IN2014CN04224A - - Google Patents
Info
- Publication number
- IN2014CN04224A IN2014CN04224A IN4224CHN2014A IN2014CN04224A IN 2014CN04224 A IN2014CN04224 A IN 2014CN04224A IN 4224CHN2014 A IN4224CHN2014 A IN 4224CHN2014A IN 2014CN04224 A IN2014CN04224 A IN 2014CN04224A
- Authority
- IN
- India
- Prior art keywords
- surfactant
- zeolite
- approximately
- hollow spherical
- preparation
- Prior art date
Links
- 229910021536 Zeolite Inorganic materials 0.000 abstract 3
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 abstract 3
- 239000004094 surface-active agent Substances 0.000 abstract 3
- 239000010457 zeolite Substances 0.000 abstract 3
- 238000002360 preparation method Methods 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- -1 cation quaternary ammonium salt Chemical class 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 239000000693 micelle Substances 0.000 abstract 1
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
- C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/40—Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
- B01J35/51—Spheres
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/30—Particle morphology extending in three dimensions
- C01P2004/32—Spheres
- C01P2004/34—Spheres hollow
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Catalysts (AREA)
Abstract
Provided are hollow spherical zeolite IM 5 and a preparation method therefor. A cation quaternary ammonium salt surfactant having a long carbon chain is added to an zeolite IM 5 preparation system where the molar ratio of a template agent/the surfactant is between approximately 0.3 and approximately 4.5 and hollow spherical zeolite IM 5 is generated via the micelle effect of the surfactant. The structure facilitates material mass transfer of a reaction process.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201110353565.4A CN103101926B (en) | 2011-11-10 | 2011-11-10 | Hollow ball-like IM-5 molecular sieve and preparation method thereof |
PCT/CN2012/001474 WO2013067765A1 (en) | 2011-11-10 | 2012-10-30 | Hollow spherical zeolite im-5 and preparation method therefor |
Publications (1)
Publication Number | Publication Date |
---|---|
IN2014CN04224A true IN2014CN04224A (en) | 2015-07-17 |
Family
ID=48288484
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
IN4224CHN2014 IN2014CN04224A (en) | 2011-11-10 | 2012-10-30 |
Country Status (7)
Country | Link |
---|---|
US (1) | US9248437B2 (en) |
EP (1) | EP2778136B1 (en) |
KR (1) | KR101915104B1 (en) |
CN (1) | CN103101926B (en) |
CA (1) | CA2855179C (en) |
IN (1) | IN2014CN04224A (en) |
WO (1) | WO2013067765A1 (en) |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103101927B (en) * | 2011-11-10 | 2014-12-31 | 中国石油化工股份有限公司 | IM-5 molecular sieve fiber and synthetic method thereof |
CN103193247A (en) * | 2013-03-09 | 2013-07-10 | 淮南师范学院 | Method for directly preparing composite porous zeolite molecular sieve ball |
CN104591220B (en) * | 2013-11-04 | 2016-08-17 | 中国石油化工股份有限公司 | A kind of hollow beta zeolite and preparation method thereof |
CN105585023B (en) * | 2014-10-22 | 2017-10-03 | 中国石油化工股份有限公司 | A kind of MCM 22 molecular sieves of cavity accumulation shape and preparation method thereof |
CN105585024B (en) * | 2014-10-22 | 2017-06-20 | 中国石油化工股份有限公司 | A kind of MCM 22/ZSM 35 coexisting molecular sieves of hollow accumulation shape and preparation method thereof |
KR101659709B1 (en) * | 2016-05-18 | 2016-09-26 | 주식회사 나노신소재 | Hollow-type aluminosilicate nanoparticle and preparation method thereof |
CN110407228B (en) * | 2018-04-26 | 2021-04-06 | 中国石油化工股份有限公司 | Method for synthesizing IM-5 molecular sieve |
CN111977668B (en) * | 2019-05-22 | 2022-08-30 | 中国石油天然气股份有限公司 | IM-5 molecular sieve and preparation method thereof |
CN112090443B (en) * | 2019-06-17 | 2023-03-10 | 中国石油化工股份有限公司 | Hydrodeoxygenation catalyst, application thereof and preparation method of cyclohexane |
CN110862098B (en) * | 2019-11-28 | 2023-01-20 | 上海华谊(集团)公司 | Method for synthesizing MCM-22 molecular sieve |
CN111617736B (en) * | 2020-04-20 | 2022-11-22 | 内江师范学院 | Cu-based-molecular sieve CO adsorbent with empty package structure and preparation method and application thereof |
CN111569827A (en) * | 2020-05-26 | 2020-08-25 | 北京泷涛环境科技有限公司 | Hollow sphere molecular sieve adsorbent and preparation method thereof |
CN113731351A (en) * | 2021-07-29 | 2021-12-03 | 浙江工业大学 | Method for preparing hollow spherical zeolite by modifying natural zeolite |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2754809B1 (en) * | 1996-10-21 | 2003-04-04 | Inst Francais Du Petrole | ZEOLITHE IM-5, ITS PREPARATION PROCESS AND ITS CATALYTIC APPLICATIONS |
FR2758810B1 (en) | 1997-01-24 | 1999-02-19 | Inst Francais Du Petrole | ZEOLITHE IM-5 DESALUMINATED |
FR2769919B1 (en) | 1997-10-16 | 1999-12-24 | Inst Francais Du Petrole | PROCESS FOR IMPROVING THE FLOW POINT OF PARAFFINIC LOADS WITH A ZEOLITHE IM-5 BASED CATALYST |
CN1093510C (en) * | 1998-09-25 | 2002-10-30 | 北京燕山石油化工公司研究院 | Process for synthesizing beta-zeolite |
US20030091504A1 (en) * | 2001-11-15 | 2003-05-15 | Gary Pasquale | Method for controlling synthesis conditions during molecular sieve synthesis using combinations of quaternary ammonium hydroxides and halides |
US7276224B2 (en) * | 2002-06-11 | 2007-10-02 | Regents Of The University Of Minnesota | Synthesis of nanoporous particles |
US7799128B2 (en) * | 2008-10-10 | 2010-09-21 | Roman Cement, Llc | High early strength pozzolan cement blends |
CN101618336B (en) | 2009-08-03 | 2012-05-23 | 大连理工大学 | Metal supported MCM-22 molecular sieve hollow sphere bifunctional catalyst preparation method and application thereof |
CN101862669B (en) * | 2010-06-23 | 2012-06-20 | 东南大学 | Catalyst for preparing isobutene through dehydrogenation of iso-butane and preparation method thereof |
-
2011
- 2011-11-10 CN CN201110353565.4A patent/CN103101926B/en active Active
-
2012
- 2012-10-30 WO PCT/CN2012/001474 patent/WO2013067765A1/en active Application Filing
- 2012-10-30 IN IN4224CHN2014 patent/IN2014CN04224A/en unknown
- 2012-10-30 US US14/356,704 patent/US9248437B2/en active Active
- 2012-10-30 KR KR1020147015502A patent/KR101915104B1/en active IP Right Grant
- 2012-10-30 EP EP12848497.9A patent/EP2778136B1/en active Active
- 2012-10-30 CA CA2855179A patent/CA2855179C/en active Active
Also Published As
Publication number | Publication date |
---|---|
CA2855179C (en) | 2019-12-24 |
KR20140118994A (en) | 2014-10-08 |
CN103101926A (en) | 2013-05-15 |
EP2778136A1 (en) | 2014-09-17 |
WO2013067765A1 (en) | 2013-05-16 |
EP2778136A4 (en) | 2015-08-12 |
US20140287910A1 (en) | 2014-09-25 |
CA2855179A1 (en) | 2013-05-16 |
US9248437B2 (en) | 2016-02-02 |
EP2778136B1 (en) | 2017-05-10 |
KR101915104B1 (en) | 2018-11-06 |
CN103101926B (en) | 2014-10-15 |
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