JP2010269342A - Method for selecting weld-material, and power generation plant - Google Patents
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本発明は、配管などの材質が異なる発電用プラント部材同士を接続する溶接継手部に適用される溶接材料を選定する方法に関する。 The present invention relates to a method for selecting a welding material to be applied to a welded joint that connects power generation plant members having different materials such as piping.
火力発電や原子力発電に用いられる圧力容器や配管には、低合金鋼(主に1〜2%Cr系鋼)や高Cr鋼(主に9〜12%Cr系鋼)が用いられる。使用温度や作用応力などの部材の使用条件と、材料の許容応力を考慮して、上記材料からなる部材が使用される場所が決定される。このようにして決定された各部材は、溶接により接続されるが、このとき、低合金鋼と高Cr鋼とを溶接する異材溶接継手部が必要となる。 Low alloy steel (mainly 1-2% Cr steel) and high Cr steel (mainly 9-12% Cr steel) are used for pressure vessels and piping used for thermal power generation and nuclear power generation. The location where the member made of the material is used is determined in consideration of the use conditions of the member such as the working temperature and the working stress and the allowable stress of the material. Each member determined in this way is connected by welding. At this time, a dissimilar weld joint for welding low alloy steel and high Cr steel is required.
異材溶接継手部には、一般にインコネル系溶接材料及びフェライト系(共金系)溶接材料が用いられる。インコネル系溶接材料は、溶接継手部と高Cr鋼との界面に脱炭層が形成されにくいため、継手部でのクリープ強度及び靭性が良好となる。しかし、インコネル系溶接材料を使用すると、熱膨張の差に起因する熱応力によって損傷が発生する可能性がある。また、インコネル系溶接材料は、フェライト系溶接材料と比較して高価である上、溶接効率が悪いために、溶接に要するコストが高くなる。一方、フェライト系溶接材料は、溶接効率が良く、熱応力が小さいという利点がある。しかし、溶接継手部に含有される炭素が高Cr鋼に移動し、溶接継手部/高Cr鋼界面の溶接継手部側に脱炭層が形成されやすくなる。脱炭層により、クリープ強度及び靭性の低下が懸念される。 Generally, an Inconel welding material and a ferrite (metal alloy) welding material are used for the dissimilar weld joint. Inconel-based welding materials are less likely to form a decarburized layer at the interface between the welded joint and high Cr steel, and therefore the creep strength and toughness at the joint are good. However, when an Inconel welding material is used, damage may occur due to thermal stress caused by a difference in thermal expansion. Inconel welding materials are more expensive than ferrite welding materials and have poor welding efficiency, which increases the cost required for welding. On the other hand, ferritic welding materials have the advantages of good welding efficiency and low thermal stress. However, the carbon contained in the weld joint moves to the high Cr steel, and a decarburized layer is easily formed on the weld joint side of the weld joint / high Cr steel interface. Due to the decarburized layer, the creep strength and toughness may be reduced.
特許文献1では、低合金鋼の開先面にインコネル系溶接材料を肉盛溶接し、次に裏当金を装着してインコネル系溶接材料を更に肉盛溶接した後に、開先加工を行って、低合金鋼とステンレス鋼とを溶接する方法が開示されている。 In Patent Document 1, after welding the Inconel welding material on the groove surface of the low alloy steel, and then mounting the backing metal and further overlay welding the Inconel welding material, the groove processing is performed. A method of welding low alloy steel and stainless steel is disclosed.
上述のように、インコネル系溶接材料とフェライト系溶接材料は、互いに相反する利点と欠点とを有する。そのため、溶接部材が使用される温度や使用時間といった環境、熱応力、コストなどを考慮して、適切な溶接材料を選択する必要がある。 As described above, the Inconel welding material and the ferrite welding material have advantages and disadvantages that are contradictory to each other. For this reason, it is necessary to select an appropriate welding material in consideration of the environment such as the temperature at which the welding member is used and the usage time, thermal stress, cost, and the like.
本発明は、上記課題に鑑みなされたものであり、異材溶接継手での脱炭層形成有無を予測して、部材の組合せや使用部位に応じた最適な溶接材料を選定する方法を提供する。 This invention is made | formed in view of the said subject, predicts the presence or absence of decarburization layer formation in a dissimilar material welded joint, and provides the method of selecting the optimal welding material according to the combination and use site | part of a member.
本発明の溶接材料の選定方法は、以下の工程を含む。
金属母材に含まれる各炭化物生成元素の所定温度における炭化物生成反応標準自由エネルギーの比率と、前記炭化物生成元素の濃度との積を合計した値を炭化物生成能パラメータと定義したときに、一の金属母材の炭化物生成能パラメータと、前記一の金属母材と材質が異なる別の金属母材の炭化物生成能パラメータとの差の絶対値を算出する。前記一の金属母材と前記別の金属母材とが溶接材料で溶接された部材の使用温度及び使用時間から、時効パラメータを算出する。予め作成された、脱炭層が形成される条件の領域と脱炭層が形成されない条件の領域とを炭化物生成能パラメータの差の絶対値と時効パラメータとで表したグラフにおいて、前記算出された炭化物生成能パラメータの差の絶対値と、前記算出された時効パラメータとの交点が、前記脱炭層が形成される条件の領域にある場合に、前記溶接材料としてインコネル系溶接材料を選定する。前記交点が、脱炭層が形成されない条件の領域にある場合に、前記溶接材料としてフェライト系溶接材料を選定する。
The method for selecting a welding material of the present invention includes the following steps.
When a value obtained by summing up the products of the carbide generation reaction standard free energy ratio at a predetermined temperature of each carbide generating element contained in the metal base material and the concentration of the carbide generating element is defined as the carbide generating ability parameter, An absolute value of a difference between a carbide generating ability parameter of the metal base material and a carbide forming ability parameter of another metal base material different from the one metal base material is calculated. An aging parameter is calculated from a use temperature and a use time of a member in which the one metal base material and the another metal base material are welded with a welding material. In the graph prepared in advance, in which the decarburized layer formation condition region and the decarburization layer formation condition region are represented by the absolute value of the difference in carbide generation ability parameter and the aging parameter, the calculated carbide generation Inconel-based welding material is selected as the welding material when the intersection between the absolute value of the difference between the performance parameters and the calculated aging parameter is in a region where the decarburized layer is formed. When the intersection is in a region where the decarburized layer is not formed, a ferrite-based welding material is selected as the welding material.
上記発明において、前記脱炭層が形成される条件の領域が、式(1):
L≧26.783−0.77812Δg …(1)
(但し、L:時効パラメータ、Δg:炭化物生成能パラメータの差の絶対値)
で表され、前記時効パラメータが、式(2):
L=(T+273)(20+log(t)) …(2)
(但し、T:部材が使用される温度(℃)、t:使用時間(時間))
で表され、前記算出された炭化物生成能パラメータの差の絶対値と、前記算出された時効パラメータとが、前記式(1)の関係を満たす場合に前記溶接材料としてインコネル系溶接材料を選定し、前記算出された炭化物生成能パラメータの差の絶対値と、前記算出された時効パラメータとが、前記式(1)の関係を満たさない場合に前記溶接材料としてフェライト系溶接材料を選定しても良い。
In the above invention, the region under which the decarburized layer is formed has the formula (1):
L ≧ 26.783-0.77812Δg (1)
(However, L: Aging parameter, Δg: Absolute value of the difference in carbide forming ability parameter)
The aging parameter is expressed by the following formula (2):
L = (T + 273) (20 + log (t)) (2)
(However, T: temperature at which the member is used (° C.), t: use time (hour))
Inconel welding material is selected as the welding material when the calculated absolute value of the difference in the carbide forming ability parameter and the calculated aging parameter satisfy the relationship of the formula (1). The ferrite welding material may be selected as the welding material when the absolute value of the difference in the calculated carbide forming ability parameter and the calculated aging parameter do not satisfy the relationship of the formula (1). good.
本発明者は、上述のように定義される2つの金属母材の炭化物生成能パラメータの差の絶対値と時効パラメータとが、2つの金属母材をフェライト系溶接材料で溶接した場合における脱炭層の形成状況と相関があることを見出した。溶接される金属母材の材質と、溶接部材が使用される環境(温度及び時間)とが判れば、上述の工程によって、金属母材の組合せ及び使用環境に応じて最適な溶接材料を選定できる。例えば、金属部材の組合せ毎に高温長時間での時効試験を実施して脱炭層の形成を確認する必要が無くなるため、最適な溶接材料を、容易かつ迅速に選定可能となる。 The inventor determined that the decarburized layer in the case where the absolute value of the difference between the carbide forming ability parameters of the two metal base materials defined as described above and the aging parameter are welded to each other with a ferritic welding material. It was found that there is a correlation with the formation status of. If the material of the metal base material to be welded and the environment (temperature and time) in which the welding member is used are known, the optimum welding material can be selected according to the combination of the metal base materials and the use environment by the above-described steps. . For example, since it is not necessary to confirm the formation of the decarburized layer by performing an aging test at a high temperature for a long time for each combination of metal members, it is possible to easily and quickly select an optimum welding material.
本発明の発電用プラントは、前記一の金属母材で作製されるプラント部材と、前記別の金属母材で作製されるプラント部材とが、上記の方法により選定された溶接材料を用いて溶接されたものとされる。 In the power plant according to the present invention, a plant member made of the one metal base material and a plant member made of the other metal base material are welded using the welding material selected by the above method. It is assumed that.
本発明の選定方法を用いると、最適な溶接材料を迅速に選定できる。例えば、本発明の選定方法を用いて、高温長時間の使用によりフェライト系溶接材料では脱炭層が発生しやすい条件である部位にのみ、インコネル系溶接材料を適用することができる。こうすれば、高価で溶接効率が悪いインコネル系溶接材料で形成された溶接継手部の数を最小限に抑えることができるため、材料コスト及び溶接コストが低減される。更には、例えば脱炭層に起因して発生する溶接継手部の破損によるトラブルを未然に防止することができるために、保守管理コストが低減される。 By using the selection method of the present invention, the optimum welding material can be selected quickly. For example, by using the selection method of the present invention, the Inconel-based welding material can be applied only to a portion where the decarburized layer is likely to be generated in the ferrite-based welding material due to the use at a high temperature for a long time. In this way, the number of welded joints formed of an inconel welding material that is expensive and has poor welding efficiency can be minimized, so that material costs and welding costs are reduced. Furthermore, for example, trouble due to breakage of a welded joint caused by a decarburized layer can be prevented in advance, so that maintenance management costs are reduced.
本発明によれば、金属母材の組合せと使用環境とから、フェライト系溶接材料及びインコネル系溶接材料のいずれが溶接継手部として最適であるかを、容易かつ迅速に判断できる。インコネル系溶接材料で形成された溶接継手部を、例えば発電用プラントの設計段階で、必要に応じて効率良く配置できるために、材料コスト及び溶接コストが低減できる上、保守管理コストも低減できる。 According to the present invention, it is possible to easily and quickly determine which of a ferritic welding material and an inconel welding material is optimal as a weld joint from the combination of metal base materials and the usage environment. For example, at the design stage of the power generation plant, the weld joint formed of the Inconel welding material can be efficiently arranged as necessary, so that material costs and welding costs can be reduced, and maintenance management costs can also be reduced.
本発明の溶接材料の選定方法の一実施形態を以下に説明する。
発電用プラントの圧力容器や配管といったプラント部材に使用される低合金鋼や高Cr鋼などの金属母材には、炭化物を生成する元素であるCr,Mo,W,V,Nbが含有される。
An embodiment of the welding material selection method of the present invention will be described below.
Metal base materials such as low alloy steel and high Cr steel used for plant members such as pressure vessels and piping of power generation plants contain Cr, Mo, W, V, and Nb, which are elements that generate carbides. .
Cr,Mo,W,V,Nbそれぞれの鋼中での炭化物生成反応の標準エネルギーΔG(cal/mol)は、式(3)〜(7)で表される。(「金属データブック」、日本金属学会編、1999年、p.151参照)
Cr: ΔG=−55550+56.06T …(3)
Mo: ΔG=−16100+19.27T …(4)
W: ΔG=−37000+34.58T …(5)
V: ΔG=−40400+28.07T …(6)
Nb: ΔG=−50520+31.875T …(7)
ただし、式(3)〜(7)において、Tは温度(K)である。
The standard energy ΔG (cal / mol) of the carbide formation reaction in each steel of Cr, Mo, W, V, and Nb is expressed by equations (3) to (7). (Refer to “Metal Data Book”, Japan Institute of Metals, 1999, p. 151)
Cr: ΔG = −55550 + 56.06T (3)
Mo: ΔG = −16100 + 19.27T (4)
W: ΔG = −37000 + 34.58T (5)
V: ΔG = −40400 + 28.07T (6)
Nb: ΔG = −50520 + 31.875T (7)
However, in Formula (3)-(7), T is temperature (K).
ここで、発電用プラントの使用環境温度に相当する温度500℃での各元素のΔGを、式(3)〜(7)から算出する。温度500℃における各元素のΔGの比を、式(8)に示す。
ΔGCr:ΔGMo:ΔGW:ΔGV:ΔGNb
=1.2:0.3:2.6:1.9:1.0 …(8)
Here, ΔG of each element at a temperature of 500 ° C. corresponding to the use environment temperature of the power generation plant is calculated from the equations (3) to (7). The ratio of ΔG of each element at a temperature of 500 ° C. is shown in Formula (8).
ΔG Cr : ΔG Mo : ΔG W : ΔG V : ΔG Nb
= 1.2: 0.3: 2.6: 1.9: 1.0 (8)
式(8)で示す比が、各元素の炭化物生成能(炭化物の形成しやすさ)を表す。金属母材中に含有される炭化物生成元素の濃度は、母材の材質により異なる。金属母材の炭化物生成能パラメータgは、式(9)で定義される。
g=1.2CCr+0.3CMo+1.0CW+1.9CV+2.6CNb …(9)
ただし、式(9)において、CCr、CMo、CW、CV、CNbはそれぞれ、金属母材中のCr、Mo、W、V、Nbの濃度(wt%)である。
The ratio shown by Formula (8) represents the carbide | carbonized_material production ability (easiness of formation of a carbide | carbonized_material) of each element. The concentration of the carbide generating element contained in the metal base material varies depending on the material of the base material. The carbide generating ability parameter g of the metal base material is defined by Expression (9).
g = 1.2C Cr + 0.3C Mo + 1.0C W + 1.9C V + 2.6C Nb ... (9)
However, in the formula (9), C Cr , C Mo , C W , C V , and C Nb are the concentrations (wt%) of Cr, Mo, W, V, and Nb in the metal base material, respectively.
2つの金属母材それぞれについて、式(9)を用いて炭化物生成能パラメータgを算出する。2つの金属母材の炭化物生成能パラメータgの差の絶対値を、Δgと定義する。 For each of the two metal base materials, the carbide generating ability parameter g is calculated using Equation (9). The absolute value of the difference between the carbide forming ability parameters g of the two metal base materials is defined as Δg.
次に、2つの金属母材が溶接されてプラント部材とされた場合に、プラント部材が使用される温度及び使用時間から、時効パラメータを算出する。時効パラメータLは、式(2)で表される。
L=(T+273)(20+log(t)) …(2)
ただし、式(2)において、Tはプラント部材が使用される温度(℃)、tは使用時間(時間)である。
Next, when two metal base materials are welded to form a plant member, an aging parameter is calculated from the temperature at which the plant member is used and the usage time. The aging parameter L is expressed by equation (2).
L = (T + 273) (20 + log (t)) (2)
However, in Formula (2), T is the temperature (degreeC) in which a plant member is used, and t is use time (hour).
ここで、脱炭層が形成される条件の領域と脱炭層が形成されない条件の領域とを、ΔgとLとの関係で表したグラフを、予め作成しておく。以下に、上記グラフの作成方法を説明する。
表1に、溶接される金属母材の鋼種と、溶接施工方法を示す。鋼種には、P122(11Cr−2W−0.4Mo−1Cu−Nb−V鋼)、P91(9Cr−1Mo−Nb−V鋼)、P23(2.25Cr−1.6W鋼)、P22(2.25Cr−1Mo鋼)を用いた。
上記金属母材の溶接には、表1に示すフェライト系溶接材料を用いた。2種類の母材を溶接した後、表1に示す温度条件で2時間の後熱処理を実施し、試験片を得た。溶接直後及び後熱処理後の試験片について、浸透探傷試験(PT)、磁気探傷試験(MT)、超音波探傷試験(UT)、放射線探傷試験(RT)を実施し、溶接不良が無いことを確認した。
Here, a graph is created in advance in which the region of the condition where the decarburized layer is formed and the region of the condition where the decarburized layer is not formed are represented by the relationship between Δg and L. Below, the preparation method of the said graph is demonstrated.
Table 1 shows the steel type of the metal base material to be welded and the welding method. Steel types include P122 (11Cr-2W-0.4Mo-1Cu-Nb-V steel), P91 (9Cr-1Mo-Nb-V steel), P23 (2.25Cr-1.6W steel), P22 (2. 25Cr-1Mo steel).
Ferrite welding materials shown in Table 1 were used for welding the metal base material. After welding the two types of base materials, post-heat treatment was performed for 2 hours under the temperature conditions shown in Table 1 to obtain test pieces. Perform penetration testing (PT), magnetic testing (MT), ultrasonic testing (UT), and radiation testing (RT) on the test specimens immediately after welding and after heat treatment to confirm that there are no welding defects. did.
上記試験片を溶接面に対して垂直に切断し、複数の観察用試料を作製した。観察用試料について、電気炉を用いて、表2示す条件で時効試験を実施した。時効試験後、溶接面周辺部を研磨し、脱炭層の生成状況を光学顕微鏡で観察した。 The test piece was cut perpendicular to the weld surface to produce a plurality of observation samples. About the sample for observation, the aging test was implemented on the conditions shown in Table 2 using the electric furnace. After the aging test, the periphery of the weld surface was polished, and the state of formation of the decarburized layer was observed with an optical microscope.
図1は、時効試験によって脱炭層が形成された試験片と、脱炭層が形成されなかった試験片とを、ΔgとLとの関係でプロットしたグラフである。同図において、横軸は炭化物生成能パラメータの差の絶対値Δg、縦軸は時効パラメータLである。図1に斜線で示された領域が、脱炭層が形成される条件の領域(脱炭層形成領域)とされる。脱炭層が形成されない条件の領域、すなわち、図1で脱炭層形成領域以外の領域が、無脱炭層領域とされる。図1において、脱炭層形成領域は、式(1)で表される。
L≧26.783−0.77812Δg …(1)
FIG. 1 is a graph in which a test piece in which a decarburized layer is formed by an aging test and a test piece in which a decarburized layer is not formed are plotted in relation to Δg and L. In the figure, the horizontal axis represents the absolute value Δg of the difference between the carbide forming ability parameters, and the vertical axis represents the aging parameter L. A region indicated by hatching in FIG. 1 is a region (decarburized layer forming region) under a condition for forming a decarburized layer. A region under a condition where the decarburized layer is not formed, that is, a region other than the decarburized layer forming region in FIG. 1 is defined as a non-decarburized layer region. In FIG. 1, the decarburized layer forming region is represented by Formula (1).
L ≧ 26.783-0.77812Δg (1)
図1に例示されるグラフにおいて、上述のように算出した溶接される2つの金属母材のΔgと、時効パラメータLとの交点が、脱炭層形成領域にあるか、無脱炭層領域にあるかを判定する。交点が脱炭層形成領域にある場合は、2つの金属母材を溶接する溶接材料として、インコネル系溶接材料(例えば、WEL MIG 82)を選定する。交点が無脱炭層領域にある場合は、溶接材料としてフェライト系溶接材料を選定する。 In the graph illustrated in FIG. 1, whether the intersection between Δg of the two metal base materials to be welded calculated as described above and the aging parameter L is in the decarburized layer formation region or the non-decarburized layer region. Determine. When the intersection is in the decarburized layer forming region, an Inconel welding material (for example, WEL MIG 82) is selected as a welding material for welding two metal base materials. When the intersection is in the non-decarburized layer region, a ferrite-based welding material is selected as the welding material.
あるいは、式(1)を用いて、溶接材料を選定することも可能である。
溶接される2つの金属母材のΔgを、式(1)の右辺に代入して、数値を算出する。この数値と式(2)から算出されたLとが式(9)の関係を満たす場合、2つの金属母材を溶接する溶接材料として、インコネル系溶接材料を選定する。上述のように求めた式(1)の右辺の数値と式(2)から求めたLとが式(1)の関係を満たさない場合は、溶接材料としてフェライト系溶接材料を選定する。
Or it is also possible to select a welding material using Formula (1).
A numerical value is calculated by substituting Δg of two metal base materials to be welded into the right side of the equation (1). When this numerical value and L calculated from Equation (2) satisfy the relationship of Equation (9), an Inconel welding material is selected as a welding material for welding two metal base materials. When the numerical value on the right side of Equation (1) obtained as described above and L obtained from Equation (2) do not satisfy the relationship of Equation (1), a ferrite-based welding material is selected as the welding material.
以上のように、2つの金属母材の材質とプラント部材の使用条件(温度、時間)とが判れば、図1に例示される脱炭層形成領域を図示したグラフや、式(1)に例示される脱炭層形成領域を表した式を用いて、2つの金属母材を連結する溶接継手部に最適な溶接材料を選定することができる。 As described above, if the material of the two metal base materials and the use conditions (temperature, time) of the plant member are known, a graph illustrating the decarburized layer forming region illustrated in FIG. An optimum welding material can be selected for the welded joint portion that connects the two metal base materials using the formula representing the decarburized layer forming region.
Claims (3)
前記一の金属母材と前記別の金属母材とが溶接材料で溶接された部材の使用温度及び使用時間から、時効パラメータを算出し、
予め作成された、脱炭層が形成される条件の領域と脱炭層が形成されない条件の領域とを炭化物生成能パラメータの差の絶対値と時効パラメータとで表したグラフにおいて、前記算出された炭化物生成能パラメータの差の絶対値と、前記算出された時効パラメータとの交点が、前記脱炭層が形成される条件の領域にある場合に、前記溶接材料としてインコネル系溶接材料を選定し、
前記交点が、脱炭層が形成されない条件の領域にある場合に、前記溶接材料としてフェライト系溶接材料を選定する溶接材料の選定方法。 When a value obtained by summing up the products of the carbide generation reaction standard free energy ratio at a predetermined temperature of each carbide generating element contained in the metal base material and the concentration of the carbide generating element is defined as the carbide generating ability parameter, Calculate the absolute value of the difference between the carbide generating capacity parameter of the metal base material and the carbide generating capacity parameter of another metal base material different from the one metal base material,
From the use temperature and use time of the member in which the one metal base material and the another metal base material are welded with a welding material, an aging parameter is calculated,
In the graph prepared in advance, in which the decarburized layer formation condition region and the decarburization layer formation condition region are represented by the absolute value of the difference in carbide generation ability parameter and the aging parameter, the calculated carbide generation When the intersection of the absolute value of the difference in the performance parameter and the calculated aging parameter is in the region of the conditions under which the decarburized layer is formed, an Inconel welding material is selected as the welding material,
A method for selecting a welding material, wherein a ferrite-based welding material is selected as the welding material when the intersection is in a region where a decarburized layer is not formed.
L≧26.783−0.77812Δg …(1)
(但し、L:時効パラメータ、Δg:炭化物生成能パラメータの差の絶対値)
で表され、
前記時効パラメータが、式(2):
L=(T+273)(20+log(t)) …(2)
(但し、T:部材が使用される温度(℃)、t:使用時間(時間))
で表され、
前記算出された炭化物生成能パラメータの差の絶対値と、前記算出された時効パラメータとが、前記式(1)の関係を満たす場合に前記溶接材料としてインコネル系溶接材料を選定し、
前記算出された炭化物生成能パラメータの差の絶対値と、前記算出された時効パラメータとが、前記式(1)の関係を満たさない場合に前記溶接材料としてフェライト系溶接材料を選定する請求項1に記載の溶接材料の選定方法。 The region under conditions where the decarburized layer is formed is the formula (1):
L ≧ 26.783-0.77812Δg (1)
(However, L: Aging parameter, Δg: Absolute value of the difference in carbide forming ability parameter)
Represented by
The aging parameter is the formula (2):
L = (T + 273) (20 + log (t)) (2)
(However, T: temperature at which the member is used (° C.), t: use time (hour))
Represented by
When the calculated absolute value of the difference between the carbide generating parameters and the calculated aging parameter satisfy the relationship of the formula (1), an Inconel welding material is selected as the welding material,
The ferrite-based welding material is selected as the welding material when the absolute value of the difference between the calculated carbide forming ability parameters and the calculated aging parameter do not satisfy the relationship of the formula (1). The welding material selection method described in 1.
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