GB983056A - Improvements in and relating to sulphonates - Google Patents

Improvements in and relating to sulphonates

Info

Publication number
GB983056A
GB983056A GB2910463A GB2910463A GB983056A GB 983056 A GB983056 A GB 983056A GB 2910463 A GB2910463 A GB 2910463A GB 2910463 A GB2910463 A GB 2910463A GB 983056 A GB983056 A GB 983056A
Authority
GB
United Kingdom
Prior art keywords
bleaching
hydrolysis
alkali metal
alkaline
hydrogen peroxide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2910463A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel AG and Co KGaA
Original Assignee
Henkel AG and Co KGaA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA
Publication of GB983056A publication Critical patent/GB983056A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/42—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/42—Separation; Purification; Stabilisation; Use of additives
    • C07C303/44—Separation; Purification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Detergent Compositions (AREA)

Abstract

"Olefin sulphonates" are prepared by reacting olefins having terminal double bonds and 8-22 carbon atoms with 1 to 1.7 moles per mole of olefin of gaseous SO3 in an inert diluent gas, at 20-100 DEG C., and bleaching the product, before, during, or after hydrolysis, with hydrogen peroxide or an alkali metal chlorite or hypochlorite, or materials forming these under the bleaching conditions. The sulphonating gas may contain 1-20% of SO3. The hydrolysis may be acid-usually achieved merely by adding water-or alkaline, when alkali metal or alkaline earth metal hydroxides, carbonates or bicarbonates, may be added, or amine bases may be used. The hydrogen peroxide may amount to 0.5-10% of the sulphonate weight, and other bleaching agents are used in equivalent quantities, the bleaching preferably occurring at 20-100 DEG C. The preferred bleaching conditions are pH 6-8, and 40-50 DEG C., using an alkali metal hypochlorite, after an alkaline hydrolysis.
GB2910463A 1962-08-01 1963-07-23 Improvements in and relating to sulphonates Expired GB983056A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEH46510A DE1185178B (en) 1962-08-01 1962-08-01 Process for the preparation of light colored olefin sulfonates

Publications (1)

Publication Number Publication Date
GB983056A true GB983056A (en) 1965-02-10

Family

ID=7156128

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2910463A Expired GB983056A (en) 1962-08-01 1963-07-23 Improvements in and relating to sulphonates

Country Status (2)

Country Link
DE (1) DE1185178B (en)
GB (1) GB983056A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3639282A (en) * 1968-07-01 1972-02-01 Chevron Res Hypochlorite bleaching of monoelefinic hydrocarbon sulfonates
JPS51138619A (en) * 1975-05-23 1976-11-30 Lion Corp Process for bleaching of olefinsulfonates
US4185034A (en) 1975-05-23 1980-01-22 Lion Fat & Oil Co., Ltd. Bleaching olefin sulfonates with phosphate and peroxide
US4197255A (en) * 1975-10-27 1980-04-08 Henkel Kommanditgesellschaft Auf Aktien (Henkel Kgaa) Method for the production of bleached, low-sultone olefin sulfonates

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1217367B (en) * 1964-04-08 1966-05-26 Farbwerke Hoechst Aktiengesellschaft vormals Meister Lucius & Brüning, Frankfurt/M Process for the preparation of alkene sulfonates
DE4017466A1 (en) * 1990-05-30 1991-12-05 Henkel Kgaa METHOD FOR PRODUCING LIGHT-COLORED PASTES OF ALPHA SULFAT FATTY ACID ALKYLESTER ALKALIMETAL SALTS

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3639282A (en) * 1968-07-01 1972-02-01 Chevron Res Hypochlorite bleaching of monoelefinic hydrocarbon sulfonates
JPS51138619A (en) * 1975-05-23 1976-11-30 Lion Corp Process for bleaching of olefinsulfonates
US4185034A (en) 1975-05-23 1980-01-22 Lion Fat & Oil Co., Ltd. Bleaching olefin sulfonates with phosphate and peroxide
US4197255A (en) * 1975-10-27 1980-04-08 Henkel Kommanditgesellschaft Auf Aktien (Henkel Kgaa) Method for the production of bleached, low-sultone olefin sulfonates

Also Published As

Publication number Publication date
DE1185178B (en) 1965-01-14

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