HUP0003325A2 - Method for producing n-alkyl-n'-nitroguanidines - Google Patents

Method for producing n-alkyl-n'-nitroguanidines

Info

Publication number
HUP0003325A2
HUP0003325A2 HU0003325A HUP0003325A HUP0003325A2 HU P0003325 A2 HUP0003325 A2 HU P0003325A2 HU 0003325 A HU0003325 A HU 0003325A HU P0003325 A HUP0003325 A HU P0003325A HU P0003325 A2 HUP0003325 A2 HU P0003325A2
Authority
HU
Hungary
Prior art keywords
alkyl
nitroguanidines
producing
formula
cyanamide
Prior art date
Application number
HU0003325A
Other languages
Hungarian (hu)
Inventor
Reinhard Lantzsch
Original Assignee
Bayer Ag.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer Ag. filed Critical Bayer Ag.
Publication of HUP0003325A2 publication Critical patent/HUP0003325A2/en
Publication of HUP0003325A3 publication Critical patent/HUP0003325A3/en
Publication of HU224129B1 publication Critical patent/HU224129B1/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C277/00—Preparation of guanidine or its derivatives, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups
    • C07C277/08—Preparation of guanidine or its derivatives, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups of substituted guanidines

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

A találmány eljárás (I) általános képletű N-alkil-N'-nitro-guanidin-származékok - képletben R jelentése C1-C4-alkilcsoport -előállítására. Az eljárás során alkilamint salétromsavvalsemlegesítenek és a víz adott esetben elvégzett eltávolítása utáncianamiddal reagáltatnak, majd a kapott alkil-guanidin-nitrátotdehidratálják. ÓThe process of the invention is for the production of N-alkyl-N'-nitroguanidine derivatives of the general formula (I) - in the formula R is a C1-C4-alkyl group. During the process, the alkylamine is neutralized with nitric acid and after the water has been removed, where appropriate, it is reacted with cyanamide, and then the resulting alkyl guanidine nitrate is dehydrated. HE

HU0003325A 1997-03-27 1998-03-12 Method for producing n-alkyl-n'-nitroguanidines HU224129B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19712885A DE19712885A1 (en) 1997-03-27 1997-03-27 Process for the preparation of N-alkyl-N'-nitroguanidines
PCT/EP1998/001428 WO1998043951A1 (en) 1997-03-27 1998-03-12 Method for producing n-alkyl-n'-nitroguanidines

Publications (3)

Publication Number Publication Date
HUP0003325A2 true HUP0003325A2 (en) 2001-02-28
HUP0003325A3 HUP0003325A3 (en) 2001-03-28
HU224129B1 HU224129B1 (en) 2005-05-30

Family

ID=7824794

Family Applications (1)

Application Number Title Priority Date Filing Date
HU0003325A HU224129B1 (en) 1997-03-27 1998-03-12 Method for producing n-alkyl-n'-nitroguanidines

Country Status (14)

Country Link
US (1) US6114581A (en)
EP (1) EP0971886B1 (en)
JP (1) JP4010570B2 (en)
KR (1) KR100488197B1 (en)
CN (1) CN1119327C (en)
AT (1) ATE231123T1 (en)
AU (1) AU6830998A (en)
BR (1) BR9808051B1 (en)
DE (2) DE19712885A1 (en)
DK (1) DK0971886T3 (en)
ES (1) ES2187014T3 (en)
HU (1) HU224129B1 (en)
IL (1) IL131579A (en)
WO (1) WO1998043951A1 (en)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19939609A1 (en) * 1999-08-20 2001-02-22 Nigu Chemie Gmbh Pure 1-methyl-3-nitroguanidine preparation in high yield for use as insecticide intermediate, by reacting cyanogen halide with methylamine then ammonium nitrate and dehydrating product
DE19947332A1 (en) * 1999-10-01 2001-04-05 Nigu Chemie Gmbh Multi-stage production of 3-Alkyl-N-nitro-4H-1,3,5-oxadiazine-4-imine compounds from alkylamine and nitric acid via alkylammonium nitrate, alkylguanidine nitrate and alkylnitroguanidine
DE10000891A1 (en) * 2000-01-12 2001-07-19 Bayer Ag Process for the preparation of N-methyl-N'-nitroguanidine
DE10003834A1 (en) * 2000-01-28 2001-08-02 Nigu Chemie Gmbh Process for the preparation of 1-methyl-3-nitroguanidine
CN101565392A (en) * 2008-04-21 2009-10-28 南通天泽化工有限公司 Methyl nitroguanidine and preparation method thereof
CN105503661A (en) * 2016-01-12 2016-04-20 西安近代化学研究所 Method for synthesizing 1-amino-3-nitroguanidine

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IE960441L (en) * 1988-12-27 1990-06-27 Takeda Chemical Industries Ltd Guanidine derivatives, their production and insecticides
AU628229B2 (en) * 1989-11-10 1992-09-10 Agro-Kanesho Co. Ltd. Hexahydrotriazine compounds and insecticides

Also Published As

Publication number Publication date
ATE231123T1 (en) 2003-02-15
WO1998043951A1 (en) 1998-10-08
IL131579A0 (en) 2001-01-28
DE59806938D1 (en) 2003-02-20
BR9808051A (en) 2000-03-08
HUP0003325A3 (en) 2001-03-28
IL131579A (en) 2003-10-31
CN1251089A (en) 2000-04-19
KR100488197B1 (en) 2005-05-10
US6114581A (en) 2000-09-05
EP0971886B1 (en) 2003-01-15
DK0971886T3 (en) 2003-05-05
AU6830998A (en) 1998-10-22
KR20000075782A (en) 2000-12-26
CN1119327C (en) 2003-08-27
BR9808051B1 (en) 2009-12-01
ES2187014T3 (en) 2003-05-16
HU224129B1 (en) 2005-05-30
JP4010570B2 (en) 2007-11-21
JP2001516362A (en) 2001-09-25
DE19712885A1 (en) 1998-10-01
EP0971886A1 (en) 2000-01-19

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Legal Events

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Effective date: 20050401

MM4A Lapse of definitive patent protection due to non-payment of fees