GB930751A - Improvements in or relating to the production of metal halides - Google Patents

Improvements in or relating to the production of metal halides

Info

Publication number
GB930751A
GB930751A GB3001159A GB3001159A GB930751A GB 930751 A GB930751 A GB 930751A GB 3001159 A GB3001159 A GB 3001159A GB 3001159 A GB3001159 A GB 3001159A GB 930751 A GB930751 A GB 930751A
Authority
GB
United Kingdom
Prior art keywords
metal
liner
aluminium
titanium
halides
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB3001159A
Inventor
Wilfrid Cooper
George Vaughan
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dunlop Rubber Co Ltd
Original Assignee
Dunlop Rubber Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dunlop Rubber Co Ltd filed Critical Dunlop Rubber Co Ltd
Priority to GB3001159A priority Critical patent/GB930751A/en
Publication of GB930751A publication Critical patent/GB930751A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/48—Halides, with or without other cations besides aluminium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G1/00—Methods of preparing compounds of metals not covered by subclasses C01B, C01C, C01D, or C01F, in general
    • C01G1/06—Halides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/02—Halides of titanium

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Chemical Vapour Deposition (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)

Abstract

Metal halides, which volatalize at temperatures below the melting point of the parent metal, particularly aluminium and titanium iodides are prepared by contacting gaseous halogen with heated metal in an evacuated reaction vessel provided with a removable liner of the same metal or of a different metal that forms an inert coherent halide film in operation. According to examples (i) a glass tube, fitted with an aluminium liner sealed to the glass with asbestos wool was filled with coarse aluminium and heated to 500 DEG -525 DEG C. under vacuum after which at 600 DEG C., iodine vapour was reacted to form the triiodide. After several runs the liner was removed and pulverised to form a fresh charge of metal, (ii) a similar run was effected with a titanium lined metal to form, at 650 DEG C., titanium tetraiodide. Reference is made to molybdenum fluorination using a copper liner and to the production of the halides of Al, Ti and Zr, tetrachlorides of V and Mo and to tungsten hexa-chloride and hexabromide.
GB3001159A 1959-09-02 1959-09-02 Improvements in or relating to the production of metal halides Expired GB930751A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB3001159A GB930751A (en) 1959-09-02 1959-09-02 Improvements in or relating to the production of metal halides

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB3001159A GB930751A (en) 1959-09-02 1959-09-02 Improvements in or relating to the production of metal halides

Publications (1)

Publication Number Publication Date
GB930751A true GB930751A (en) 1963-07-10

Family

ID=10300831

Family Applications (1)

Application Number Title Priority Date Filing Date
GB3001159A Expired GB930751A (en) 1959-09-02 1959-09-02 Improvements in or relating to the production of metal halides

Country Status (1)

Country Link
GB (1) GB930751A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1996020892A1 (en) * 1995-01-06 1996-07-11 Materials Research Corporation METHODS AND SYSTEMS FOR PRODUCING ULTRA HIGH PURITY TITANIUM TETRAIODIDE (TiI4) AND ULTRA HIGH PURITY TITANIUM METAL
EP1184339A2 (en) * 2000-09-01 2002-03-06 A.R.T.-Photonics GmbH Optical fibre and manufacturing processes for an optical fibre

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1996020892A1 (en) * 1995-01-06 1996-07-11 Materials Research Corporation METHODS AND SYSTEMS FOR PRODUCING ULTRA HIGH PURITY TITANIUM TETRAIODIDE (TiI4) AND ULTRA HIGH PURITY TITANIUM METAL
EP1184339A2 (en) * 2000-09-01 2002-03-06 A.R.T.-Photonics GmbH Optical fibre and manufacturing processes for an optical fibre
EP1184339A3 (en) * 2000-09-01 2002-09-04 A.R.T.-Photonics GmbH Optical fibre and manufacturing processes for an optical fibre
US6564587B2 (en) 2000-09-01 2003-05-20 Viatcheslav Artiouchenko Method of producing an optical fiber by gathering material from a molten bath

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