JP2013013394A - Kind of preparation method of electronic cigarette atomizing liquid - Google Patents

Kind of preparation method of electronic cigarette atomizing liquid Download PDF

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JP2013013394A
JP2013013394A JP2011235884A JP2011235884A JP2013013394A JP 2013013394 A JP2013013394 A JP 2013013394A JP 2011235884 A JP2011235884 A JP 2011235884A JP 2011235884 A JP2011235884 A JP 2011235884A JP 2013013394 A JP2013013394 A JP 2013013394A
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electronic cigarette
atomizing liquid
extract
minutes
aroma
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JP5752008B2 (en
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Junxiang Zheng
ジュンキシアング ゼング
Zhixuan Zheng
ジクアン ゼング
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    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
    • A24B15/303—Plant extracts other than tobacco
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/10—Devices using liquid inhalable precursors

Abstract

PROBLEM TO BE SOLVED: To provide a kind of preparation method of electronic cigarette atomizing liquid to eliminate shortcomings of electronic cigarette atomizing liquid comprising weak aroma and taste and short time for keeping the aroma.SOLUTION: There is provided a kind of preparation method of electronic cigarette atomizing liquid, atomizing liquid by putting tobacco leaves with 5-20% of electronic cigarette atomizing liquid amount into an extracting tank and adding a mixed solvent into the tank and soaking the tobacco leaves for 30-100 minutes; heating the mixture up to 40-60°C and extracting it with warm soak for 2-8 hours; filtering the extract and adding a cocoa bean extract with amount of 1-10% of the electronic cigarette atomizing liquid volume into the filtrate and stirring it for 20-40 minutes; and complementing the electronic cigarette atomizing liquid volume with 100% planning preparation with propanediol or polyglycol, and stirring them until mix uniformly to get the product. Natural aroma elements of a tobacco leaf enter the electronic cigarette atomizing liquid by the method to make the aroma and taste of the cigarette come practically from the tobacco leaf, make the aroma further close to the aroma of tobacco catering further to the smoking feeling of customers and make the time much longer for keeping the natural aroma in the electronic cigarette atomizing liquid.

Description

本発明は、化学工業製作技術領域に属する、一種の電子タバコの煙液製作方法に関する。 The present invention relates to a kind of electronic cigarette smoke production method belonging to the chemical industry production technical field.

電子タバコの煙液（又は電子煙霧化液と称される）は、現在一番流行しているタバコの代替製品である。電子タバコの煙液処方調合、製作プロセス及び保健機能等の面について、多くの文献又は特許報道があった。中国特許200910104922.6で公開された電子模擬タバコ煙霧化液は、25-90取り分のポリグリコール、9-50取り分のプロパンジオール及び0.3-52取り分の味わい調節剤で調合されており、典型的な香料エッセンス調合製品に属する。
中国特許200910310536.2で公開された電子模擬タバコ煙霧化液は、3-5%w/vタバコの葉抽出物、3-5% w/vタバコ香料エッセンス、0-3% w/vコチン、0.2-1% w/v分解防止剤、3-8% w/v増粘剤、5-10% w/v純水、50-70%プロパンジオール及び燐酸コデイン、クロルフェニラミンなどのほかの成分で配合されており、タバコの葉抽出物を使用しているが、依然としてタバコの味わいを模倣してタバコの葉抽出物と他の香料エッセンスで調合された製品である。
電子タバコでタバコを代替することを受け入れる人は日増しに多くなっているので、これらの電子タバコに使用される煙液の不足も日増しに著しくなる。喫煙者の普遍的な意見によって、電子タバコは、タバコと比べると、形状・手触りと煙霧等がタバコと相似していると感じられるが、香りと味わい等の面でタバコの感覚と大きな差異があり、特に各種の香料エッセンスで調合された製品に対して、喫煙者達はその香りと味わいに慣れ・受け入れにくい。そればかりか、現在電子タバコの煙液の香り成分は長期的に保留し難く、一番長くとも半年位で、「タバコ味」が薄くなるか又は殆どなくなり、この問題も普遍的に反映されている。これらの不足は、電子タバコの品質に大きく影響すると同時に、電子タバコの普及と流行を制約している。 Electronic cigarette smoke (or electronic atomizer) is currently the most popular tobacco replacement product. There have been many literature or patent reports on aspects such as the formulation of electronic cigarette smoke, the manufacturing process and health functions. The electronic simulated cigarette fumes published in Chinese Patent 200910104922.6, formulated with 25-90 portions of polyglycol, 9-50 portions of propanediol and 0.3-52 portions of taste modifier, is a typical fragrance essence. Belongs to formulated products.
Electronic simulated cigarette fumes published in China patent 200910310536.2 is 3-5% w / v tobacco leaf extract, 3-5% w / v tobacco fragrance essence, 0-3% w / v cochin, 0.2- 1% w / v decomposition inhibitor, 3-8% w / v thickener, 5-10% w / v pure water, 50-70% propanediol, codeine phosphate, chlorpheniramine and other ingredients Although it uses tobacco leaf extract, it is still a product formulated with tobacco leaf extract and other fragrance essences that mimics the taste of tobacco.
Since the number of people who accept to replace cigarettes with electronic cigarettes is increasing day by day, the shortage of smoke liquids used in these electronic cigarettes is also becoming increasingly common. According to the general opinion of smokers, electronic cigarettes appear to be similar to tobacco in shape, texture, and fog compared to tobacco, but there is a big difference from the sense of tobacco in terms of aroma and taste. Yes, especially for products formulated with various fragrance essences, smokers are not accustomed to accepting the scent and taste. In addition, the scent component of the smoke of electronic cigarettes is difficult to hold for a long time, and the “cigarette taste” becomes faint or almost disappeared at the longest around half a year, and this problem is universally reflected. Yes. These deficiencies greatly affect the quality of electronic cigarettes and at the same time limit the spread and popularity of electronic cigarettes.

本発明の目的は、電子タバコの煙液に存在する弱い香りと味わい及び短い香り保留時間等の不足に対して、これを改善する一種の電子タバコの煙液の製作方法を提供する。 An object of the present invention is to provide a method for producing a kind of electronic cigarette smoke liquid which improves the weak fragrance and taste, short fragrance retention time and the like present in the electronic cigarette smoke liquid.

この方法によって、タバコの葉での天然の香り成分を電子タバコの煙液に入らせて、これで電子タバコの煙液にある香りと味わいが殆どタバコの葉から来て、タバコの香りに一層似て、消費者の喫煙感覚に一層迎合するほか、電子タバコの煙液にある天然の香りが一層長くなる。   By this method, the natural scent component in the tobacco leaf is put into the smoke of the electronic cigarette, so that the scent and taste in the smoke of the electronic cigarette almost comes from the tobacco leaf, and the scent of the tobacco is further increased. Similarly, in addition to being more responsive to the consumer's smoking sensation, the natural scent of the electronic cigarette smoke is even longer.

本発明は下記の技術計画によって実施される。
計画通りに一定量の電子タバコの煙液を製作する。５-２０％ （w/v）電子タバコの煙液量(体積)のタバコの葉(重量)を取って抽出缶に投入し、調合された溶媒を抽出缶に投入してタバコの葉を30-100分間浸して、40-60℃に加熱して、2-8時間温熱浸漬抽出を行った。この抽出液を濾過して濾過液を得て、濾過液に1-10%（ w/v）電子タバコの煙液量のココア豆抽出物を入れて、20-40分間撹拌・混合してから、ポリグリコール又はプロパンジオールで100%製作計画の電子タバコの煙液体積に補充し、均一に撹拌・混合した後、製品を得る。 The present invention is implemented by the following technical plan.
Produce a certain amount of electronic cigarette smoke as planned. 5-20% (w / v) Tobacco leaf (weight) of electronic cigarette smoke volume (volume) is taken and put into an extraction can. Soaked for -100 minutes, heated to 40-60 ° C, and subjected to hot immersion extraction for 2-8 hours. This extract is filtered to obtain a filtrate, and 1-10% (w / v) e-cigarette smoke amount of cocoa bean extract is added to the filtrate and stirred and mixed for 20-40 minutes. The product is obtained after replenishing 100% production volume of electronic cigarette smoke liquid with polyglycol or propanediol and stirring and mixing uniformly.

上記溶媒の調合方法は、それぞれ30-80%電子タバコの煙液量のプロパンジオール及び/又はポリグリコールと0.1-0.5%のポリソルベート80を取って、この二者を20-40分間撹拌・混合することによって、均一に混合された溶媒を得ることである。   The above-mentioned solvent preparation method takes propanediol and / or polyglycol of 30-80% electronic cigarette smoke amount and 0.1-0.5% polysorbate 80, and the two are stirred and mixed for 20-40 minutes. To obtain a uniformly mixed solvent.

上記ココア豆抽出物の製作方法は、ココア豆を20-60メッシュに粉砕してから、中間層付き抽出缶に投入し、ココア豆粉重量の3-10倍の蒸留水を入れてココア豆粉を30-90分間浸し、加熱して80-90C°まで加温した後、保温して2-6時間抽出し、放出して抽出液を濾過する。こしかすを別の用途に保留し、濾過液を比重1.1-1.4のエキス剤に減圧・濃縮することによって、ココア豆抽出物を得る。   The above cocoa bean extract is made by pulverizing cocoa beans to 20-60 mesh, then putting them in an extraction can with an intermediate layer, and adding distilled water 3-10 times the weight of the cocoa bean flour. Is soaked for 30-90 minutes, heated to 80-90 ° C, kept warm, extracted for 2-6 hours, discharged and filtered. The cocoa bean extract is obtained by holding the kojikasu for another use and depressurizing and concentrating the filtrate to an extract having a specific gravity of 1.1-1.4.

上記プロパンジオール及びポリグリコール溶媒及びポリソルベート80はすべて薬用又は食用級で、プロパンジオール及びポリグリコールは単独に使用できると同時に、それに混合して使用しても良い。   The propanediol and polyglycol solvents and polysorbate 80 are all medicinal or edible grades, and propanediol and polyglycol can be used alone or in admixture.

ポリソルベート80を含むプロパンジオール又はポリグリコール溶媒を抽出液として、比較的に穏やかな条件の下で直接タバコの葉を抽出することによって、まずタバコの葉の香り成分を直接抽出液に入らせて、その次に、穏やかな条件の下で直接タバコの葉を抽出することによって、複雑なプロセス及び高温濃縮条件の下で一部分の揮発し易い又は温度に敏感なタバコの葉の損失と破壊を避けて、その上、他の良く使われる香り成分の溶媒と比べると、プロパンジオール又はポリグリコール等の溶媒の粘度が大きく、一定な保湿性を持つ等の特徴によって、香りの成分に対してより良い保留作用を持つ。
大量の顧客は、本発明の製品を使用した後、タバコの味わいに近いことを知り、これを反映して、彼らはこの製品がより好きで、それに、この製品は二年乃至三年貯蔵されても、香りが相変わらず良く保留される。 By extracting tobacco leaves directly under relatively mild conditions using propanediol or polyglycol solvent containing polysorbate 80 as an extract, first let the tobacco leaf fragrance component enter the extract directly, Then, by directly extracting tobacco leaves under mild conditions, avoid loss and destruction of some volatile or temperature sensitive tobacco leaves under complex process and high temperature concentration conditions. In addition, compared with other commonly used scent component solvents, propanediol or polyglycol and other solvents have a higher viscosity and have a certain moisturizing property, which makes them better reserved for scent components. Has an effect.
A large number of customers know that after using the product of the present invention, it is close to the taste of tobacco, reflecting this, they are more fond of this product, and this product has been stored for two to three years However, the scent is still well held.

実施例1: 計画通りに500リットルの電子タバコの煙液を製作する。50キログラムタバコの葉を計って、中間層付き抽出缶に投入して、それぞれ350リットルのプロパンジオールと1リットルのポリソルベート80を計り、ポリソルベート80をプロパンジオールに入れて30分間混合・撹拌し、この混合液を抽出缶に入れてタバコの葉を50分間浸漬してから、中間層に蒸気を通して50℃まで加熱・加温し、4時間保温・浸漬抽出を行った後、抽出液を放出し、これを濾過することによって、濾過液を得る。この濾過液に18キログラムのココア豆抽出物を入れて、30分間混合・撹拌してから、濾過液にプロパンジオールを入れて、製作計画の500リットルに補足した後、又35分間混合・撹拌することによって、上記の電子タバコの煙液を得る。 Example 1: Producing 500 liters of electronic cigarette smoke as planned. Weigh 50 kilograms of tobacco leaves, put them in an extraction can with an intermediate layer, measure 350 liters of propanediol and 1 liter of polysorbate 80, add polysorbate 80 to propanediol, and mix and stir for 30 minutes. Put the mixed solution in an extraction can and soak tobacco leaves for 50 minutes, then heat and warm to 50 ° C through steam through the middle layer, and after 4 hours of heat retention and immersion extraction, release the extract, By filtering this, a filtrate is obtained. Add 18 kilograms of cocoa bean extract to this filtrate, mix and stir for 30 minutes, then add propanediol to the filtrate to supplement 500 liters of the production plan, and then mix and stir again for 35 minutes Thus, the smoke liquid of the electronic cigarette is obtained.

実施例2：計画通りに500リットル電子タバコの煙液を製作する。50キログラムタバコの葉を計って、中間層付き抽出缶に投入して、まず1：1の比率でプロパンジオールとポリグリコール380リットルを計って混合してから、1.5リットルポリソルベート80を計り、ポリソルベート80をプロパンジオールとポリグリコール混合液に入れ、40分間混合・撹拌し、抽出缶に入れてタバコの葉を60分間浸してから、中間層に蒸気を通して60℃まで加熱・加温し、6時間保温・浸漬抽出を行った後、抽出液を放出し、これを濾過することによって、濾過液を得る。この濾過液に20キログラムココア豆抽出物を入れて、40分間を混合・撹拌し、濾過液にプロパンジオールを入れて、製作計画の500リットルに補足した後、又30分間混合・撹拌することによって、上記の電子タバコの煙液を得る。

Example 2: A 500 liter electronic cigarette smoke is produced as planned. Weigh 50 kilograms of tobacco leaves, put them in an extraction can with an intermediate layer, measure and mix 380 liters of propanediol and polyglycol at a 1: 1 ratio, then measure 1.5 liters of polysorbate 80, and measure polysorbate 80 In a mixed solution of propanediol and polyglycol, mixed and stirred for 40 minutes, put into an extraction can, soaked tobacco leaves for 60 minutes, then heated and heated to 60 ° C through steam through the middle layer and kept warm for 6 hours -After performing immersion extraction, the extract is discharged and filtered to obtain a filtrate. By adding 20 kilograms of cocoa bean extract to this filtrate and mixing and stirring for 40 minutes, adding propanediol to the filtrate and supplementing 500 liters of the production plan, and then mixing and stirring for 30 minutes To obtain the above-mentioned electronic cigarette smoke liquid.

Claims (4)

5-20%電子タバコの煙液量w/vのタバコの葉を計って、抽出缶に投入して、調合された溶媒を抽出缶に入れて、タバコの葉を30-100分間浸してから、40-60℃まで加温し、2-8時間保温・浸漬抽出を行った後、抽出液を濾過し、濾過液に1-10% w/v電子タバコの煙液量のココア豆抽出物を入れて、20-40分間混合・撹拌し、ついで、プロパンジオール又はポリグリコールで100%製作計画の電子タバコの煙液体積に補足し、均一に混合・撹拌することによって製品を得ることを特徴とする一種の電子タバコの煙液製作方法。 5-20% Electronic cigarette smoke amount w / v tobacco leaf is measured, put into an extraction can, the formulated solvent is put into the extraction can, and the tobacco leaf is soaked for 30-100 minutes After warming up to 40-60 ℃ and keeping warm and soaking for 2-8 hours, the extract is filtered, and the cocoa bean extract is 1-10% w / v e-cigarette smoke in the filtrate. , Mixed and stirred for 20-40 minutes, then supplemented with 100% production cigarette smoke volume with propanediol or polyglycol, and mixed and stirred to obtain a product A kind of electronic cigarette smoke production method. 前記の溶媒の調合方法が、それぞれ30-80%電子タバコの煙液体積量のプロパンジオール及び/又はポリグリコールと0.1-0.5%のポリソルベート80を計って、この二者を20-40分間混合・撹拌して、均一に混合された溶媒を得ることを特徴とする請求項１に記載の電子タバコの煙液製作方法。 The above-mentioned solvent blending method measures 30-80% e-cigarette smoke volume of propanediol and / or polyglycol and 0.1-0.5% polysorbate 80, and mixes the two for 20-40 minutes. The method for producing a smoke liquid for an electronic cigarette according to claim 1, wherein the solvent is stirred to obtain a uniformly mixed solvent. 上記ココア豆抽出物の製作方法は、ココア豆を20-60メッシュに粉砕してから、中間層付き抽出缶に投入し、ココア豆粉重量の3-10倍の蒸留水を入れてココア豆粉を30-90分間浸し、加熱して80-90C°まで加温した後、保温して2-6時間抽出し、放出して抽出液を濾過し、濾過液を比重1.1-1.4のエキス剤に減圧・濃縮することによって、ココア豆抽出物を得ることを特徴とする請求項１又は２に記載の電子タバコの煙液製作方法。 The above cocoa bean extract is made by pulverizing cocoa beans to 20-60 mesh, then putting them in an extraction can with an intermediate layer, and adding distilled water 3-10 times the weight of the cocoa bean flour. Soak for 30-90 minutes, heat to 80-90 ° C, keep warm, extract for 2-6 hours, discharge, filter the extract, and filter the filtrate to an extract with a specific gravity of 1.1-1.4 The method for producing a smoke solution for an electronic cigarette according to claim 1 or 2, wherein a cocoa bean extract is obtained by decompression and concentration. 上記プロパンジオール及びポリグリコール溶媒及びポリソルベート80がすべて薬用又は食用級で、プロパンジオール及びポリグリコールが単独に使用できると同時に、それに混合して使用しても良いことを特徴とする請求項１〜３のいずれかに記載の電子タバコの煙液製作方法。




The propanediol and polyglycol solvent and polysorbate 80 are all medicinal or edible grade, and propanediol and polyglycol can be used alone or at the same time, and may be used as a mixture. The method for producing smoke liquid for electronic cigarettes according to any one of the above.




JP2011235884A 2011-07-04 2011-10-27 A kind of electronic cigarette smoke production method Expired - Fee Related JP5752008B2 (en)

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