IN2015DN01078A - - Google Patents
Info
- Publication number
- IN2015DN01078A IN2015DN01078A IN1078DEN2015A IN2015DN01078A IN 2015DN01078 A IN2015DN01078 A IN 2015DN01078A IN 1078DEN2015 A IN1078DEN2015 A IN 1078DEN2015A IN 2015DN01078 A IN2015DN01078 A IN 2015DN01078A
- Authority
- IN
- India
- Prior art keywords
- phosphonomethyl
- salts
- phosphonate
- diketopiperazine
- glycine
- Prior art date
Links
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical class OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 abstract 3
- XDDAORKBJWWYJS-UHFFFAOYSA-N glyphosate Chemical compound OC(=O)CNCP(O)(O)=O XDDAORKBJWWYJS-UHFFFAOYSA-N 0.000 abstract 2
- 230000003647 oxidation Effects 0.000 abstract 2
- 238000007254 oxidation reaction Methods 0.000 abstract 2
- -1 phosphonate ester salts Chemical class 0.000 abstract 2
- 125000004437 phosphorous atom Chemical group 0.000 abstract 2
- 239000011541 reaction mixture Substances 0.000 abstract 2
- 150000003839 salts Chemical class 0.000 abstract 2
- VRDOHMYPSMRJQK-UHFFFAOYSA-N 2-[4-(carboxymethyl)-2,5-dioxopiperazin-1-yl]acetic acid Chemical compound OC(=O)CN1CC(=O)N(CC(O)=O)CC1=O VRDOHMYPSMRJQK-UHFFFAOYSA-N 0.000 abstract 1
- 229910004856 P—O—P Inorganic materials 0.000 abstract 1
- ROKAXOISGALEAP-UHFFFAOYSA-N [2,5-dioxo-4-(phosphonomethyl)piperazin-1-yl]methylphosphonic acid Chemical compound OP(O)(=O)CN1CC(=O)N(CP(O)(O)=O)CC1=O ROKAXOISGALEAP-UHFFFAOYSA-N 0.000 abstract 1
- 239000003377 acid catalyst Substances 0.000 abstract 1
- 150000008064 anhydrides Chemical group 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 230000003301 hydrolyzing effect Effects 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 238000003786 synthesis reaction Methods 0.000 abstract 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds
- A01N57/20—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds containing acyclic or cycloaliphatic radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
- C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
- C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl
- C07F9/3813—N-Phosphonomethylglycine; Salts or complexes thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
- A01N59/20—Copper
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Biochemistry (AREA)
- Dentistry (AREA)
- Engineering & Computer Science (AREA)
- Plant Pathology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Inorganic Chemistry (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
The present invention is related to a new method for the synthesis of N- (phosphonomethyl)glycine or one of its derivatives selected from the group consisting of its salts, its phosphonate esters and its phosphonate ester salts, comprising the steps of: a) forming a reaction mixture comprising an acid catalyst, N,N'- bis(carboxymethyl)-2,5-diketopiperazine and a compound comprising one or more P-O-P anhydride moieties, wherein said moieties comprise one P atom at the oxidation state (+1 11) and the other P atom at the oxidation state (+1 11) or (+V), to form N,N'-bis(phosphonomethyl)-2,5- diketopiperazine, its dehydrated forms or their phosphonate esters; b) hydrolyzing the reaction mixture to form N-(phosphonomethyl)glycine or one of its derivatives selected from the group consisting of its salts, its phosphonate esters and its phosphonate ester salts.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP12176751 | 2012-07-17 | ||
| PCT/EP2013/065122 WO2014012988A1 (en) | 2012-07-17 | 2013-07-17 | Method for the synthesis of n-(phosphonomethyl)glycine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| IN2015DN01078A true IN2015DN01078A (en) | 2015-06-26 |
Family
ID=49000444
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IN1078DEN2015 IN2015DN01078A (en) | 2012-07-17 | 2013-07-17 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US9150599B2 (en) |
| EP (1) | EP2875034B1 (en) |
| CN (1) | CN104812763B (en) |
| BR (1) | BR112015000966B1 (en) |
| ES (1) | ES2632779T3 (en) |
| IN (1) | IN2015DN01078A (en) |
| PL (1) | PL2875034T3 (en) |
| RU (1) | RU2674023C9 (en) |
| WO (1) | WO2014012988A1 (en) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BR112015000990B1 (en) | 2012-07-17 | 2020-04-28 | Monsanto Technology Llc | METHOD FOR THE SYNTHESIS OF AN AMINO ALKYLENE PHOSPHONIC ACID OUSEUS PHOSPHATE ESTERS |
| CN104812765B (en) * | 2012-07-17 | 2017-06-06 | 斯特雷特马克控股股份公司 | Method for synthesizing α amino alkylidenyl phosphonic acids |
| IN2015DN01080A (en) | 2012-07-17 | 2015-06-26 | Straitmark Holding Ag | |
| BR112015000988A2 (en) | 2012-07-17 | 2017-06-27 | Straitmark Holding Ag | method for the synthesis of n-phosphonomethyliminodiacetic acid or derivatives thereof |
| CN112898338A (en) * | 2019-12-04 | 2021-06-04 | 利尔化学股份有限公司 | Glufosinate-ammonium intermediate and preparation method of glufosinate-ammonium |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3799758A (en) | 1971-08-09 | 1974-03-26 | Monsanto Co | N-phosphonomethyl-glycine phytotoxicant compositions |
| US3969398A (en) | 1974-05-01 | 1976-07-13 | Monsanto Company | Process for producing N-phosphonomethyl glycine |
| HU173170B (en) | 1974-06-27 | 1979-03-28 | Chinoin Gyogyszer Es Vegyeszet | Process for producing n-phosphonomethyl-glycine |
| US3927080A (en) | 1974-09-03 | 1975-12-16 | Monsanto Co | Process for producing N-phosphonomethyl glycine |
| IL48619A (en) | 1974-12-11 | 1978-04-30 | Monsanto Co | Process for the production of n-(phosphonomethyl)-glycine compounds |
| US4084499A (en) * | 1977-01-21 | 1978-04-18 | Moehlenpah Walter George | Apparatus for fabricating wood structures |
| CH647528A5 (en) | 1978-10-27 | 1985-01-31 | Bcap Biolog Chem Act Pat | PROCESS FOR THE PREPARATION OF N-phosphonomethylglycine. |
| US4624937A (en) | 1984-05-10 | 1986-11-25 | Monsanto Company | Process for removing surface oxides from activated carbon catalyst |
| US4804499A (en) * | 1985-09-23 | 1989-02-14 | Monsanto Company | Process for the preparation of N-substituted aminomethylphosphonic acids |
| HUP0002032A3 (en) | 1997-02-13 | 2001-12-28 | Monsanto Company Saint Louis | Method of preparing amino carboxylic acids |
| CA2339839A1 (en) | 1998-08-12 | 2000-02-24 | Monsanto Company | Continuous process for the preparation of n-(phosphonomethyl) iminodiacetic acid |
| US20020058834A1 (en) | 2000-06-01 | 2002-05-16 | Franczyk Thaddeus S. | Preparation of N-acyl amino carboxylic acids, amino carboxylic acids and their derivatives by metal-catalyzed carboxymethylation in the presence of a promoter |
| DE10130135A1 (en) * | 2001-06-22 | 2003-01-02 | Basf Ag | Process for the preparation of N-phosphonomethylglycine |
| BRPI0607713A2 (en) | 2005-04-01 | 2009-09-22 | Monsanto Technology Llc | methods for monitoring or detecting the conversion of n- (phosphonomethyl) iminodiacetic acid to n- (phosphonomethyl) glycine or other intermediate to n- (phosphonomethyl) glycine in the course of catalytically oxidizing n- (phosphonomethyl) iminodiacetic acid to an aqueous medium |
| CL2008003539A1 (en) | 2007-11-28 | 2009-07-03 | Process for the production of p4o6 that comprises mixing o2 or a mixture of o2 plus an inert gas and phosphorus where the product obtained is kept within a reaction unit at a temperature between 1600 and 2000 k for at least 1 second. | |
| ES2533731T3 (en) * | 2008-04-25 | 2015-04-14 | Straitmark Holding Ag | Process for the manufacture of aminoalkylene phosphonic acid |
| CN102216209B (en) | 2008-11-12 | 2013-10-30 | 斯特瑞马克控股公司 | Process for manufacture of P4O6 with high yield |
-
2013
- 2013-07-17 PL PL13750513T patent/PL2875034T3/en unknown
- 2013-07-17 EP EP13750513.7A patent/EP2875034B1/en active Active
- 2013-07-17 RU RU2015103316A patent/RU2674023C9/en active
- 2013-07-17 BR BR112015000966A patent/BR112015000966B1/en active IP Right Grant
- 2013-07-17 CN CN201380037315.7A patent/CN104812763B/en active Active
- 2013-07-17 WO PCT/EP2013/065122 patent/WO2014012988A1/en active Application Filing
- 2013-07-17 IN IN1078DEN2015 patent/IN2015DN01078A/en unknown
- 2013-07-17 ES ES13750513.7T patent/ES2632779T3/en active Active
- 2013-07-17 US US14/415,687 patent/US9150599B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| RU2674023C2 (en) | 2018-12-04 |
| EP2875034A1 (en) | 2015-05-27 |
| US9150599B2 (en) | 2015-10-06 |
| RU2674023C9 (en) | 2019-01-24 |
| BR112015000966B1 (en) | 2020-04-28 |
| RU2015103316A (en) | 2016-09-10 |
| WO2014012988A1 (en) | 2014-01-23 |
| CN104812763B (en) | 2016-11-23 |
| US20150175635A1 (en) | 2015-06-25 |
| EP2875034B1 (en) | 2017-05-03 |
| ES2632779T3 (en) | 2017-09-15 |
| CN104812763A (en) | 2015-07-29 |
| PL2875034T3 (en) | 2017-12-29 |
| BR112015000966A2 (en) | 2017-06-27 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| IN2015DN01078A (en) | ||
| TN2010000304A1 (en) | New processes | |
| EA201490361A1 (en) | Method of producing surfactant on the basis of fatty acylamido carboxylic acids | |
| CY1115336T1 (en) | COMPOSITION OF VORETZOMIBI | |
| MY163216A (en) | Compositions and methods for modulating fxr | |
| WO2008007392A3 (en) | Process for the preparation of tenofovir | |
| IN2015DN01081A (en) | ||
| EA200701810A1 (en) | ISOXAZOLINE DERIVATIVE AND A NEW METHOD FOR ITS PREPARATION | |
| MX2013005241A (en) | Crystalline 6,7-unsaturated-7-carbamoyl morphinane derivative, and method for producing same. | |
| TW200734316A (en) | Epoxide intermediate in the tamiflu synthesis | |
| TN2009000167A1 (en) | Crystalline potassium salt of lipoxin a4 analogs | |
| WO2012008785A3 (en) | Method for preparing ramalin | |
| IN2014CN03482A (en) | ||
| IN2015DN01082A (en) | ||
| EA201200498A1 (en) | A NEW METHOD FOR SYNTHESIS OF IVABRADIN AND ITS PHARMACEUTICALLY ACCEPTABLE ACID ADDITIVE SALTS | |
| EP3604273A3 (en) | Process for the synthesis of highly pure cationic surfactant products | |
| EA201170057A1 (en) | METHOD FOR PRODUCING SUBSTITUTED 2-AMINOTHIAZOLONES | |
| BR112012017447A2 (en) | heterocyclic carboxylic acid derivatives having a 2,5-substituted oxazolopyrimidine ring | |
| MY144746A (en) | Process for the preparation of agomelatine | |
| IN2015DN01080A (en) | ||
| EA201200123A1 (en) | A NEW METHOD FOR SYNTHESIS OF IVABRADIN AND ITS PHARMACEUTICALLY ACCEPTABLE ACID ADDITIVE SALTS | |
| MX341198B (en) | Branched polyesters with sulfonate groups. | |
| MX2013004193A (en) | Process for the preparation of 3-(6-amino-pyridin-3yl)-2-acrylic acid derivatives. | |
| MY147697A (en) | New process for the synthesis of ivabradine and addition salts thereof with a pharmaceutically acceptable acid | |
| JO2664B1 (en) | New addition salts of angiotensin converting enzyme inhibitors with NO donor acids, a process for their preparation and pharmaceutical compositions containing them |