JP2000329619A - Apparatus for measuring temperature of fluid - Google Patents
Apparatus for measuring temperature of fluidInfo
- Publication number
- JP2000329619A JP2000329619A JP11136927A JP13692799A JP2000329619A JP 2000329619 A JP2000329619 A JP 2000329619A JP 11136927 A JP11136927 A JP 11136927A JP 13692799 A JP13692799 A JP 13692799A JP 2000329619 A JP2000329619 A JP 2000329619A
- Authority
- JP
- Japan
- Prior art keywords
- thermometer
- fluid
- temperature
- protecting pipe
- temperature measuring
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Measuring Temperature Or Quantity Of Heat (AREA)
Abstract
Description
【０００１】[0001]
【発明の属する技術分野】本発明は、流体の温度測定装
置、詳しくは温度計を保護しながら精度よく温度を測定
する部分に用いる温度測定装置に関する。さらには、該
温度測定装置を用いた温度測定方法および石油製品の製
造方法に関する。BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a temperature measuring device for a fluid, and more particularly to a temperature measuring device used for a portion for accurately measuring a temperature while protecting a thermometer. Further, the present invention relates to a temperature measuring method using the temperature measuring device and a method for producing a petroleum product.
【０００２】[0002]
【従来の技術】石油精製工業における流動接触分解装置
のライザー（上昇流反応管）内部では気体として水蒸
気、油蒸気、固体として触媒、液体として原料油の三相
流体が１５ｍ／ｓｅｃ〜３０ｍ／ｓｅｃという高速で流
れている。従来は、分解反応の制御は、ライザー末端に
設置されたディスエンゲージャー（分離塔、旧来の呼び
方は反応塔）に設置された温度計によって行われてい
た。ここでは触媒と反応生成物を分離するため内部流速
はｌｍ／ｓｅｃ程度と遅い。しかし、流動接触分解装置
の触媒は近年急速に改善され必要反応時間が０．１秒か
ら２秒と短縮されてきた。これは、ライザー部分で反応
が完結するため、これを制御する必要性を意味してい
る。ライザー部分の反応を監視し、制御するにはライザ
ー内部に温度測定装置を設置し、直接内部三相流体の温
度を測定する必要がある。しかし、上記条件のように高
速で流体が流れ、かつ三相流体では下記の二つの問題が
有り、そのような温度測定装置は設置できなかった。2. Description of the Related Art Inside a riser (upflow reaction tube) of a fluid catalytic cracking unit in the petroleum refining industry, a three-phase fluid of steam as a gas, an oil vapor, a catalyst as a solid, and a raw oil as a liquid is 15 m / sec to 30 m / sec. It flows at a high speed. Conventionally, the decomposition reaction has been controlled by a thermometer installed in a disengager (separation tower, conventionally called a reaction tower) installed at the end of the riser. Here, the internal flow rate is as low as about lm / sec in order to separate the catalyst and the reaction product. However, the catalyst of the fluid catalytic cracking apparatus has been rapidly improved in recent years, and the required reaction time has been reduced from 0.1 seconds to 2 seconds. This means that the reaction is completed at the riser portion and that it is necessary to control the reaction. In order to monitor and control the reaction of the riser section, it is necessary to install a temperature measuring device inside the riser and directly measure the temperature of the internal three-phase fluid. However, a fluid flows at a high speed under the above-mentioned conditions, and a three-phase fluid has the following two problems, and such a temperature measuring device cannot be installed.
【０００３】問題点の１つは、通常流体中では温度計の
周辺でカルマン渦が出来やすく、これによる温度計の共
振、折損が起こることがある。そこでこのカルマン渦発
生条件の計算をして温度計の共振を防止する設計を行っ
ている。しかし、このカルマン渦発生条件の計算はせい
ぜい２相流体までの経験・知見が有るのみで三相流体に
ついては正確に温度計の共振を防止する設計を行うこと
は難しいのが現状である。あるいは、これを防止しよう
とすると通常の温度計より非常に太い温度計が必要とな
り、温度計の精度、流体抵抗など他の面での不都合が生
じてくる。問題点の２つ目は、高速で流れる触媒は硬度
が高く、研磨剤に近いので通常の金属（ステンレス鋼
等）では１年以内に磨耗して破損してしまう。本発明者
らは実際に温度計表面のステンレス鋼を硬度化処理して
磨耗試験を実施したが１年も寿命はなかった例がある。One of the problems is that a Karman vortex is likely to be formed around a thermometer in a normal fluid, which may cause resonance and breakage of the thermometer. Therefore, a design is made to calculate the Karman vortex generation conditions and prevent the thermometer from resonating. However, the calculation of the Karman vortex generation conditions has at most experience and knowledge up to a two-phase fluid, and it is difficult at present to design a three-phase fluid to accurately prevent resonance of a thermometer. Alternatively, to prevent this, a thermometer that is much thicker than a normal thermometer is required, and disadvantages in other aspects such as accuracy of the thermometer and fluid resistance arise. The second problem is that the catalyst flowing at a high speed has a high hardness and is close to an abrasive, so that a normal metal (such as stainless steel) is worn and damaged within one year. The inventors of the present invention have actually conducted a wear test by hardening stainless steel on the surface of a thermometer, but there is an example in which the life of the thermometer was not one year.
【０００４】上記問題の解決のため、米国石油精製協会
（ＮＰＲＡ）等で発表された例でも、サーモウェルの流
体接触部分の最小化、上流側への衝突緩衝板設置、温度
計先端を金属塊にする等のアイデアが提示されている
が、いずれも温度を正確に測定出来ない、又は寿命が極
端に短い等の欠点があり、流体中の温度の監視用温度計
としての性能は満足するものではなかった。また、流体
中の温度測定時のカルマン渦対策として特定の断面形状
をもつ保護管をつけたり（特開平１０−０６２２６
０）、保護管にコイルばねを取り付ける方法（特開平０
７−１９８４９９）などが提案されている。しかし、こ
れらの方法では温度計が温度測定対象物から隔離されて
しまい迅速に、かつ正確に温度を測定出来ないという欠
点があった。さらに、特開平１０−２２１１７８には保
護管と温度計の間隙部に電熱促進物質を充填したり、保
護管先端部に温度計の感温部付近を密着させて温度測定
の迅速性、正確性の向上をはかっている。しかし、保護
管の存在による温度測定の遅れや誤差の発生は完全には
解消できていない。特に、カルマン渦対策や耐摩耗性を
十分にするためには保護管を大きく、肉厚のものとせざ
るを得ず上記の欠点は顕著なものとなった。[0004] In order to solve the above-mentioned problem, even in an example published by the National Petroleum Refining Association (NPRA) or the like, minimization of the fluid contact portion of the thermowell, installation of the impact buffer plate on the upstream side, and the use of a thermometer with a metal lump However, there are drawbacks such as not being able to accurately measure temperature or having an extremely short life, and the performance as a thermometer for monitoring temperature in fluids is satisfactory. Was not. Also, as a countermeasure against Karman vortex at the time of measuring the temperature in a fluid, a protective tube having a specific cross-sectional shape is provided (Japanese Patent Laid-Open No. 10-06226).
0), a method of attaching a coil spring to a protection tube
7-198499). However, these methods have a disadvantage that the thermometer is isolated from the object to be measured and the temperature cannot be measured quickly and accurately. Further, Japanese Patent Application Laid-Open No. Hei 10-221178 discloses that the gap between the thermowell and the thermometer is filled with an electrothermal accelerating substance, or the temperature sensing part of the thermometer is brought into close contact with the tip of the thermowell to quickly and accurately measure the temperature. To improve. However, delays and errors in temperature measurement due to the presence of the protection tube have not been completely eliminated. In particular, in order to prevent Karman vortices and ensure sufficient wear resistance, the protective tube must be large and thick, and the above-mentioned disadvantages have become significant.
【０００５】[0005]
【発明が解決しようとする課題】本発明は、上記のよう
なカルマン渦対策や耐摩耗性を必要とし、かつ正確、迅
速に流体の温度を測定する温度測定装置、および該温度
測定装置を用いた温度測定方法および石油製品の製造方
法を提供することを目的とする。SUMMARY OF THE INVENTION The present invention provides a temperature measuring apparatus which requires the above-described measures against Karman vortex and abrasion resistance, and which accurately and quickly measures the temperature of a fluid. It is an object of the present invention to provide a method for measuring temperature and a method for producing petroleum products.
【０００６】[0006]
【課題を解決するための手段】本発明者は鋭意研究の結
果、温度計の側面に先端部を開口した保護管を配置した
温度測定装置が上記課題を解決できることを見出し、こ
の知見に基づいて本発明を完成したものである。すなわ
ち、本発明の要旨は下記のとおりである。Means for Solving the Problems As a result of earnest research, the present inventors have found that a temperature measuring device in which a protective tube having an open end on the side surface of a thermometer can solve the above-mentioned problems, and based on this finding. The present invention has been completed. That is, the gist of the present invention is as follows.
【０００７】（１） 温度計の側面に、先端部を開口し
た保護管を配置した流体の温度測定装置。 （２） 保護管の外側を耐摩耗性材料とした（１）記載
の温度測定装置。 （３） 温度計と保護管の間に充填剤を充填した（１）
または（２）記載の温度測定装置。(1) A temperature measuring device for a fluid in which a protective tube having an open end is disposed on the side surface of a thermometer. (2) The temperature measuring device according to (1), wherein the outside of the protective tube is made of a wear-resistant material. (3) Filler was filled between thermometer and protective tube (1)
Or the temperature measuring device according to (2).
【０００８】（４） 被測定流体が多相流体である
（１）〜（３）のいずれかに記載の温度測定装置。 （５） （１）〜（４）のいずれかに記載の温度測定装
置を用いて石油精製工業における接触分解装置のライザ
ー内部の温度を測定する方法。 （６） 石油精製装置により石油製品を製造する方法に
おいて、（１）〜（４）のいずれかに記載の温度測定装
置を石油精製装置内の流体の温度測定に用いることを特
徴とする石油製品の製造方法。(4) The temperature measuring device according to any one of (1) to (3), wherein the fluid to be measured is a multiphase fluid. (5) A method for measuring the temperature inside a riser of a catalytic cracking device in the petroleum refining industry using the temperature measuring device according to any one of (1) to (4). (6) A method for producing a petroleum product using a petroleum refining device, wherein the temperature measuring device according to any one of (1) to (4) is used for measuring the temperature of a fluid in the petroleum refining device. Manufacturing method.
【０００９】[0009]
【発明の実施の形態】まず、本発明の温度測定装置につ
いて説明する。本発明の保護管は先端部を開口した管状
のものであればよい。この保護管の内側に温度計を挿入
した構造になっている（図１参照）。温度計は、通常、
熱電対温度計、抵抗温度計が用いられるが、水銀温度
計、アルコール温度計などその先端部に測温部がある接
触型の温度計なら何でもよい。代表的な例として図１に
従って説明すれば、温度計１は測定対象流体等の外側か
ら、その先端部が測定対象流体に対し開口している保護
管２の内部に挿入された構造になっている。温度計１は
先端部に測温部があり、その先端部がほぼ保護管２の開
口部３と同じ位置となっていることが好ましい。保護管
から飛び出しているとその部分が摩耗を受けやすく、へ
こみすぎていると正確な温度測定ができなかったり、固
体や液体がそのへこんだ部分に触媒が巻き込まれ、この
部分に摩耗が発生することがある。また、保護管２と温
度計１との間隙は温度計１の挿入、取り外しができる範
囲で狭いほうが良い。広すぎると異物（触媒やタール分
など）が詰まったり、温度計が振動したり、温度測定が
不正確になったりする。DESCRIPTION OF THE PREFERRED EMBODIMENTS First, a temperature measuring device according to the present invention will be described. The protective tube of the present invention may be a tubular one having an open end. The structure is such that a thermometer is inserted inside the protective tube (see FIG. 1). Thermometers are usually
A thermocouple thermometer or a resistance thermometer is used, but any mercury thermometer, alcohol thermometer, or any other contact-type thermometer having a temperature measuring section at its tip may be used. If it demonstrates according to FIG. 1 as a typical example, the thermometer 1 will become the structure inserted into the inside of the protective tube 2 which the front-end | tip part opens to the fluid to be measured from the outside of the fluid to be measured. I have. It is preferable that the thermometer 1 has a temperature measuring portion at a tip portion, and the tip portion is located substantially at the same position as the opening 3 of the protective tube 2. If it protrudes from the protective tube, that part is susceptible to abrasion.If it is too dent, accurate temperature measurement cannot be performed, or the catalyst is caught in the dent part of solids or liquids, and this part wears out Sometimes. Further, the gap between the protective tube 2 and the thermometer 1 is preferably as small as possible within a range where the thermometer 1 can be inserted and removed. If it is too wide, foreign matter (catalyst, tar content, etc.) will be clogged, the thermometer will vibrate, and the temperature measurement will be inaccurate.
【００１０】本発明の被測定流体は通常の流体（単相
流、多相流）のほかに正確には流体とは呼べないかもし
れないが沸騰床や流動床あるいは粉体や粒子が振動して
いるものであってもよい。通常は、多相流体、特に固体
を含んだ多相流体が本発明の効果を発揮する被測定流体
として適している。その中でも、気体または液体と固体
の二相流体または気体、液体、固体の三相流体の場合に
最も有効である。また、カルマン渦への対策等が十分取
れることから高速の流体の測定に適している。気体、液
体、固体の三相流体の例としては石油精製工業における
接触分解装置に用いられる場合が挙げられる。接触分解
装置の反応部分であるライザーの温度測定は前記したよ
うに従来は難しかったが、本発明の温度測定装置により
好適に実施できる。The fluid to be measured according to the present invention may not be exactly called a fluid in addition to a normal fluid (single-phase flow, multi-phase flow), but a boiling bed, a fluidized bed, or powder or particles vibrates. May be available. Usually, a multi-phase fluid, particularly a multi-phase fluid containing a solid, is suitable as the fluid to be measured to exhibit the effects of the present invention. Among them, the two-phase fluid of gas or liquid and solid or the three-phase fluid of gas, liquid and solid is most effective. In addition, it is suitable for high-speed fluid measurement because sufficient measures against Karman vortices can be taken. Examples of gas, liquid, and solid three-phase fluids include those used in catalytic cracking equipment in the petroleum refining industry. As described above, conventionally, it has been difficult to measure the temperature of the riser, which is the reaction part of the catalytic cracking device, but it can be suitably performed by the temperature measuring device of the present invention.
【００１１】本発明の温度測定装置の保護管はその外側
を耐摩耗性材料とすることが好ましい。本発明の被測定
流体が多相流体、その中でも、気体または液体と固体の
二相流体または気体、液体、固体の三相流体の場合には
固体粒子による摩耗の影響が大きく、保護管を通常の材
料で作製すると寿命が短くなる。このような場合は、保
護管の外側を耐摩耗性の材料とすることが好適である。
耐摩耗性の材料としては、アルミナ、シリカ、シリカア
ルミナや耐火材、キャスタブルなどが挙げられる。特
に、耐熱性も要求される雰囲気下では耐火材、キャスタ
ブルなどが好適である。保護管の外側を耐摩耗性の材料
とすることが好適であるが保護管の構造的強度を考える
と内側は金属材料（ステンレス鋼など）とし、その外側
にキャスタブルなどをライニングしたものが好ましい。
この場合、内側の金属材料の外表面に凹凸を付けたり、
突起物を設置するなどして外側のキャスタブルなどのラ
イニングの施工を容易にし、剥離し難いものとすること
ができる（図２参照）。温度計等を摩耗させ易い流体の
測定の場合は温度計先端の直接流体の接触している部分
（通常は温度計のシース管の先端部分）の肉厚を増加し
て多少の減肉に耐えうるようにすることが好ましい。The outside of the protective tube of the temperature measuring device of the present invention is preferably made of a wear-resistant material. When the fluid to be measured of the present invention is a multi-phase fluid, and among them, a two-phase fluid of gas or liquid and a solid or a three-phase fluid of gas, liquid, and solid, the effect of abrasion due to solid particles is large, and a protective tube is usually used. When made of the above material, the life is shortened. In such a case, it is preferable that the outside of the protective tube is made of a wear-resistant material.
Examples of the wear-resistant material include alumina, silica, silica-alumina, refractory materials, castables, and the like. Particularly, in an atmosphere where heat resistance is required, a refractory material, castable, or the like is preferable. It is preferable that the outside of the protection tube is made of a wear-resistant material, but in consideration of the structural strength of the protection tube, it is preferable that the inside of the protection tube is made of a metal material (such as stainless steel) and the outside is lined with castables or the like.
In this case, the outer surface of the inner metal material may have irregularities,
Installation of a lining such as an outer castable can be facilitated by installing a projection or the like, and it can be made difficult to peel off (see FIG. 2). When measuring a fluid that easily wears a thermometer, etc., increase the wall thickness of the portion of the thermometer tip that is in direct contact with the fluid (usually the tip of the sheath tube of the thermometer) and withstand some thinning. Preferably.
【００１２】保護管と温度計との間隙は狭いほうが良い
が、あまり狭いと温度計の挿入、取り外しが難しくなっ
たり、時には保護管や温度計の温度変化による熱変形に
より保護管と温度計が固着してしまうことがある。そこ
で、この間隙はあまり狭くしないで温度計と保護管の間
に充填剤を充填することで、この間隙への異物の進入や
温度計の振動を防ぐことができる（図３参照）。充填剤
としては、通常、ガラス繊維、アスベスト、セラミック
ペーパー、布、紙、繊維、フィルム、など充填したとき
に多少弾力のあるものが用いられる。しかし、測定雰囲
気の温度等によってはその雰囲気に適合するものを用い
る必要がある。適当な充填材を選べば保護管への温度計
の挿入、取り出しが容易になる。The gap between the protective tube and the thermometer is preferably narrow. However, if the gap is too small, it becomes difficult to insert and remove the thermometer. It may stick. Therefore, by filling the space between the thermometer and the protective tube with a filler without making the gap too narrow, it is possible to prevent foreign substances from entering the gap and vibration of the thermometer (see FIG. 3). As the filler, those which are somewhat resilient when filled, such as glass fiber, asbestos, ceramic paper, cloth, paper, fiber, and film, are usually used. However, depending on the temperature of the measurement atmosphere or the like, it is necessary to use one that is compatible with the atmosphere. If an appropriate filler is selected, it becomes easy to insert and remove the thermometer from the protective tube.
【００１３】石油精製工業においては、高温、高圧の流
体を取り扱うことが多く、さらに、気液混合流体、気固
混合流体、気液固混合流体も多い。このため、石油精製
装置により石油製品を製造する方法において、本発明の
温度測定装置を用いて気液混合流体、気固混合流体、気
液固混合流体等の被測定流体の温度を測定し、石油精製
装置の運転条件を制御しながら効率よく石油製品を製造
することができる。特に、前述したように接触分解装
置、その中でも特に残油接触分解装置のライザー部の温
度測定は本発明の温度測定装置が非常に好適に用いら
れ、分解率、熱バランスなどの制御が容易になる。この
場合、接触分解装置のライザー部の温度測定装置の保護
管は比較的太く、長さは１２０ｍｍ程度であり、カルマ
ン渦に対する耐性が特によい条件と考えられる。In the petroleum refining industry, high-temperature, high-pressure fluids are often handled, and there are also many gas-liquid mixed fluids, gas-solid mixed fluids, and gas-liquid-solid mixed fluids. For this reason, in the method of manufacturing a petroleum product by a petroleum refining device, the temperature of a fluid to be measured such as a gas-liquid mixed fluid, a gas-solid mixed fluid, a gas-liquid-solid mixed fluid is measured using the temperature measuring device of the present invention, A petroleum product can be manufactured efficiently while controlling the operating conditions of the petroleum refinery. In particular, as described above, the temperature measurement device of the present invention is very suitably used for the temperature measurement of the riser section of the catalytic cracking device, particularly the residual oil catalytic cracking device as described above, and the control of the cracking rate, heat balance, etc. is easy. Become. In this case, the protection tube of the temperature measuring device in the riser portion of the catalytic cracking device is relatively thick and has a length of about 120 mm, which is considered to be a condition particularly excellent in resistance to Karman vortex.
【００１４】[0014]
【実施例】次に、本発明を実施例により具体的に説明す
るが、これらの実施例になんら制限されるものではな
い。 〔実施例１〕実際に、本発明の温度測定装置を流動接触
分解装置（ＦＣＣ）のライザー部へ適用し、正しい温度
指示値を示し正確な反応制御をしながら４年以上の寿命
を保って石油製品を製造しきた実績を保有しているので
これについて説明する。Next, the present invention will be described in detail with reference to examples, but the present invention is not limited to these examples. [Example 1] Actually, the temperature measuring device of the present invention was applied to a riser section of a fluid catalytic cracking device (FCC) to give a correct temperature indication value and perform accurate reaction control while maintaining a life of 4 years or more. We have a track record of producing petroleum products.
【００１５】ＦＣＣにおいては、近年の触媒活性の向上
によりライザーは移送管から反応管へと機能が変化して
きた。ライザー中では気液固の三相流体が高速で流れて
いるため、カルマン渦による共振を防止しかつ触媒の磨
耗により１年以上の寿命を持ち、流体温度を直接接触的
に、且つ精度良く測定できる温度計はなかった。そこ
で、本発明の温度測定装置を適用した。温度計保護管
は、ライザー内部へ突き出され、突き出し長さが内壁面
から１２０ｍｍとした。この長さは、通常２５ｍｍ以
上、とくに１００ｍｍ以上とすることが望ましい。ライ
ザー壁面における触媒の逆流による温度降下等の影響を
受けない長さとするためである。触媒による磨耗防止用
の保護管の外形は流体の条件等からカルマン渦発生条件
に対する計算を行い共振範囲に入らないよう設計する
（正確にはできないので安全率をみた形状とすることが
好ましい。）。温度計は先端の開口部を除き流体に晒さ
れていないので流体のカルマン渦からの応力はほとんど
受けない構造になっている。保護管の内側の材質はステ
ンレス鋼で５５０℃以上の耐熱性を持つ。保護管の外側
はアンカーで補強された耐磨耗性キャスタブルライニン
グとする。In the FCC, the function of the riser has been changed from a transfer tube to a reaction tube due to the recent improvement in catalytic activity. Gas-liquid-solid three-phase fluid flows in the riser at high speed, preventing resonance due to Karman vortex and having a life of one year or more due to wear of the catalyst. Directly and accurately measuring fluid temperature No thermometer was available. Then, the temperature measuring device of the present invention was applied. The thermometer protection tube was protruded into the riser, and the protruding length was 120 mm from the inner wall surface. This length is usually preferably at least 25 mm, particularly preferably at least 100 mm. This is because the length is not affected by the temperature drop or the like due to the backflow of the catalyst on the riser wall surface. The outer shape of the protection tube for preventing abrasion by the catalyst is designed so that it does not fall into the resonance range by calculating the Karman vortex generation condition from the fluid condition and the like (because it cannot be accurately made, it is preferable to have a shape that takes into account the safety factor). . Since the thermometer is not exposed to the fluid except for the opening at the tip, the thermometer has a structure that receives almost no stress from the Karman vortex of the fluid. The material inside the protection tube is stainless steel and has a heat resistance of 550 ° C. or more. The outside of the protection tube shall be a wear-resistant castable lining reinforced with anchors.
【００１６】温度計はステンレス鋼のシース管に封入さ
れた熱電対を用いた。温度計にセラミックペーパーを巻
き保護管に差し込むことによりセラミックペーパーを温
度計と保護管の間の充填材とした。温度計のライザー内
部への突き出し長さは保護管の突き出し長さとほぼ同じ
（内壁面から１２０ｍｍ）とする。測温部である温度計
先端部の軸に直角の面のみが保護管の先端の開口部にお
いて流体に露出している状態が好ましい。温度計先端部
は磨耗による肉厚低下に対応するためシース管の使用材
料を３ｍｍ程度の腐食代の余裕を見た厚みとした。この
温度測定装置をライザー内部に設置したＦＣＣを４年間
運転したところこの温度測定装置は十分な寿命を持って
いた。ＦＣＣの運転においては、ライザー部の反応温度
の測定が正確、迅速にでき、分解率等の目的因子を正確
に制御し、効率的な運転を達成することが出来た。As the thermometer, a thermocouple sealed in a stainless steel sheath tube was used. The ceramic paper was used as a filler between the thermometer and the protective tube by winding the ceramic paper around the thermometer and inserting it into the protective tube. The protruding length of the thermometer into the riser is almost the same as the protruding length of the protective tube (120 mm from the inner wall surface). It is preferable that only the surface perpendicular to the axis of the thermometer tip, which is the temperature measuring section, is exposed to the fluid at the opening at the tip of the protective tube. At the tip of the thermometer, the material used for the sheath tube was set to a thickness of about 3 mm with a margin for corrosion allowance of about 3 mm in order to cope with a decrease in wall thickness due to wear. When the FCC in which the temperature measuring device was installed inside the riser was operated for four years, the temperature measuring device had a sufficient life. In the operation of the FCC, the measurement of the reaction temperature in the riser section was performed accurately and quickly, and the target factors such as the decomposition rate were accurately controlled, so that the efficient operation was achieved.
【００１７】[0017]
【発明の効果】本発明の温度測定装置は、流体、特にＦ
ＣＣ装置のライザー内部のような高速の多相流体の温度
を正確、迅速に測定でき、温度計寿命も長い優れた温度
測定装置であることを示している。According to the temperature measuring apparatus of the present invention, a fluid, particularly F
This shows that it is an excellent temperature measuring device that can accurately and quickly measure the temperature of a high-speed multiphase fluid such as inside the riser of a CC device and has a long thermometer life.
【００１８】[0018]
【図１】 本発明の温度測定装置の概念図（断面図）。FIG. 1 is a conceptual diagram (cross-sectional view) of a temperature measuring device according to the present invention.
【図２】 保護管の外側を耐摩耗材で被覆した本発明の
温度測定装置の概念図（断面図）。FIG. 2 is a conceptual diagram (cross-sectional view) of the temperature measuring device of the present invention in which the outside of a protective tube is covered with a wear-resistant material.
【図３】 保護管と温度計の間に充填材を充填した本発
明の温度測定装置の概念図（断面図）。FIG. 3 is a conceptual diagram (cross-sectional view) of a temperature measuring device according to the present invention in which a filler is filled between a protective tube and a thermometer.
【００１７】[0017]
１：温度計 ２：保護管（断面内部は省略） ３：保護管先端の開口部 ４：耐摩耗材 ５：補強用アンカーボルト ６：充填材 ７：流体の境界壁 1: Thermometer 2: Protection tube (omitted inside section) 3: Opening of protection tube tip 4: Wear resistant material 5: Reinforcement anchor bolt 6: Filler 7: Boundary wall of fluid
Claims (6)
管を配置した流体の温度測定装置。1. A fluid temperature measuring device in which a protective tube having an open end is disposed on a side surface of a thermometer.
項１記載の温度測定装置。2. The temperature measuring device according to claim 1, wherein the outside of the protective tube is made of a wear-resistant material.
請求項１または２記載の温度測定装置。3. The temperature measuring device according to claim 1, wherein a filler is filled between the thermometer and the protective tube.
３のいずれかに記載の温度測定装置。4. The fluid to be measured is a multi-phase fluid.
3. The temperature measuring device according to any one of 3.
定装置を用いて石油精製工業における接触分解装置のラ
イザー内部の温度を測定する方法。5. A method for measuring the temperature inside a riser of a catalytic cracking unit in the petroleum refining industry using the temperature measuring device according to claim 1. Description:
方法において、請求項１〜４のいずれかに記載の温度測
定装置を石油精製装置内の流体の温度測定に用いること
を特徴とする石油製品の製造方法。6. A method for producing a petroleum product by a petroleum refining device, wherein the temperature measuring device according to claim 1 is used for measuring the temperature of a fluid in the petroleum refining device. Manufacturing method.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11136927A JP2000329619A (en) | 1999-05-18 | 1999-05-18 | Apparatus for measuring temperature of fluid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11136927A JP2000329619A (en) | 1999-05-18 | 1999-05-18 | Apparatus for measuring temperature of fluid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JP2000329619A true JP2000329619A (en) | 2000-11-30 |
Family
ID=15186827
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP11136927A Pending JP2000329619A (en) | 1999-05-18 | 1999-05-18 | Apparatus for measuring temperature of fluid |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP2000329619A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003065504A (en) * | 2001-08-22 | 2003-03-05 | Babcock Hitachi Kk | Fluidized bed device |
| CN110231107A (en) * | 2019-04-02 | 2019-09-13 | 马鞍山市嘉逸科技工贸有限责任公司 | A kind of combined type temperature sensors of high precision |
Citations (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS54163670U (en) * | 1978-05-08 | 1979-11-16 | ||
| JPS57192446U (en) * | 1981-06-01 | 1982-12-06 | ||
| JPS6046043U (en) * | 1983-09-06 | 1985-04-01 | 山里産業株式会社 | Furnace gas temperature measuring device |
| JPS60118738U (en) * | 1984-01-20 | 1985-08-10 | 石塚電子株式会社 | temperature detector |
| JPS61245951A (en) * | 1985-04-22 | 1986-11-01 | Kurosaki Refract Co Ltd | Nozzle for casting |
| JPS63253224A (en) * | 1987-04-10 | 1988-10-20 | Toa Nenryo Kogyo Kk | Fluid temperature measuring method for tower, tank, or the like |
| JPS6450331U (en) * | 1987-09-24 | 1989-03-28 | ||
| JPH02118235U (en) * | 1989-03-08 | 1990-09-21 | ||
| JPH03243838A (en) * | 1990-02-21 | 1991-10-30 | Toshiba Corp | Thermocouple device |
| JPH0628667U (en) * | 1992-09-07 | 1994-04-15 | バブコック日立株式会社 | Thermocouple protection tube |
| JPH07200066A (en) * | 1993-12-29 | 1995-08-04 | Yamatake Honeywell Co Ltd | Method and device for controlling changeover of compressor |
| JPH08240485A (en) * | 1995-03-06 | 1996-09-17 | Hitachi Ltd | Exhaust gas temperature measuring device of gas turbine |
| JPH09318459A (en) * | 1996-05-31 | 1997-12-12 | Ichirou Yachie | Protective tube for molten-metal temperature sensor |
| JPH10160585A (en) * | 1996-11-26 | 1998-06-19 | Tokyo Yogyo Co Ltd | Thermometer for molten metal |
-
1999
- 1999-05-18 JP JP11136927A patent/JP2000329619A/en active Pending
Patent Citations (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS54163670U (en) * | 1978-05-08 | 1979-11-16 | ||
| JPS57192446U (en) * | 1981-06-01 | 1982-12-06 | ||
| JPS6046043U (en) * | 1983-09-06 | 1985-04-01 | 山里産業株式会社 | Furnace gas temperature measuring device |
| JPS60118738U (en) * | 1984-01-20 | 1985-08-10 | 石塚電子株式会社 | temperature detector |
| JPS61245951A (en) * | 1985-04-22 | 1986-11-01 | Kurosaki Refract Co Ltd | Nozzle for casting |
| JPS63253224A (en) * | 1987-04-10 | 1988-10-20 | Toa Nenryo Kogyo Kk | Fluid temperature measuring method for tower, tank, or the like |
| JPS6450331U (en) * | 1987-09-24 | 1989-03-28 | ||
| JPH02118235U (en) * | 1989-03-08 | 1990-09-21 | ||
| JPH03243838A (en) * | 1990-02-21 | 1991-10-30 | Toshiba Corp | Thermocouple device |
| JPH0628667U (en) * | 1992-09-07 | 1994-04-15 | バブコック日立株式会社 | Thermocouple protection tube |
| JPH07200066A (en) * | 1993-12-29 | 1995-08-04 | Yamatake Honeywell Co Ltd | Method and device for controlling changeover of compressor |
| JPH08240485A (en) * | 1995-03-06 | 1996-09-17 | Hitachi Ltd | Exhaust gas temperature measuring device of gas turbine |
| JPH09318459A (en) * | 1996-05-31 | 1997-12-12 | Ichirou Yachie | Protective tube for molten-metal temperature sensor |
| JPH10160585A (en) * | 1996-11-26 | 1998-06-19 | Tokyo Yogyo Co Ltd | Thermometer for molten metal |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003065504A (en) * | 2001-08-22 | 2003-03-05 | Babcock Hitachi Kk | Fluidized bed device |
| JP4540272B2 (en) * | 2001-08-22 | 2010-09-08 | 中国電力株式会社 | Fluidized bed equipment |
| CN110231107A (en) * | 2019-04-02 | 2019-09-13 | 马鞍山市嘉逸科技工贸有限责任公司 | A kind of combined type temperature sensors of high precision |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CA1321826C (en) | Method and apparatus for measuring wall erosion | |
| EP1782041B1 (en) | Fouling and corrosion detector for process control industries | |
| US5022266A (en) | Passive acoustics process to monitor fluidized bed flow | |
| EP0385788B1 (en) | Passive acoustics method to monitor fluidized bed level | |
| US9212956B2 (en) | Ultrasonic temperature measurement device | |
| JP6140822B2 (en) | Method and apparatus for measuring cast iron and slag levels in a blast furnace | |
| US4103539A (en) | Non-destructive refractory erosion indicator | |
| US20080133152A1 (en) | Method And Apparatus For Fluid Leak Detection | |
| US10989328B2 (en) | Erosion monitoring system | |
| KR20110059870A (en) | Material withdrawal apparatus and methods of regulating material inventory in one or more units | |
| JP2000329619A (en) | Apparatus for measuring temperature of fluid | |
| WO1990013380A1 (en) | Process and equipment to determine disturbance variables when pouring molten metal from a container | |
| US5356219A (en) | Aerodynamic instrumentation probe | |
| US4460130A (en) | High temperature gas distribution injector | |
| JP4685497B2 (en) | Sintering machine exhaust gas flow measurement system | |
| JPS62156521A (en) | Measuring means for flow rate | |
| CN209591058U (en) | A kind of dust collector ash hopper ash tube blockage-prevention alarm device | |
| FI117451B (en) | Fluidised bed condition monitoring method | |
| JP2004163256A (en) | Apparatus for measuring behavior of high-temperature fluid | |
| Ellingson | Advances in nondestructive evaluation methods for inspection of refractory concretes | |
| JPS61118650A (en) | High temperature corrosion monitor apparatus | |
| JPS588447B2 (en) | Holding device for hopper internal measuring device | |
| SE466622B (en) | Arrangement for measuring changes in mass by detecting resonant frequency |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20060203 |
|
| RD02 | Notification of acceptance of power of attorney |
Free format text: JAPANESE INTERMEDIATE CODE: A7422 Effective date: 20060203 |
|
| A977 | Report on retrieval |
Free format text: JAPANESE INTERMEDIATE CODE: A971007 Effective date: 20090331 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20090630 |
|
| A521 | Written amendment |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20090821 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20091104 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20100406 |
|
| A02 | Decision of refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A02 Effective date: 20100831 |