GB546596A - A process for the manufacture of quaternary ammonium compounds - Google Patents
A process for the manufacture of quaternary ammonium compoundsInfo
- Publication number
- GB546596A GB546596A GB1752740A GB1752740A GB546596A GB 546596 A GB546596 A GB 546596A GB 1752740 A GB1752740 A GB 1752740A GB 1752740 A GB1752740 A GB 1752740A GB 546596 A GB546596 A GB 546596A
- Authority
- GB
- United Kingdom
- Prior art keywords
- pyridine
- malonic acid
- ammonium chloride
- chloride
- quaternary ammonium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Abstract
546,596. Crotonic acid betaine compounds. ROCHE PRODUCTS, Ltd., BERGEL, F., COHEN, A., and HINDLEY, N. C. Dec. 10, 1940, No. 17527. [Class 2 (iii)] Crotonic acid betaine compounds and quaternary ammonium compounds of similar constitution are prepared by the condensation of malonic acid with a quaternary ammonium salt of the general formula where R, R<SP>1</SP>, and R" are alkyl aryl; or aralkyl groups and X is halogen. The condensation is preferably carried out in the presence of a base such as pyridine. In examples (1) a reaction mixture comprising malonic acid, anhydrous pyridine and the hydrate of trimethylethylal-ammonium chloride is heated on the water bath, evaporated to dryness, and purified by. fractional precipitation to give crotonic acid betaine chloride. (2) Triethylethylalammonium chloride, malonic acid and dry pyridine are heated on a hot water bath and worked up as in example (1) and the product purified by formation of a reineckate to form γ-carboxyallyl-triethyl ammonium chloride. (3) Trimethyl-#-propional-ammonium chloride, malonic acid and dry 'pyridine are treated as in example (1) to produce #-carboxy-# γ-#- butenyltrimethyl ammonium chloride.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1752740A GB546596A (en) | 1940-12-10 | 1940-12-10 | A process for the manufacture of quaternary ammonium compounds |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1752740A GB546596A (en) | 1940-12-10 | 1940-12-10 | A process for the manufacture of quaternary ammonium compounds |
Publications (1)
Publication Number | Publication Date |
---|---|
GB546596A true GB546596A (en) | 1942-07-21 |
Family
ID=10096732
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1752740A Expired GB546596A (en) | 1940-12-10 | 1940-12-10 | A process for the manufacture of quaternary ammonium compounds |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB546596A (en) |
-
1940
- 1940-12-10 GB GB1752740A patent/GB546596A/en not_active Expired
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