JP2008510695A - フレーバー又はフレグランス成分又は組成物を炭水化物マトリックス中に導入する方法 - Google Patents
フレーバー又はフレグランス成分又は組成物を炭水化物マトリックス中に導入する方法 Download PDFInfo
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- JP2008510695A JP2008510695A JP2007526600A JP2007526600A JP2008510695A JP 2008510695 A JP2008510695 A JP 2008510695A JP 2007526600 A JP2007526600 A JP 2007526600A JP 2007526600 A JP2007526600 A JP 2007526600A JP 2008510695 A JP2008510695 A JP 2008510695A
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Abstract
Description
本発明は、カプセル化の分野に関する。本発明は、特に、揮発性成分又は組成物、例えばフレーバー又はフレグランス化合物、又はカプセル化による保護により利益を受け得る他の物質を、炭水化物を基礎とするマトリックス中に導入することに関する公知の方法の加工コスト及び安全性並びに最終製品の品質についての改善に関する。本発明は特に、固体のフレーバー又はフレグランス粒子状組成物の製造方法において、炭水化物材料の水溶液を製造し、前記溶液から水を蒸発させ、得られた濃縮溶液中に有効成分又は組成物を乳化させ、それをダイを介して冷媒中に押出してこの炭水化物/有効材料溶融物をガラス化し、そして最後に、このように得られた粒状組成物を乾燥させることを含む方法に関する。本発明にかかる方法は、冷却段階を、この溶融物を、特に選択された冷却手段、特に液体窒素又はその噴霧物と接触させるか、又は更には液体窒素で冷却された金属表面と接触させることにより行うことを特徴とする。
目下のところ驚くべきことに、以下の段階:
a)有効成分又は組成物と、少なくとも1種の炭水化物材料及び場合により乳化剤の水溶液を有するマトリックスとを有効な温度及び撹拌条件下で合し、そしてブレンドして、適切な湿分含有率を有するこれらの均質な溶融物を得る段階;
b)この均質な溶融物を、ダイを介して押出する段階;
c)この溶融物を冷却する段階;
d)得られた材料を、それがダイを出る際か又はこの溶融物を冷却した後に細断、切断、粉砕又は粉末化する段階;及び
e)場合により乾燥させる段階を含み、
段階c)の溶融物の冷却を、押出された材料と−25℃未満の温度を有する冷媒とを接触させることにより実施する、有効成分、更には「有効」、すなわちフレーバー又はフレグランス成分又は組成物と称される有効成分をカプセル化する方法を提供することにより、従来技術の方法が直面する欠点を解消した。
図1及び図2は、それぞれIPA、液体窒素中への押出を含む本発明にかかる方法により得られた生成物のうち、実施例3に記載された条件下で撮影された写真を示している。
本発明を、以下により詳細に説明する。
炭水化物材料は、マルトデキストリンを好ましくは30〜70質量%、特に好ましくは40〜60質量%有する。
本発明を以下の実施例においてより詳細に記載し、その際、温度は摂氏温度であり、省略形は当業者において慣用の意味を有する。
本発明による回分法
以下の成分を、示された割合で用いて、回分式法を使用して押出生成物を製造した。
マルトデキストリン18DE 9660 46.26
スクロース 8920 42.72
オレンジオイル 2100 10.06
レシチン 200 0.96
水 5200 −
26100 100.00
マルトデキストリン及びスクロースを水中に溶解させ、そして130℃に加熱して含水率を約6質量%に減らした。レシチンをオレンジオイル中に溶解させ、次いで撹拌しつつ混合して均一な溶融物を形成させた。この混合物を0.8mmの穴を有するダイプレートを介して、3バールの圧力下で、約30リットルの液体窒素を含有する受取容器中に浸漬させた0.5mmの穿孔を有するバスケット中に押出した。この押出を完了させた後に、このバスケット中に回収された低温ストランドをこの液体窒素浴から取り出して、乾燥器中に入れた。乾燥後に、1%の二酸化ケイ素を易流動化剤として添加した。この最終生成物は、フレーバー9.8質量%、湿分4.3%を含有し、かつ46℃のガラス転移温度を有していた。
本発明による連続法
以下の組成:
成分 質量部
スクロース 40
マルトデキストリン18DE 40
水 20
のシロップ溶液を、80℃で第1の熱交換器中に8.0kg/分の速度でポンプ輸送した。
比較例
実施例1に記載したものと同様の、それぞれオレンジオイル10%を含有する2つの20kgの炭水化物マトリックスの予備バッチを、回分法と同様に押出して液体窒素、又はイソプロピルアルコール(IPA)中に入れ、次いで乾燥させた。以下の工程は、実施例1で上述したものと同様であった。これらの最終生成物を比較した−これらは、同じものが生じ、かつオレンジオイルの香りは有しなかった。この最終生成物の分析によれば、湿分含有率、ガラス転移温度又はフレーバー含有率に関して押出冷却の2つの方法の差異は示されなかった。2種の冷却処理を用いて得られた試料間での表面形態の識別できる差異は、拡大撮影か又は走査型電子顕微鏡(SEM)により試験した際には見られなかった。
魚油粒子の製造
アラビアゴム20質量%水溶液を調製した。この溶液3.166kgと、水3.66kgとを、10バールまでの圧力に耐えるのに好適でありかつ底部上にダイ穴を備えた出口弁を有する槽中で混合した。この槽は、機械的撹拌器を備えるものであった。
Claims (29)
- 有効成分又は組成物をカプセル化する方法において、以下の段階:
a)有効成分又は組成物と、少なくとも1種の炭水化物材料及び場合により乳化剤の水溶液を有するマトリックスとを有効な温度及び撹拌条件下で合し、そしてブレンドして、適切な湿分含有率を有するこれらの均質溶融物を製造する段階;
b)この均質溶融物を、ダイを介して押出する段階;
c)この溶融物を冷却する段階;
d)得られた材料を、それがダイを出る際か又はこの溶融物を冷却した後に細断、切断、粉砕又は粉末化する段階;及び
e)場合により乾燥させる段階を含み、
段階c)の溶融物の冷却を、押出された材料と−25℃未満の温度を有する冷媒とを接触させることにより実施する方法。 - 冷媒が−50℃〜−200℃の温度を有する、請求項1に記載の方法。
- 冷媒が液体窒素である、請求項1に記載の方法。
- 押出温度が90〜130℃であり、かつ溶融した均質混合物を、それがダイを出る際に細断して、マトリックス担体材料と実質的に同じであるガラス転移温度Tgを有する生成物を提供する、請求項1に記載の方法。
- マトリックスが3〜12質量%の湿分を有する炭水化物溶融物からなる、請求項1に記載の方法。
- 全ての段階を連続的に実施し、かつ段階a)において形成された均質溶融物を、この連続法の段階a)の設計に適切に配置された2つの熱交換器により得る、請求項1に記載の方法。
- 炭水化物材料の水溶液を第1の熱交換器を介して濃縮してその水の量を減らし、そしてカプセル化されるべき有効材料と混合し、次いでこの混合物、すなわち炭水化物/有効材料混合物を第2の熱交換器の表面上を通過させ、押出されるべき前記混合物に所望の押出温度値をもたらす、請求項6に記載の方法。
- 第1の熱交換器が表面掃引式熱交換器である、請求項7に記載の方法。
- 第2の熱交換器が表面掻取式熱交換器である、請求項7に記載の方法。
- 炭水化物溶液を第1の熱交換器で105〜150℃の温度に加熱する、請求項7に記載の方法。
- 第1の熱交換器における溶液の平均滞留時間が1〜10分である、請求項7に記載の方法。
- 段階a)の水溶液がこの溶液の全質量に対して12〜40質量%の水を含有する、請求項6に記載の方法。
- 段階a)の水溶液を、出発材料を乾燥固体質量槽から混合槽及び加熱槽に搬送し、次いでこの加熱槽から多管式熱交換器を介してポンプ輸送し、この高温槽にループで返送することにより製造する、請求項6に記載の方法。
- 第1の熱交換器での濃縮段階の終盤での混合物が2〜11質量%の湿分含有率を有する、請求項7に記載の方法。
- 混合物の滞留時間が1分未満の高剪断ホモジナイザーにより、有効材料の混合を実施する、請求項7に記載の方法。
- 混合物を押出前に102〜135℃の温度に冷却する、請求項7に記載の方法。
- 押出段階を1×105〜6×105Paの圧力で実施する、請求項7に記載の方法。
- フレーバーもしくはフレグランス有効材料、ビタミン、酸化防止剤、栄養補助剤もしくはポリ不飽和脂肪酸、又はこれらの源の押出のための、請求項1から17までの何れか1項に記載の方法。
- 請求項1に記載の方法により得られ、かつ冷媒を実質的に有しない、有効成分又は組成物の押出されたデリバリーシステム。
- フレグランスもしくはフレーバー有効材料、ビタミン、酸化防止剤、栄養補助剤もしくはポリ不飽和脂肪酸、又はこれらの源の運搬のための、請求項19に記載の押出されたデリバリーシステム。
- 全ての段階を連続的に実施し、かつ段階a)で形成された均質溶融物を、この連続法の段階a)の設計に適切に配置された2つの熱交換器により得て、その際、炭水化物材料の水溶液を第1の熱交換器を介して濃縮してこの溶液中の水の量を減らして、そしてカプセル化されるべき有効材料と混合し、次いで、この混合物、すなわち炭水化物溶液/有効材料混合物を第2の熱交換器の表面上を通過させ、押出されるべき前記混合物に所望の押出温度値をもたらす方法により得られる、請求項19に記載の押出されたデリバリーシステム。
- ショ糖か又はショ糖誘導体のマトリックスを有する、請求項19に記載の押出されたデリバリーシステム。
- マトリックスが、スクロース、グルコース、ラクトース、レブロース、フルクトース、マルトース、リボース、デキストローズ、イソマルト、ソルビトール、マンニトール、キシリトール、ラクチトール、マルチトール、ペンタトール、アラビノース、ペントース、キシロース、ガラクトース、水素化されたデンプン水解物、マルトデキストリン、STABILITE(R)、寒天、カラゲナン、ゴム、ポリデキストローズ、並びにこれらの誘導体及び混合物からなる群から選択された、請求項22に記載の押出されたデリバリーシステム。
- マトリックスがマルトデキストリンか又はマルトデキストリン混合物と、スクロース、グルコース、ラクトース、レブロース、マルトース、フルクトース、イソマルト、ソルビトール、マンニトール、キシリトール、ラクチトール、マルチトール及び水素化トウモロコシシロップを有する群から選択された少なくとも1種の材料から形成された、請求項22に記載の押出されたデリバリーシステム。
- マトリックスが、場合により20よりも小さいDE当量を有するマルトデキストリンを有する、請求項22に記載の押出されたデリバリーシステム。
- 有効成分として請求項20に記載の押出されたデリバリーシステムを有する消費者製品。
- フレーバー付与された組成物か又はフレーバー付与用組成物、チューインガムか又は咀嚼が必要な軟質菓子、アイスクリーム、ビスケット、医薬組成物か又は練り歯磨の形である、請求項26に記載の消費者製品。
- ポリ不飽和脂肪酸を有する組成物の形である、請求項26に記載の消費者製品。
- 賦香された組成物か又は賦香用組成物、石鹸、化粧品調製物、消臭剤か又は固体界面活性剤もしくは洗浄用製品の形である、請求項26に記載の消費者製品。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
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EP04104014A EP1627573A1 (en) | 2004-08-20 | 2004-08-20 | A process for the incorporation of a flavor or fragrance ingredient or composition into a carbohydrate matrix |
US60395404P | 2004-08-23 | 2004-08-23 | |
PCT/IB2005/002412 WO2006038067A1 (en) | 2004-08-20 | 2005-08-12 | Process for the incorporation of a flavor or fragrance ingredient or composition into a carbohydrate matrix |
Publications (2)
Publication Number | Publication Date |
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JP2008510695A true JP2008510695A (ja) | 2008-04-10 |
JP2008510695A5 JP2008510695A5 (ja) | 2008-08-21 |
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JP2007526600A Pending JP2008510695A (ja) | 2004-08-20 | 2005-08-12 | フレーバー又はフレグランス成分又は組成物を炭水化物マトリックス中に導入する方法 |
Country Status (7)
Country | Link |
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US (1) | US20070128234A1 (ja) |
EP (2) | EP1627573A1 (ja) |
JP (1) | JP2008510695A (ja) |
CN (1) | CN101005771B (ja) |
BR (1) | BRPI0514389A (ja) |
RU (1) | RU2007110176A (ja) |
WO (1) | WO2006038067A1 (ja) |
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Publication number | Publication date |
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CN101005771B (zh) | 2011-09-14 |
BRPI0514389A (pt) | 2008-06-10 |
RU2007110176A (ru) | 2008-09-27 |
WO2006038067A1 (en) | 2006-04-13 |
EP1781121A1 (en) | 2007-05-09 |
CN101005771A (zh) | 2007-07-25 |
EP1627573A1 (en) | 2006-02-22 |
US20070128234A1 (en) | 2007-06-07 |
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