GB786381A - Polymeric materials - Google Patents

Polymeric materials

Info

Publication number
GB786381A
GB786381A GB14691/55A GB1469155A GB786381A GB 786381 A GB786381 A GB 786381A GB 14691/55 A GB14691/55 A GB 14691/55A GB 1469155 A GB1469155 A GB 1469155A GB 786381 A GB786381 A GB 786381A
Authority
GB
United Kingdom
Prior art keywords
vinyl
acid
beta
allyl
methyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB14691/55A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Societe dElectro Chimie dElectro Metallurgie et des Acieries Electriques Dugine SA SECEMAU
Original Assignee
Societe dElectro Chimie dElectro Metallurgie et des Acieries Electriques Dugine SA SECEMAU
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Societe dElectro Chimie dElectro Metallurgie et des Acieries Electriques Dugine SA SECEMAU filed Critical Societe dElectro Chimie dElectro Metallurgie et des Acieries Electriques Dugine SA SECEMAU
Publication of GB786381A publication Critical patent/GB786381A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M103/00—Lubricating compositions characterised by the base-material being an inorganic material
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C3/00—Glass compositions
    • C03C3/12—Silica-free oxide glass compositions
    • C03C3/16—Silica-free oxide glass compositions containing phosphorus
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C3/00—Glass compositions
    • C03C3/12—Silica-free oxide glass compositions
    • C03C3/16—Silica-free oxide glass compositions containing phosphorus
    • C03C3/17—Silica-free oxide glass compositions containing phosphorus containing aluminium or beryllium
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C3/00—Glass compositions
    • C03C3/12—Silica-free oxide glass compositions
    • C03C3/16—Silica-free oxide glass compositions containing phosphorus
    • C03C3/19—Silica-free oxide glass compositions containing phosphorus containing boron
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F20/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride, ester, amide, imide or nitrile thereof
    • C08F20/02—Monocarboxylic acids having less than ten carbon atoms, Derivatives thereof
    • C08F20/10—Esters
    • C08F20/12—Esters of monohydric alcohols or phenols
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F20/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride, ester, amide, imide or nitrile thereof
    • C08F20/02—Monocarboxylic acids having less than ten carbon atoms, Derivatives thereof
    • C08F20/10—Esters
    • C08F20/40—Esters of unsaturated alcohols, e.g. allyl (meth)acrylate
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F20/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride, ester, amide, imide or nitrile thereof
    • C08F20/62—Monocarboxylic acids having ten or more carbon atoms; Derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F36/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds
    • C08F36/02—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds the radical having only two carbon-to-carbon double bonds
    • C08F36/20—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds the radical having only two carbon-to-carbon double bonds unconjugated
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/12—Glass
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/24—Metal working without essential removal of material, e.g. forming, gorging, drawing, pressing, stamping, rolling or extruding; Punching metal
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/241—Manufacturing joint-less pipes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/242—Hot working
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/243—Cold working
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/244—Metal working of specific metals
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/244—Metal working of specific metals
    • C10N2040/245—Soft metals, e.g. aluminum
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/244—Metal working of specific metals
    • C10N2040/246—Iron or steel
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/244—Metal working of specific metals
    • C10N2040/247—Stainless steel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S71/00—Chemistry: fertilizers
    • Y10S71/903—Soil conditioner
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T29/00—Metal working
    • Y10T29/49—Method of mechanical manufacture
    • Y10T29/4981—Utilizing transitory attached element or associated separate material
    • Y10T29/49812—Temporary protective coating, impregnation, or cast layer

Abstract

Vinyl and allyl esters of beta,beta-dialkyl acrylic acids are prepared by the following methods: (a) in the case of vinyl esters by reaction of the acid with acetylene, or by transesterification of the acid with a vinyl ester, and (b) in the case of allyl esters by the esterification of the acid with allyl alcohol, by the transesterification of the acid with an allyl ester, or by the reaction of allyl chloride with a metallic salt of the acid. In examples: (1) vinyl beta-beta-dimethylacrylate is prepared by ester interchange between vinyl acetate and beta-beta-dimethylacrylic acid in the presence of mercuric sulphate as a catalyst, the reaction mixture being washed with a solution of sodium bicarbonate before distilling. The product is characterized by means of its density, boiling point and refractive index; (8) allyl beta-beta-dimethylacrylate is prepared by esterifying the acid with allyl alcohol in presence of sulphuric acid and benzene. The product is characterized by means of its density, boiling point and refractive index; (9) vinyl methyl-3-pentene-2-oate is prepared by ester interchange between the acid and vinyl acetate.ALSO:Insoluble, infusible three-dimensional polymers are obtained by polymerizing manomeric material which includes at least one monomer of the formula <FORM:0786381/IV (a)/1> in which R1 and R2 are alkyl radicals and R3 is a group comprising an ethylenic bond of the form CH2=C<, the polymerization being carried out in two stages of temperature: (1) at a temperature less than that which would cause gelification, e.g. 100 DEG C., thus obtaining a fusible soluble linear polymer, and (2) at a higher temperature in order to produce an insoluble, infusible polymer. Monomers specified are vinyl and allyl senecioates, the vinyl ester of methyl-3-pentene-2-oic acid and the N-allyl amide of senecioic acid. These compounds may be copolymerized with other monomers such as vinyl acetate, vinyl chloride, acrylic and alpha-substituted acrylic acids and their nitriles, amides and esters, e.g. methyl acrylate and methacrylate and acrylonitrile, styrene, alpha-methyl styrene, vinyl naphthalene, maleic anhydride, methyl vinyl and methyl isopropenyl ketones and vinyl alkyl ethers. The first stage of polymerization may be carried out in bulk, in solution in solvents such as benzine, or in aqueous emulsion with the acid of emulsifiers such as sulphonated diheptylsuccinate or a mixture of sodium sulphoricinoleate and a condensation product of ethylene oxide and oleyl alcohol. Catalysts may be employed such as barium and hydrogen peroxides, ammonium and potassium persulphates, benzoyl peroxide, cumene hydroperoxide and azo-diisobutyronitrile and redox systems including reducing agents such as sodium bisulphite and thiosulphate. Also present may be polymerization regulators such as halogenated hydrocarbons and mercaptans. In the second stage of polymerization the polymers, after preliminary processing if desired, are subjected to a higher temperature, e.g. 100-150 DEG C., with the addition, if required, of further quantities of catalyst.
GB14691/55A 1954-05-26 1955-05-20 Polymeric materials Expired GB786381A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1100960X 1954-05-26

Publications (1)

Publication Number Publication Date
GB786381A true GB786381A (en) 1957-11-20

Family

ID=9620728

Family Applications (2)

Application Number Title Priority Date Filing Date
GB14691/55A Expired GB786381A (en) 1954-05-26 1955-05-20 Polymeric materials
GB17010/55A Expired GB774248A (en) 1954-05-26 1955-06-13 Glass compositions

Family Applications After (1)

Application Number Title Priority Date Filing Date
GB17010/55A Expired GB774248A (en) 1954-05-26 1955-06-13 Glass compositions

Country Status (7)

Country Link
US (1) US2920972A (en)
BE (2) BE538888A (en)
CH (2) CH334653A (en)
DE (2) DE1100960B (en)
FR (4) FR1105938A (en)
GB (2) GB786381A (en)
NL (2) NL91245C (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3255139A (en) * 1962-03-21 1966-06-07 Bayer Ag Preparation of n-(alkenyloxymethylene) acrylamide copolymers and products thereof

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1065997B (en) * 1955-02-12 1959-09-24
DE1065996B (en) * 1955-02-12 1959-09-24 Societe Anonyme des Manufactures des Glaces et Produits Chimiques de Saint-Gobain, Chauny S. Cirey, Paris Alkali-phosphoric-acid-alumina glasses
FR1152757A (en) * 1956-05-25 1958-02-25 Saint Gobain Aluminum alkaline phosphoric glass compositions
US3067135A (en) * 1959-03-04 1962-12-04 Sulzer Frers S A Bearing comprising polytetrafluoroethylene and phosphate glass
US3067655A (en) * 1959-09-08 1962-12-11 Benjamin S Miller Artificial ice and snow and methods of making the same
DE1494078B2 (en) * 1960-01-08 1972-03-02 The Glacier Metal Co. Ltd., Wembley, Middlesex (Grossbritannien) MOLDING COMPOUNDS FOR THE MANUFACTURING OF SLIDING BEARINGS
NL272061A (en) * 1960-12-08
GB1002612A (en) * 1960-12-09 1965-08-25 Ian Griffith Slater Lubricant for use in the hot extrusion of metals and metal alloys
DE1257334B (en) * 1961-05-05 1967-12-28 Hydraulik Gmbh Lubricant plate template for pressing carbon steel blocks out of extrusion presses
NL289576A (en) * 1962-02-28
US3485646A (en) * 1965-10-21 1969-12-23 Ppg Industries Inc Glass compositions
DE1527820A1 (en) * 1966-08-19 1969-12-04 Mannesmann Meer Ag Process and system for the production of pipes and profiles, preferably made of steel, in extrusion presses using preheated plate-shaped disks made of silicates
US3926649A (en) * 1971-10-15 1975-12-16 Ici Ltd Borosphosphate glass compositions with high water resistance and low softening point
US3964919A (en) * 1972-02-14 1976-06-22 Imperial Chemical Industries Limited Glass compositions
GB1395942A (en) * 1972-04-27 1975-05-29 Ici Ltd Inorganic oxide glasses
GB1404622A (en) * 1972-06-08 1975-09-03 Ici Ltd Phosphate glass
GB1404914A (en) * 1973-02-21 1975-09-03 Ici Ltd Optical article
US3979322A (en) * 1973-04-09 1976-09-07 Nikolai Efimovich Alexeev Phosphate glass for laser use
US3958973A (en) * 1973-10-18 1976-05-25 Ferro Corporation Micronutrient metal-containing phosphate glasses
US3930833A (en) * 1973-10-18 1976-01-06 Ferro Corporation Micronutrient metal-containing phosphate glasses
GB1501735A (en) * 1975-09-19 1978-02-22 Ici Ltd Phosphate glass composition
US4076541A (en) * 1976-03-22 1978-02-28 Owens-Illinois, Inc. Glasses suitable for laser application, glass lasers, and method for making same
US4110002A (en) * 1977-03-02 1978-08-29 Gte Laboratories Incorporated Optical fibers formed of aluminum borophosphate glass compositions
US4202700A (en) * 1979-05-02 1980-05-13 The United States Of America As Represented By The United States Department Of Energy Glassy composition for hermetic seals
GB2057420B (en) * 1979-08-30 1984-05-10 Standard Telephones Cables Ltd Controlled release glass
NL8104778A (en) * 1981-10-22 1983-05-16 Philips Nv PRECISIONALLY PRESSED GLASS OPTICS AND SUITABLE GLASS.
FR2542228B1 (en) * 1983-03-10 1985-08-02 Cegedur PRESSURE SINTERING OF ALUMINUM ALLOY POWDERS

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1016352A (en) * 1908-07-09 1912-02-06 Charles Nicholas Meriwether Phosphate and the method of making same.
US1654404A (en) * 1924-12-23 1927-12-27 Stockholders Syndicate Acid metal phosphate and process of making same
US2192939A (en) * 1937-05-17 1940-03-12 Owens Corning Fiberglass Corp Agricultural application of glass wool
US2273891A (en) * 1939-02-18 1942-02-24 Pittsburgh Plate Glass Co Method of polymerizing polymerizable materials containing more than one polymerizable grouping
GB658426A (en) * 1947-09-04 1951-10-10 Borden Co Improvements in or relating to a polymerisation process and products resulting therefrom

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3255139A (en) * 1962-03-21 1966-06-07 Bayer Ag Preparation of n-(alkenyloxymethylene) acrylamide copolymers and products thereof

Also Published As

Publication number Publication date
BE538888A (en)
NL91245C (en)
DE1100960B (en) 1961-03-02
CH334653A (en) 1958-12-15
CH337996A (en) 1959-04-30
DE1102351B (en) 1961-03-16
FR1105938A (en) 1955-12-09
FR67846E (en) 1958-03-24
FR67841E (en) 1958-03-24
GB774248A (en) 1957-05-08
FR1107913A (en) 1956-01-06
BE538225A (en)
US2920972A (en) 1960-01-12
NL197538A (en)

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