JP2014510011A5 - - Google Patents
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- Publication number
- JP2014510011A5 JP2014510011A5 JP2013557743A JP2013557743A JP2014510011A5 JP 2014510011 A5 JP2014510011 A5 JP 2014510011A5 JP 2013557743 A JP2013557743 A JP 2013557743A JP 2013557743 A JP2013557743 A JP 2013557743A JP 2014510011 A5 JP2014510011 A5 JP 2014510011A5
- Authority
- JP
- Japan
- Prior art keywords
- hollow microspheres
- feedstock composition
- total weight
- less
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000004005 microsphere Substances 0.000 claims 7
- 239000000203 mixture Substances 0.000 claims 5
- 239000011521 glass Substances 0.000 claims 4
- 239000006185 dispersion Substances 0.000 claims 2
- 239000002245 particle Substances 0.000 claims 2
- 239000004604 Blowing Agent Substances 0.000 claims 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N Boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims 1
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N Boron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 claims 1
- 239000004327 boric acid Substances 0.000 claims 1
- 229910052810 boron oxide Inorganic materials 0.000 claims 1
- 239000004088 foaming agent Substances 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 238000001694 spray drying Methods 0.000 claims 1
Claims (2)
- 中空微小球が得られる供給原料組成物の総重量に基づいて少なくとも45重量%のリサイクルガラスを含む、中空微小球であって、1.25g/cm3未満の真密度、20MPaを超える20%体積減少での強度を有し、実質的に単一セル構造を有し、更に、前記中空微小球が得られる前記供給原料組成物の総重量に基づいて0.05重量%未満の添加された有効な発泡剤を有する供給原料組成物から製造されてなる、中空微小球。
- リサイクルガラス粒子を含み、供給原料組成物の総重量に基づいて0.05重量%未満の添加された有効な発泡剤を含む、前記供給原料組成物を提供することと、
リサイクルガラス粒子と、ホウ酸及び酸化ホウ素の少なくとも1つとの水性分散液を形成することと、
前記水性分散液を噴霧乾燥して、球状ガラス凝集物を形成することと、
前記凝集物を加熱して、中空微小球を形成することと、
を含み、前記中空微小球が実質的に単一セル構造を有する、中空微小球の作製方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201161449808P | 2011-03-07 | 2011-03-07 | |
US61/449,808 | 2011-03-07 | ||
PCT/US2012/026434 WO2012134679A2 (en) | 2011-03-07 | 2012-02-24 | Hollow microspheres |
Publications (3)
Publication Number | Publication Date |
---|---|
JP2014510011A JP2014510011A (ja) | 2014-04-24 |
JP2014510011A5 true JP2014510011A5 (ja) | 2015-04-09 |
JP5990203B2 JP5990203B2 (ja) | 2016-09-07 |
Family
ID=46932218
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2013557743A Expired - Fee Related JP5990203B2 (ja) | 2011-03-07 | 2012-02-24 | 中空微小球 |
Country Status (8)
Country | Link |
---|---|
US (1) | US20130344337A1 (ja) |
EP (1) | EP2683668A4 (ja) |
JP (1) | JP5990203B2 (ja) |
KR (1) | KR20140011352A (ja) |
CN (1) | CN103415481B (ja) |
BR (1) | BR112013022871A2 (ja) |
RU (1) | RU2586128C2 (ja) |
WO (1) | WO2012134679A2 (ja) |
Families Citing this family (24)
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US10435177B2 (en) | 2006-02-17 | 2019-10-08 | Earthstone International Llc | Foamed glass composite arrestor beds having predetermined failure modes |
BR112013013237A2 (pt) * | 2010-12-20 | 2016-09-06 | 3M Innovative Properties Co | método de formação de microesferas ocas, microesferas ocas e aparelho para formação de microesferas ocas de vidro |
US9540276B2 (en) | 2012-06-06 | 2017-01-10 | 3M Innovative Properties Company | Low density glass particles with low boron content |
US20140194328A1 (en) * | 2013-01-07 | 2014-07-10 | Vince Alessi | Thermoset ceramic compositions and a method of preparation therefor |
US10111424B2 (en) | 2013-05-17 | 2018-10-30 | 3M Innovative Properties Company | Release of biologically active agents from polymeric composite particles |
CN105228820B (zh) | 2013-05-17 | 2017-08-29 | 3M创新有限公司 | 反应混合物、多孔粒子以及制备方法 |
US9016090B2 (en) * | 2013-06-12 | 2015-04-28 | Hamid Hojaji | Glass microspheres comprising sulfide, and methods of producing glass microspheres |
EP3022161B1 (en) | 2013-07-18 | 2020-03-11 | 3M Innovative Properties Company | Glass microbubbles and method of making a raw product comprising the glass microbubbles |
CN103435322A (zh) * | 2013-08-19 | 2013-12-11 | 南京大学 | 一种耐高温陶瓷基地聚合物的制备方法 |
CN103723910B (zh) * | 2013-12-14 | 2016-06-29 | 蚌埠玻璃工业设计研究院 | 一种多孔玻璃微珠的制备方法 |
SI3154860T1 (sl) | 2014-06-11 | 2021-11-30 | Earthstone International, Llc | Postopek za upočasnitev letala, kije prevozilo vzletno-pristajalno stezo, postopek za izdelavo sistema za zaustavljanje za letališča in varnostno območje vzletno-pristajalne steze |
US20170157582A1 (en) * | 2014-07-02 | 2017-06-08 | Corning Incorporated | Spray drying mixed batch material for plasma melting |
GB201415005D0 (en) * | 2014-08-22 | 2014-10-08 | Univ Nottingham | Porous and non-pourous bodies |
US10196296B2 (en) | 2015-01-17 | 2019-02-05 | Hamid Hojaji | Fluid permeable and vacuumed insulating microspheres and methods of producing the same |
CN105036555A (zh) * | 2015-07-13 | 2015-11-11 | 安徽天堂唯高塑业科技有限公司 | 一种用于汽车车牌级反光膜的玻璃微珠及其制备方法 |
US9643876B2 (en) | 2015-10-04 | 2017-05-09 | Hamid Hojaji | Microspheres and methods of making the same |
EP3526510A4 (en) | 2016-10-17 | 2020-06-03 | Whirlpool Corporation | INSULATING CORE MATERIAL HAVING COATED INSULATED SPHERES AND METHOD OF MANUFACTURING THE INSULATING CORE MATERIAL |
US10330394B2 (en) | 2017-06-16 | 2019-06-25 | Ford Global Technologies, Llc | Heat transfer mediums |
JP2019112283A (ja) * | 2017-12-26 | 2019-07-11 | 日本電気硝子株式会社 | ガラスフィラーの製造方法 |
RU2719466C1 (ru) | 2019-02-21 | 2020-04-17 | Общество с ограниченной ответственностью "УралНИПИнефть" | Способ получения полых гранул из неорганического сырья и устройство для его осуществления |
US11555113B2 (en) | 2019-09-10 | 2023-01-17 | Ticona Llc | Liquid crystalline polymer composition |
CN112897897A (zh) * | 2020-05-10 | 2021-06-04 | 中国科学院理化技术研究所 | 提高中空玻璃微球耐久性的方法及获得的中空玻璃微球 |
CN115645552B (zh) * | 2021-10-22 | 2023-09-29 | 中山大学肿瘤防治中心(中山大学附属肿瘤医院、中山大学肿瘤研究所) | 一种放射性栓塞玻璃微球及其制备方法和应用 |
CN117263501A (zh) * | 2023-10-07 | 2023-12-22 | 中国原子能科学研究院 | 含钇中空玻璃球的制备方法及应用 |
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SU812780A1 (ru) * | 1979-01-10 | 1981-03-15 | Ленинградский Ордена Трудовогокрасного Знамени Технологическийинститут Им. Ленсовета | Способ получени полых стекл нныхМиКРОСфЕР |
US4370166A (en) * | 1980-09-04 | 1983-01-25 | Standard Oil Company (Indiana) | Low density cement slurry and its use |
US4391646A (en) * | 1982-02-25 | 1983-07-05 | Minnesota Mining And Manufacturing Company | Glass bubbles of increased collapse strength |
US4767726A (en) * | 1987-01-12 | 1988-08-30 | Minnesota Mining And Manufacturing Company | Glass microbubbles |
US5069702A (en) * | 1990-12-20 | 1991-12-03 | W. R. Grace & Co.-Conn. | Method of making small hollow glass spheres |
US5366571A (en) * | 1993-01-15 | 1994-11-22 | The United States Of America As Represented By The Secretary Of The Interior | High pressure-resistant nonincendive emulsion explosive |
NZ274610A (en) * | 1993-09-08 | 1996-10-28 | Pq Corp | Hollow borosilicate microspheres and method of making |
DE19734791B4 (de) * | 1997-08-11 | 2005-06-09 | Hermsdorfer Institut Für Technische Keramik E.V. | Verfahren zur Herstellung eines offenporigen Blähglasgranulats |
EP1172341A4 (en) * | 1999-06-30 | 2003-06-04 | Asahi Glass Co Ltd | FINE HOLLOW GLASS SPHERES AND PROCESS FOR PREPARING THE SAME |
EP1156021A1 (en) * | 2000-05-19 | 2001-11-21 | Asahi Glass Co., Ltd. | Hollow aluminosilicate glass microspheres and process for their production |
JP2002037645A (ja) * | 2000-05-19 | 2002-02-06 | Asahi Glass Co Ltd | 微小中空アルミノシリケートガラス球状体およびその製造方法 |
JP2002037636A (ja) * | 2000-07-26 | 2002-02-06 | Toshiba Eng Co Ltd | 微小中空球体の製造方法、その製造装置および廃棄物リサイクル方法 |
JP2002338279A (ja) * | 2001-05-22 | 2002-11-27 | Asahi Glass Co Ltd | 微小中空ガラス球状体の製造方法 |
EP1549427B1 (en) * | 2002-08-23 | 2017-11-01 | James Hardie Technology Limited | Method for producing synthetic hollow microspheres |
JP2006193373A (ja) * | 2005-01-13 | 2006-07-27 | Tokai Kogyo Kk | 微小ガラスバブル及びその製造方法 |
WO2006118901A1 (en) * | 2005-04-29 | 2006-11-09 | 3M Innovative Properties Company | Glass microbubble-containing syntactic foams, explosives, and method of making |
CN101638295A (zh) * | 2008-07-30 | 2010-02-03 | 中国建材国际工程有限公司 | 一种空心玻璃微珠及其生产方法 |
CN101781083B (zh) * | 2009-12-21 | 2011-12-28 | 浙江通达机械有限公司 | 憎水空心玻璃微珠制备方法和所制备的憎水空心玻璃微珠 |
-
2012
- 2012-02-24 CN CN201280012465.8A patent/CN103415481B/zh not_active Expired - Fee Related
- 2012-02-24 RU RU2013141023/03A patent/RU2586128C2/ru not_active IP Right Cessation
- 2012-02-24 KR KR1020137025698A patent/KR20140011352A/ko not_active Application Discontinuation
- 2012-02-24 JP JP2013557743A patent/JP5990203B2/ja not_active Expired - Fee Related
- 2012-02-24 BR BR112013022871A patent/BR112013022871A2/pt active Search and Examination
- 2012-02-24 WO PCT/US2012/026434 patent/WO2012134679A2/en active Application Filing
- 2012-02-24 US US14/003,589 patent/US20130344337A1/en not_active Abandoned
- 2012-02-24 EP EP12763493.9A patent/EP2683668A4/en not_active Withdrawn
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