GB720487A - Lubricating greases - Google Patents
Lubricating greasesInfo
- Publication number
- GB720487A GB720487A GB5402/52A GB540252A GB720487A GB 720487 A GB720487 A GB 720487A GB 5402/52 A GB5402/52 A GB 5402/52A GB 540252 A GB540252 A GB 540252A GB 720487 A GB720487 A GB 720487A
- Authority
- GB
- United Kingdom
- Prior art keywords
- allyl
- acids
- copolymer
- maleic anhydride
- salts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M5/00—Solid or semi-solid compositions containing as the essential lubricating ingredient mineral lubricating oils or fatty oils and their use
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- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/04—Elements
- C10M2201/041—Carbon; Graphite; Carbon black
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- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/10—Compounds containing silicon
- C10M2201/102—Silicates
- C10M2201/103—Clays; Mica; Zeolites
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- C10M2201/10—Compounds containing silicon
- C10M2201/105—Silica
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- C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
- C10M2205/022—Ethene
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- C10M2205/024—Propene
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- C10M2207/122—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms monocarboxylic
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2010/00—Metal present as such or in compounds
- C10N2010/06—Groups 3 or 13
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2010/00—Metal present as such or in compounds
- C10N2010/08—Groups 4 or 14
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/02—Bearings
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2050/00—Form in which the lubricant is applied to the material being lubricated
- C10N2050/10—Semi-solids; greasy
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Abstract
Metallic salts of acidic copolymers of aliphatic vinyl compounds and a ,b -unsaturated polycarboxylic acids or anhydrides are added to lubricating oils as gelling agents to form lubricating greases. The vinyl compounds may be a -olefines, R - CH = CH2, where R is an alkyl radical having 1- to 30 carbon atoms, such as 1-dodecene, 1-hexadecene, 1-octadecene, and the higher olefines obtained by the thermal cracking of petroleum wax or waxy petroleum stocks; allyl esters R.COOCH2.CH=CH2 such as allyl laurate, myristate, palmitate, stearate and mixed allyl esters of hydrogenated fish oil fatty acids, or allyl esters of mixtures of stearic with oleic or linseed oil acids; allyl ethers, e.g. allyl methyl, amyl, heptyl, lauryl and hexadecyl ethers and methallyl butyl, octyl and octadecyl ethers, vinyl esters and vinyl ethers. Preferred polycarboxylic acids are maleic, fumaric, itaconic, glutaconic, mesaconic, citraconic and aconitic acids. The salts are those of metals of Group I to IV of the Periodic System particularly lithium, calcium, barium and aluminium. The copolymerization is carried out, with or without a solvent such as toluene, xylene, dioxane, and white oil, by heating with catalysts such as benzoyl, p di-t-butyl and lauryl peroxides and cumene hydroperoxide, and the copolymers are neutralized with the oxide, hydroxide or alcoholate of the metal or the alkali metal or ammonium salt may be reacted with the chloride, hydroxide, or carbonate of the metal whose salt is required. Examples are given of the preparation of allyl stearate-maleic anhydride, allyl stearate and oleate-maleic anhydride, allyl laurate-maleic anhydride, octadecene-maleic anhydride copolymers and a copolymer of the allyl ester of hydrogenated fish oil fatty acids with maleic anhydride. The salts may be formed in situ in the mineral oil vehicle, e.g. of a naphthenic paraffinic, or mixed base type, which may be replaced wholly or in part by synthetic oils of polyester, e.g. 2-ethyl hexyl sebacate, polyether, e.g. polyalkylene glycol, silicone, e.g. methyl polysiloxane, or polymer oil types, e.g. polyethylene. In a modification salts may be formed from a mixture of the copolymer with a saturated aliphatic monocarboxylic acid containing 10-22 carbon atoms, e.g. cupric, lauric, stearic, hydroxystearic and hydrogenated fish oil fatty acids. In a further modification, 1 to 2 per cent of an aliphatic monocarboxylic acid having less than 6 carbon atoms in the molecule, e.g. formic, acetic, butyric and valeric acids, may also be included and the resulting grease has a higher drop point. Additives such as rubber latex, polyisobutylene, acrylic ester polymers, sulphurized sperm oil, phenyl a -naphthylamine, phenothiazine, carbon black and silica flour may be included in the grease. U.S.A. Specifications 2,197,263 and 2,417,433 are referred to.ALSO:Lubricating greases comprise a lubricating oil and a metallic salt of an acidic copolymer of a long chain aliphatic vinyl compound and an a , b -unsaturated polycarboxylic acid or anhydride as gelling agent. The vinyl compounds may be a -olefines, R-CH=CH2, where R is an alkyl with 10-30 carbon atoms, such as 1-dodecene 1-hexadecene, 1-octadecene, and the higher olefines obtained by the thermal cracking of petroleum wax or petroleum stock; allyl esters, R.COOCH2 CH=CH2, such as allyl laurate, myristate, palmitate, stearate and mixed allyl esters of hydrogenated fish oil fatty acids, or allyl esters of mixtures such as stearic and oleic, and stearic and linseed oil acids; and allyl ethers, e.g. allyl methyl, amyl, heptyl, lauryl, hexadecyl ethers and methallyl, butyl, octyl and octadecyl ethers. Polycarboxylic acids mentioned are maleic, fumaric, itaconic, glutaconic, mesaconic, citraconic and aconitic acids and the salts are those of metals of the Periodic Groups I to IV, particularly lithium, calcium, barium and aluminium. Examples show the preparation of greases using Li, Ba, Ca, Al and Zn salts of a copolymer of allyl stearate with maleic anhydride; a calcium salt of a copolymer of allyl stearate and oleate with maleic anhydride; barium salts of a copolymer of allyl laurate and maleic anhydride; a calcium salt of a copolymer of an allyl ester of hydrogenated fish oil fatty acids and maleic anhydride; and the barium salt of an octadecene-maleic anhydride copolymer. In a modification, salts may be formed from a mixture of the copolymer with a saturated aliphatic monocarboxylic acid containing 10-22 carbon atoms, e.g. capric, lauric, stearic, hydroxystearic acids and hydrogenated fish oil fatty acids. The salts may be formed in situ in the mineral oil vehicle, e.g. of naphthenic, paraffinic or mixed base type, which may be replaced wholly or in part by synthetic oils of polyester, e.g. 2-ethylhexyl sebacate, polyether e.g. polyalkylene glycol, silicone e.g. methyl polysiloxane, or polymer oil types e.g. polyethylene. In a further modification, 1-2 per cent. of an aliphatic monocarboxylic acid having less than 6 carbon atoms in the molecule, e.g. formic, acetic, butyric and valeric acids, may also be included and the resulting grease has a higher drop point. The acidic copolymer and the higher molecular weight fatty acid are blended in an oil base by heating to about 150 DEG F. The low molecular weight acid and sufficient metallic oxide, hydroxide or salt to neutralize the three acidic components together with a small amount of water is added and the mixture stirred and heated at 300-400 DEG F. to permit saponification and dehydration to take place, the grease is then cooled. Additives such as rubber latex, polyisobutylene, acrylic ester polymers, sulphurized sperm oil, phenyl a -naphthylamine, phenothiazine, carbon black and silica flour may be included in the grease. U.S.A. Specifications 2,417,433 and 2,197,263 are referred to.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US215859A US2698298A (en) | 1951-03-15 | 1951-03-15 | Lubricating greases containing an acidic copolymer salt |
Publications (1)
Publication Number | Publication Date |
---|---|
GB720487A true GB720487A (en) | 1954-12-22 |
Family
ID=22804698
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB5402/52A Expired GB720487A (en) | 1951-03-15 | 1952-02-29 | Lubricating greases |
Country Status (3)
Country | Link |
---|---|
US (1) | US2698298A (en) |
FR (1) | FR1058915A (en) |
GB (1) | GB720487A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2143848A1 (en) * | 1970-09-23 | 1972-03-30 | Mobil Oll Corp , New York, N Y (V St A) | Grease |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2929785A (en) * | 1954-08-06 | 1960-03-22 | Exxon Research Engineering Co | Grease compositions containing salts of carboxylic copolymers |
US2868729A (en) * | 1957-02-26 | 1959-01-13 | Sinclair Refining Co | Lubricating oil thickened to a grease with an anhydrous calcium soap of an alkenyl substituted succinic acid |
US3076763A (en) * | 1958-04-28 | 1963-02-05 | Sinclair Research Inc | Calcium alkenyl succinate grease |
US3136725A (en) * | 1958-09-18 | 1964-06-09 | Sinclair Research Inc | Calcium alkenyl succinate grease making |
US3142643A (en) * | 1959-03-20 | 1964-07-28 | Exxon Research Engineering Co | Greases thickened with salts of copolymers of unsaturated dicarboxylic acid esters and vinyl acetate |
US3296131A (en) * | 1965-10-22 | 1967-01-03 | Sinclair Research Inc | Antifoamer for hydrocarbon oils |
US3422015A (en) * | 1966-12-16 | 1969-01-14 | Union Oil Co | Grease composition |
FR2205570B1 (en) * | 1972-11-07 | 1976-06-04 | Mobil Oil France | |
US4306980A (en) * | 1979-12-03 | 1981-12-22 | Nl Industries, Inc. | Invert emulsion well-servicing fluids |
US10858467B2 (en) * | 2013-10-28 | 2020-12-08 | Joseph Laurino | Conducting polymer, 1-octadecene, polymer with 2,5 furnadione, metal salts |
Family Cites Families (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE623404C (en) * | 1930-05-26 | |||
USRE22299E (en) * | 1938-09-24 | 1943-04-13 | Lubricating composition | |
US2197263A (en) * | 1939-02-23 | 1940-04-16 | Socony Vacuum Oil Co Inc | Grease composition |
US2394595A (en) * | 1943-08-09 | 1946-02-12 | Fred A Corbin | Apparatus for controlling the pressure of furnace gases |
US2460035A (en) * | 1946-01-25 | 1949-01-25 | Standard Oil Dev Co | Synthetic lubricant |
US2533376A (en) * | 1946-06-14 | 1950-12-12 | Libbey Owens Ford Glass Co | Copolymerization of maleic anhydride and allyl esters of long chain monocarboxylic acids |
US2497432A (en) * | 1947-04-03 | 1950-02-14 | Monsanto Chemicals | Antirusting composition |
US2615864A (en) * | 1947-06-21 | 1952-10-28 | Socony Vacuum Oil Co Inc | Esterified allyl ester-polycarboxylic acid copolymers |
US2543964A (en) * | 1947-07-09 | 1951-03-06 | Socony Vacuum Oil Co Inc | Mineral oil compositions containing copolymers of olefins and esters of alpha, beta-unsaturated polybasic acids |
US2491028A (en) * | 1947-10-11 | 1949-12-13 | Standard Oil Dev Co | Lubricating grease compositions |
US2570788A (en) * | 1948-02-17 | 1951-10-09 | Socony Vacuum Oil Co Inc | Synthetic lubricants |
US2483960A (en) * | 1948-02-26 | 1949-10-04 | Monsanto Chemicals | Polymerization of vinyl halides in an aqueous dispersion |
US2483959A (en) * | 1948-02-26 | 1949-10-04 | Monsanto Chemicals | Vinyl chloride polymer compositions containing maleic-vinyl acetate heteropolymers and compounds of lead, calcium, or barium |
US2542542A (en) * | 1948-08-02 | 1951-02-20 | Standard Oil Dev Co | Lubricating oil additives |
US2615845A (en) * | 1948-08-02 | 1952-10-28 | Standard Oil Dev Co | Lubricating oil additives |
US2577706A (en) * | 1948-11-26 | 1951-12-04 | California Research Corp | High melting-high water-resistant grease |
US2637698A (en) * | 1948-12-30 | 1953-05-05 | Standard Oil Dev Co | Mineral oil lubricating composition containing a copolymer of an alkyl ester of itaconic acid and an alkyl acrylate or methacrylate |
US2513680A (en) * | 1949-01-18 | 1950-07-04 | Socony Vacuum Oil Co Inc | Lime base grease |
US2634256A (en) * | 1949-02-15 | 1953-04-07 | Standard Oil Dev Co | Modified olefin-diolefin resin |
US2565981A (en) * | 1949-02-18 | 1951-08-28 | Standard Oil Dev Co | Production of lubricating grease |
US2616849A (en) * | 1949-05-11 | 1952-11-04 | Socony Vacuum Oil Co Inc | Copolymers of maleic anhydride with esters of itaconic acid and salts thereof as viscosity index improvers and pour point depressants |
-
1951
- 1951-03-15 US US215859A patent/US2698298A/en not_active Expired - Lifetime
-
1952
- 1952-02-29 GB GB5402/52A patent/GB720487A/en not_active Expired
- 1952-03-14 FR FR1058915D patent/FR1058915A/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2143848A1 (en) * | 1970-09-23 | 1972-03-30 | Mobil Oll Corp , New York, N Y (V St A) | Grease |
Also Published As
Publication number | Publication date |
---|---|
US2698298A (en) | 1954-12-28 |
FR1058915A (en) | 1954-03-19 |
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