HUP0105237A2 - Mass spectrometric screening of catalysts - Google Patents

Mass spectrometric screening of catalysts

Info

Publication number
HUP0105237A2
HUP0105237A2 HU0105237A HUP0105237A HUP0105237A2 HU P0105237 A2 HUP0105237 A2 HU P0105237A2 HU 0105237 A HU0105237 A HU 0105237A HU P0105237 A HUP0105237 A HU P0105237A HU P0105237 A2 HUP0105237 A2 HU P0105237A2
Authority
HU
Hungary
Prior art keywords
reaction
mixed
test
products
catalyst
Prior art date
Application number
HU0105237A
Other languages
Hungarian (hu)
Inventor
Peter Chen
Christian Hinderling
Original Assignee
Thales Technologies Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Thales Technologies Ag filed Critical Thales Technologies Ag
Publication of HUP0105237A2 publication Critical patent/HUP0105237A2/en
Publication of HUP0105237A3 publication Critical patent/HUP0105237A3/en

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
    • G01N31/10—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using catalysis
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/0068—Means for controlling the apparatus of the process
    • B01J2219/00702—Processes involving means for analysing and characterising the products
    • B01J2219/00707—Processes involving means for analysing and characterising the products separated from the reactor apparatus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718—Type of compounds synthesised
    • B01J2219/0072—Organic compounds
    • B01J2219/00738—Organic catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718—Type of compounds synthesised
    • B01J2219/00745—Inorganic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718—Type of compounds synthesised
    • B01J2219/00745—Inorganic compounds
    • B01J2219/00747—Catalysts
    • C—CHEMISTRY; METALLURGY
    • C40—COMBINATORIAL TECHNOLOGY
    • C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
    • C40B30/00—Methods of screening libraries
    • C40B30/08—Methods of screening libraries by measuring catalytic activity
    • C—CHEMISTRY; METALLURGY
    • C40—COMBINATORIAL TECHNOLOGY
    • C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
    • C40B40/00—Libraries per se, e.g. arrays, mixtures
    • C40B40/18—Libraries containing only inorganic compounds or inorganic materials
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J49/00—Particle spectrometers or separator tubes

Abstract

A tal lm ny t rgya elj r s egy vegyület azonosít s ra, amely egy vlasztott reakcióban kataliz torként funkcion l, amelynek sor n - egyvagy t"bb teszt kataliz tort biztosítanak egy v lasztott katalitikusreakcióra; - a teszt kataliz torokat érintkeztetik egy v lasztottreakt ns vegyülettel olyan k"rülmények k"z"tt, amelyeknél a v lasztottkatalitikus reakció lej tszódhat és reakciótermékek keletkeznek areagens vegyületből; - a reakt ns vegyület b rmely katalitikusreakciój t kvencselik; - a kvencselt reakció termékeitt"megspektrometri val analiz lj k azon ionok azonosít s ra at"megspektrumban, amelyek egy vagy t"bb v lasztott reakciótermékkelvannak kapcsolatban, ahol a v lasztott reakciótermék b rmelyintermedier reakciótermék, amely a teszt kataliz torhoz vagy a tesztkataliz tor egy részéhez kapcsolódik; és - a v lasztottreakciótermékekkel kapcsolatos ionokat analiz lj k annak meghat roz sra, hogy mely teszt kataliz tor llította elő a v lasztott terméket, ésez ltal azon vegyületet azonosítj k, amely a v lasztott reakciókataliz toraként funkcion l. A tal lm ny t rgya tov bb elj r s a lncn"vekedési (propag l si) sebesség és a l nc tviteli sebesség ar nynak meghat roz s ra egy katalitikus polimeriz ciós reakcióban,amelynek sor n - egy teszt polimeriz ciós kataliz tort reag ltatnakegy v lasztott monomerrel a kiv lasztott reakciók"rülmények k"z"tt apolimer termékek kialakít s ra; - a reakciót kvencselik; - areakciótermékeket analiz lj k a kvencselt reakcióbólt"megspektrometria alkalmaz s val, mérik a p ros tagú l nc/p ratlantagú l nc eloszl st és ezzel a l ncn"vekedési sebesség l nc tvitelisebességhez viszonyított ar ny t meghat rozz k. ÓThe object of the invention is to identify a compound that functions as a catalyst in a selected reaction, in which order - one or more test catalysts are provided for a selected catalytic reaction; - the test catalysts are brought into contact with a selected reaction with a compound under conditions in which the mixed catalytic reaction can occur and reaction products are formed from the reagent compound; - any catalytic reaction of the reactive compound is quenched; - the products of the quenched reaction are analyzed by spectrometry to identify the ions that are associated with one or more mixed reaction products, where the mixed reaction product is an intermediate reaction product that is related to the test catalyst or a part of the test catalyst is connected; and - the ions associated with the mixed reaction products are analyzed to determine which test catalysis produced the mixed product, thereby identifying the compound that functions as the mixed reaction catalyst. the chain growth (propagation) speed and the chain transfer speed are determined in a catalytic polymerization reaction, during which - a test polymerization catalyst is reacted with a dissolved monomer under the conditions of the selected reactions for the formation of polymer products; - the reaction is quenched; - the reaction products from the quenched reaction are analyzed using spectrometry. size relative to transmission speed is determined. HE

HU0105237A 1999-01-22 2000-01-24 Mass spectrometric screening of catalysts HUP0105237A3 (en)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
CH12599 1999-01-22
US11720599P 1999-01-25 1999-01-25
US13641699P 1999-05-28 1999-05-28
CH114799 1999-06-21
PCT/IB2000/000062 WO2000043771A1 (en) 1999-01-22 2000-01-24 Mass spectrometric screening of catalysts

Publications (2)

Publication Number Publication Date
HUP0105237A2 true HUP0105237A2 (en) 2002-04-29
HUP0105237A3 HUP0105237A3 (en) 2003-08-28

Family

ID=27427768

Family Applications (1)

Application Number Title Priority Date Filing Date
HU0105237A HUP0105237A3 (en) 1999-01-22 2000-01-24 Mass spectrometric screening of catalysts

Country Status (8)

Country Link
EP (1) EP1149286A1 (en)
KR (1) KR20010093267A (en)
CN (1) CN1295506C (en)
AU (1) AU3068900A (en)
CZ (1) CZ20012641A3 (en)
HU (1) HUP0105237A3 (en)
PL (1) PL349046A1 (en)
WO (1) WO2000043771A1 (en)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7153916B2 (en) * 2001-03-12 2006-12-26 Tosoh Corporation Transition metal compound, catalyst for polymerization of olefin, and process for polymerization of ofelin using the catalyst
DE10140203A1 (en) * 2001-08-16 2003-02-27 Bayer Ag Catalysts for olefin polymerization
US6974665B2 (en) 2001-09-06 2005-12-13 University Of Nebraska In situ screening to optimize variables in organic reactions
CN105136972A (en) * 2015-09-09 2015-12-09 武汉理工大学 Comparison detection method for nano photocatalytic activity capability
KR102414474B1 (en) * 2016-03-16 2022-06-30 한국과학기술원 Method of Screening Optically Electrochemical Catalyst Using Fluorophore Metal-Organic Complex
US10825672B2 (en) * 2016-11-21 2020-11-03 Waters Technologies Corporation Techniques for mass analyzing a complex sample based on nominal mass and mass defect information

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4626412A (en) * 1984-12-14 1986-12-02 Monsanto Company Method and apparatus for carrying out catalyzed chemical reactions and for studying catalysts
DE69735411T2 (en) * 1996-10-09 2006-09-07 Symyx Technologies, Inc., Santa Clara INFRARED SPECTROSCOPY AND LIBRARY IMAGING

Also Published As

Publication number Publication date
PL349046A1 (en) 2002-07-01
EP1149286A1 (en) 2001-10-31
CN1340160A (en) 2002-03-13
WO2000043771A1 (en) 2000-07-27
CN1295506C (en) 2007-01-17
CZ20012641A3 (en) 2002-07-17
HUP0105237A3 (en) 2003-08-28
AU3068900A (en) 2000-08-07
KR20010093267A (en) 2001-10-27

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