5
粘度 2.5mPa・s
析出(スクリュー管) ○
色安定性(スクリュー管) ○
析出(ペン塗布体) ○
色安定性(描線) ○
Claims (7)
- 多価アルコール及びカルミン酸を含み、カルミン酸の含有量が水性化粧料全量に対して0.2質量%以上2質量%未満である、水性化粧料。
- 前記多価アルコールの含有量が、水性化粧料全量に対して0.5〜70質量%である、請求項1に記載の水性化粧料。
- 水の含有量が、水性化粧料全量に対して30〜99.3質量%である、請求項1又は2に記載の水性化粧料。
- 前記多価アルコールが2〜6個の水酸基を有する、請求項1〜3のいずれか一項に記載の水性化粧料。
- ブルックフィールド型粘度計により測定される25℃での粘度が2〜50mPa・sである、請求項1〜4のいずれか一項に記載の水性化粧料。
- 目元用である、請求項1〜5のいずれか一項に記載の水性化粧料。
- ペン型容器、及び該ペン型容器に充填された請求項1〜6のいずれか一項に記載の水性化粧料を有する、ペン型水性化粧料。
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US16/846,408 US11642292B2 (en) | 2019-04-25 | 2020-04-13 | Aqueous cosmetic |
FR2003690A FR3095342B1 (fr) | 2019-04-25 | 2020-04-14 | Cosmétique aqueux |
KR1020200048716A KR20200125487A (ko) | 2019-04-25 | 2020-04-22 | 수성 화장료 |
CN202010322715.4A CN111840114A (zh) | 2019-04-25 | 2020-04-22 | 水性化妆料 |
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US11642292B2 (en) | 2023-05-09 |
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FR3095342B1 (fr) | 2023-11-03 |
US12005133B2 (en) | 2024-06-11 |
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US20200337966A1 (en) | 2020-10-29 |
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