JP2013511702A - 熱分析システムおよび熱分析方法 - Google Patents
熱分析システムおよび熱分析方法 Download PDFInfo
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- JP2013511702A JP2013511702A JP2012539181A JP2012539181A JP2013511702A JP 2013511702 A JP2013511702 A JP 2013511702A JP 2012539181 A JP2012539181 A JP 2012539181A JP 2012539181 A JP2012539181 A JP 2012539181A JP 2013511702 A JP2013511702 A JP 2013511702A
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- 238000001382 dynamic differential scanning calorimetry Methods 0.000 claims description 9
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- 238000005260 corrosion Methods 0.000 claims description 4
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- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 claims description 3
- 229910052714 tellurium Inorganic materials 0.000 claims description 3
- PORWMNRCUJJQNO-UHFFFAOYSA-N tellurium atom Chemical group [Te] PORWMNRCUJJQNO-UHFFFAOYSA-N 0.000 claims description 3
- 238000004458 analytical method Methods 0.000 claims description 2
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- 229910052737 gold Inorganic materials 0.000 description 4
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 4
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Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
- G01N25/20—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity
- G01N25/48—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation
- G01N25/4806—Details not adapted to a particular type of sample
- G01N25/4813—Details not adapted to a particular type of sample concerning the measuring means
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
- G01N25/20—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity
- G01N25/48—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation
- G01N25/4806—Details not adapted to a particular type of sample
- G01N25/4826—Details not adapted to a particular type of sample concerning the heating or cooling arrangements
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Combustion & Propulsion (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analyzing Materials Using Thermal Means (AREA)
Abstract
【選択図】図1
Description
2 測定チャンバ
3 試料用るつぼ
4 試料側
5 基準物質用るつぼ
6 基準物質側
7,8 ペルチェシステム
9,10 電力供給手段
11 冷却ブロック
12,13 アルミニウム酸化物層
14,15 pドープおよびnドープしたシリコンゲルマニウム半導体素材キューブまたはブロック
16 金接点
17 電気コネクタ
Claims (14)
- 熱分析システム(1)であって、測定チャンバ(2)内で試料側(4)に配置された試料用るつぼ(3)および基準物質側(6)に配置された基準物質用るつぼ(5)を備え、前記試料用るつぼ(3)および前記基準物質用るつぼ(5)は、温度を記録および/または調整するペルチェシステム(7,8)を備えてなることを特徴とする熱分析システム。
- 請求項1に記載の熱分析システム(1)であって、ペルチェシステム(7,8)の代わりに熱電発電器を用いて温度を記録することができることを特徴とする熱分析システム。
- 請求項1または2に記載の熱分析システム(1)であって、熱分析システム(1)は動的示差走査熱量分析もしくは示差熱分析を実行するよう構成され、または、好適には動的示差走査熱量計である、熱分析システム。
- 請求項1〜3の何れか1項に記載の熱分析システム(1)であって、前記熱分析システム(1)の前記試料側および基準物質側(4、6)が対称に構成された、熱分析システム。
- 請求項1〜4の何れか1項に記載の熱分析システム(1)であって、それぞれのペルチェシステム(7,8)および/またはそれぞれの熱電発電器が、200℃超、好ましくは700℃超で用いられるよう設計された材料から形成された、熱分析システム。
- 請求項1〜5の何れか1項に記載の熱分析システム(1)であって、それぞれのペルチェシステム(7,8)および/またはそれぞれの熱電発電器が、複数の同一の構成要素によって構成されたモジュール構造を有する、熱分析システム。
- 請求項1〜6の何れか1項に記載の熱分析システム(1)であって、それぞれのペルチェシステム(7,8)は、熱分析システム(1)が熱流束型動的示差走査熱量計および/または入力補償型動的示差走査熱量計として動作可能であるような方法で、電気的に接続された、熱分析システム。
- 請求項1〜7の何れか1項に記載の熱分析システム(1)であって、熱分析システム(1)が、随意に、動的入力補償型または熱流束型の動的示差走査熱量計として動作が可能である、ペルチェシステムに基づいた複合的な動的示差走査熱量計として構成される、熱分析システム。
- 請求項1〜8の何れか1項に記載の熱分析システム(1)であって、ペルチェシステム(7,8)および/または熱電発電器の面は、耐ひっかき性および/または耐食性を有する、熱分析システム。
- 請求項1〜9の何れか1項に記載の熱分析システム(1)であって、動的示差走査熱量計に配置されたペルチェシステムおよび/または熱電発電器は、シリコンゲルマニウム半導体素材から形成される、熱分析システム。
- 請求項1〜10の何れか1項に記載の熱分析システム(1)であって、前記動的示差走査熱量計におけるそれぞれのペルチェシステム(7,8)および/または熱電発電器は、テルル、鉛、ビスマスまたは合金および/またはこれらの材料の合成物を含む、熱分析システム。
- 請求項1〜11の何れか1項に記載の熱分析システム(1)であって、特に前記動的示差走査熱量計におけるそれぞれのペルチェシステム(7,8)および/または熱電発電器は、スクッテルド鉱で構成されるシステムである、熱分析システム。
- 測定チャンバ(2)内で試料側(4)に配置された試料用るつぼ(3)および基準物質側(6)に配置された基準物質用るつぼ(5)を備えた熱分析方法であって、ペルチェ効果に基づいたシステムを用いて、前記試料用るつぼ(3)および前記基準物質用るつぼ(5)上の温度を記録および/または調整する、熱分析方法。
- 請求項13に記載の熱分析方法であって、熱電発電器を用いて前記試料用るつぼ(3)および前記基準物質用るつぼ(5)上の温度を記録する、熱分析方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
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DE102009054086.5 | 2009-11-20 | ||
DE102009054086 | 2009-11-20 | ||
PCT/DE2010/001350 WO2011060768A1 (de) | 2009-11-20 | 2010-11-17 | System und verfahren zur thermischen analyse |
Publications (1)
Publication Number | Publication Date |
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JP2013511702A true JP2013511702A (ja) | 2013-04-04 |
Family
ID=44059211
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JP2012539181A Pending JP2013511702A (ja) | 2009-11-20 | 2010-11-17 | 熱分析システムおよび熱分析方法 |
Country Status (6)
Country | Link |
---|---|
US (1) | US20120250723A1 (ja) |
EP (1) | EP2502057B1 (ja) |
JP (1) | JP2013511702A (ja) |
CN (1) | CN102713586A (ja) |
DE (1) | DE112010004495A5 (ja) |
WO (1) | WO2011060768A1 (ja) |
Cited By (2)
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KR20190029468A (ko) * | 2017-09-12 | 2019-03-20 | 에스펙 가부시키가이샤 | 열용량 측정 장치 및 열용량 측정 방법 |
JP2021515902A (ja) * | 2019-01-23 | 2021-06-24 | 深▲セン▼供電局有限公司Shenzhen Power Supply Bureau Co., Ltd. | 高温超伝導ケーブルの温度測定システム |
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US10107696B2 (en) | 2015-09-16 | 2018-10-23 | Alliance For Sustainable Energy, Llc | Methods and devices for electrochemical system analysis |
RU2651931C2 (ru) * | 2016-06-08 | 2018-04-24 | Общество с ограниченной ответственностью "Объединенная Компания РУСАЛ Инженерно-технологический центр" | Способ и устройство для определения состава электролита |
DE102018113412A1 (de) * | 2018-06-06 | 2019-12-12 | Netzsch - Gerätebau Gesellschaft mit beschränkter Haftung | Messanordnung und Verfahren für eine thermische Analyse einer Probe |
EP3870961B1 (en) * | 2018-10-22 | 2024-03-06 | Waters Technologies Corporation | High sample throughput differential scanning calorimeter |
IT202000014695A1 (it) | 2020-06-19 | 2021-12-19 | Duedi S R L | Apparecchiatura per l'analisi di leghe metalliche non ferrose e particolarmente per analisi di tipo 's.t.a.', sistema per il controllo della qualita' di leghe leggere comprendente tale apparecchiatura e metodo di funzionamento di tale apparecchiatura |
AT524363B1 (de) * | 2020-10-30 | 2022-06-15 | Anton Paar Gmbh | Messgerät mit elektrothermischem Wandler zum Einstellen eines thermischen Widerstandes, und Betriebsverfahren |
DE102022104400B3 (de) * | 2022-02-24 | 2022-10-06 | Netzsch - Gerätebau Gesellschaft mit beschränkter Haftung | Vorrichtung und Verfahren für eine thermische Analyse einer Probe |
EP4246109A1 (en) | 2022-03-16 | 2023-09-20 | Crino GmbH | Test system for at least one battery cell |
DE102022203563A1 (de) | 2022-04-08 | 2023-10-12 | Robert Bosch Gesellschaft mit beschränkter Haftung | Prüfaufbau |
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- 2010-11-17 WO PCT/DE2010/001350 patent/WO2011060768A1/de active Application Filing
- 2010-11-17 CN CN2010800523502A patent/CN102713586A/zh active Pending
- 2010-11-17 JP JP2012539181A patent/JP2013511702A/ja active Pending
- 2010-11-17 DE DE112010004495T patent/DE112010004495A5/de not_active Ceased
- 2010-11-17 EP EP10818070.4A patent/EP2502057B1/de active Active
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2012
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Also Published As
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WO2011060768A1 (de) | 2011-05-26 |
US20120250723A1 (en) | 2012-10-04 |
EP2502057A1 (de) | 2012-09-26 |
DE112010004495A5 (de) | 2012-09-06 |
EP2502057B1 (de) | 2020-01-01 |
CN102713586A (zh) | 2012-10-03 |
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