GB884775A - Hydrazinium salts - Google Patents
Hydrazinium saltsInfo
- Publication number
- GB884775A GB884775A GB9049/59A GB904959A GB884775A GB 884775 A GB884775 A GB 884775A GB 9049/59 A GB9049/59 A GB 9049/59A GB 904959 A GB904959 A GB 904959A GB 884775 A GB884775 A GB 884775A
- Authority
- GB
- United Kingdom
- Prior art keywords
- lower alkyl
- alkyl
- prepared
- hydroxy
- alkenyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/22—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with hetero atoms directly attached to ring nitrogen atoms
- C07D295/28—Nitrogen atoms
- C07D295/30—Nitrogen atoms non-acylated
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L75/00—Compositions of polyureas or polyurethanes; Compositions of derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M1/00—Liquid compositions essentially based on mineral lubricating oils or fatty oils; Their use as lubricants
- C10M1/08—Liquid compositions essentially based on mineral lubricating oils or fatty oils; Their use as lubricants with additives
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/02—Water
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2211/00—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
- C10M2211/02—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions containing carbon, hydrogen and halogen only
- C10M2211/022—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions containing carbon, hydrogen and halogen only aliphatic
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2211/00—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
- C10M2211/06—Perfluorinated compounds
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2215/042—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/08—Amides
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/08—Amides
- C10M2215/082—Amides containing hydroxyl groups; Alkoxylated derivatives
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/18—Containing nitrogen-to-nitrogen bonds, e.g. hydrazine
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
- C10M2215/221—Six-membered rings containing nitrogen and carbon only
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
- C10M2215/225—Heterocyclic nitrogen compounds the rings containing both nitrogen and oxygen
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
- C10M2215/225—Heterocyclic nitrogen compounds the rings containing both nitrogen and oxygen
- C10M2215/226—Morpholines
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/26—Amines
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/28—Amides; Imides
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/30—Heterocyclic compounds
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2217/04—Macromolecular compounds from nitrogen-containing monomers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2217/046—Polyamines, i.e. macromoleculars obtained by condensation of more than eleven amine monomers
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2217/06—Macromolecular compounds obtained by functionalisation op polymers with a nitrogen containing compound
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- General Chemical & Material Sciences (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Stable oil and water emulsions are prepared by the addition of carbon tetrachloride to aqueous solutions of hydrazinium salts of the formula <FORM:0884775/III/1> (wherein R is an alkyl- or alkenyl-amino lower alkyl, alkyl- or alkenyl-carbonylamino lower alkyl, alkyl- or alkenyl-carbonyloxy lower alkyl, saturated or unsaturated aliphatic hydrocarbon or alkycarbonyloxy lower alkylamino lower alkyl radical containing a total of 8 to 24 carbon atoms; or R is an N:N-disubstituted-amino lower alkyl group, the substituents being alkyl, hydroxy lower alkyl, hydroxypoly lower alkoxy lower alkyl, alkyl- or alkenyl-carbonyloxy lower alkyl or alkenylcarbonyl radicals, the total maximum number of carbon atoms being 50; R1 is an aliphatic hydrocarbon, hydroxy lower alkyl, hydroxy lower alkoxy, lower alkyl, hydroxypoly lower alkoxy lower alkyl, alkyl- or -alkenylcarbonyloxy lower alkyl, alkylcarbonylamino lower alkyl or alkylcarbonyloxy lower alkylamino lower alkyl radical containing a total of 1 to 50 carbon atoms; R11 is a lower alkyl, hydroxy lower alkyl, hydroxy lower alkoxy lower alkyl, hydroxypoly lower alkoxy lower alkyl, alkyl carbonyloxy lower alkyl or alkylcarbonyloxy lower alkylamino lower alkyl radical; or R1 and R11 together with the adjacent nitrogen atom form a morpholine ring or a piperazine ring which may be substituted on the free nitrogen atom by an alkanoyl radical: X is a chloride, bromide or iodide ion, and "lower" signifies a radical having 1 to 4 carbon atoms) excluding the hydrazinium chlorides described and claimed in Specification 824,357. Specifications 858,488 and U.S.A. Specifications 2,404,695, 2,678,258 and 2,710,248 also are referred to.ALSO:<FORM:0884775/IV (a)/1> hydrazinium chloride is reacted with tolylene diisocyanate isomers (Nacconate 80) to give a granular polymer, the equation for the formation of which is <FORM:0884775/IV (a)/2> Specification 858,488 and U.S.A. Specifications 2,404,695, 2,678,258 and 2,710,248 are referred to.ALSO:The invention comprises hydrazinium compounds of the general formula <FORM:0884775/IV (b)/1> wherein R is an alkyl- or alkenyl-amino lower alkyl, alkyl- or alkenyl-carbonylamino lower alkyl, alkyl- or alkenyl-carbonyloxy lower alkyl, saturated or unsaturated aliphatic hydrocarbon of alkylcarbonyloxy lower alkylamino lower alkyl radical containing a total of 8 to 24 carbon atoms; or R is an N : N-disubstituted-amino lower alkyl group, the substituents being alkyl, hydroxy lower alkyl, hydroxypoly lower alkoxy lower alkyl, alkyl- or alkenyl-carbonyloxy lower alkyl or alkenylcarbonyl radicals, the total maximum number of carbon atoms being 50; R1 is an aliphatic hydrocarbon, hydroxy lower alkyl, hydroxy lower alkoxy-lower alkyl, hydroxypoly lower alkoxy lower alkyl, alkyl- or -alkenylcarbonyloxy lower alkyl, alkylcarbonylaminolower alkyl or alkylcarbonyloxy lower alkylaminolower alkyl radical containing a total of 1 to 50 carbon atoms; R11 is a lower alkyl, hydroxy lower alkyl, hydroxy lower alkoxy lower alkyl, hydroxypoly lower alkoxy lower alkyl, alkylcarbonyloxy lower alkyl or alkyl-carbonyloxy lower alkyl amino lower alkyl radical; or R1 and R11 together with the adjacent nitrogen atom form a morpholine ring or a piperazine ring which may be substituted on the free nitrogen atom by an alkanoyl radical; X is a chloride, bromide or iodide ion, and "lower" signifies a radical having 1 to 4 carbon atoms) but excludes the hydrazinium chlorides described and claimed in Specification 824,357. The chlorides may be prepared by reacting chloramine with the appropriate tertiary amine, or by direct reaction of chlorine, ammonia and the amine, the bromides and iodides being prepared by a metathetical reaction between the hydrazinium chlorides and for example, alkali metal salts of the desired anion. Esters and amides may be prepared from hydrazinium salts, containing hydroxy or amino groups respectively, and acids. Examples are given and salts of the hydrazinium cations of the invention with anions derived from penicillin, sulphonamides, detergent sulphates, barbiturates and N : N - dimethyldithiocarbamic, hexafluorophosphoric, mercuri-iodic and picric acids are described or referred to. 4 - (Oleoylaminopropyl) - morpholine is prepared from oleic acid and 4-(3-aminopropyl)-morpholine. 4 - Amino - 4 - (2 - hydroxyethyl) morpholinium chloride is prepared from 2 - hydroxyethyl - morpholine and chloramine. 4 - Amino - 4 - (3 - aminopropyl) - morpholinium chloride is prepared similarly, and is converted into a 5-nitrobarbiturate and a tannate. 4 - Stearoyl - 1 - [2 - (stearoylamino) - ethyl] - piperazine is prepared by heating aminoethylpiperazine distearate. 3 - Stearoylaminopropyldimethylamine is prepared by heating stearic acid with dimethylaminopropylamine. 3 - Lauroylaminopropyldimethylamine is prepared similarly. A mixture of hydroxyethylated diamines of the formula <FORM:0884775/IV (b)/2> (wherein R is the hydrocarbon radical of hydrogenated tallow fatty acids) is prepared by reacting tallowamine with acrylonitrile, reducing the nitrile so formed to the amine RNHCH2CH2 CH2NH2 and reacting this with ethylene oxide A mixture of amines having the structures <FORM:0884775/IV (b)/3> is prepared similarly. Tetra - (2 - hydroxypropyl) - ethylenediamine is prepared from ethylene diamine and propylene oxide, and is converted to a mono stearate by reaction with stearic acid. The corresponding mono-oleate is prepared similarly. 1 : 1 - Bis - (2 - hydroxyethyl) - 2 - (oleoyloxy) - ethane is prepared by heating triethanolamine oleate. Tertiary-butylamine sulphate is prepared by reacting urea with isobutylene to give t-butyl-urea and hydrolysing this with sulphuric acid. Specification 858,488 and U.S.A. Specifications 2,404,695, 2,678,258 and 2,710,248 also are referred to.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB9049/59A GB884775A (en) | 1959-03-16 | 1959-03-16 | Hydrazinium salts |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB9049/59A GB884775A (en) | 1959-03-16 | 1959-03-16 | Hydrazinium salts |
Publications (1)
Publication Number | Publication Date |
---|---|
GB884775A true GB884775A (en) | 1961-12-20 |
Family
ID=9864417
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB9049/59A Expired GB884775A (en) | 1959-03-16 | 1959-03-16 | Hydrazinium salts |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB884775A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1651726B1 (en) * | 2003-08-04 | 2008-03-19 | Akzo Nobel N.V. | Process for the manufacture of a bitumen-aggregate mix suitable for road pavement |
-
1959
- 1959-03-16 GB GB9049/59A patent/GB884775A/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1651726B1 (en) * | 2003-08-04 | 2008-03-19 | Akzo Nobel N.V. | Process for the manufacture of a bitumen-aggregate mix suitable for road pavement |
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